2-HYDROXYMETHYL-1,3-DIOXOLANE
- Product Name
- 2-HYDROXYMETHYL-1,3-DIOXOLANE
- CAS No.
- 5694-68-8
- Chemical Name
- 2-HYDROXYMETHYL-1,3-DIOXOLANE
- Synonyms
- 1,3-dioxane-2-methanol;1,3-Dioxolane-2-methanol;2-HYDROXYMETHYL-1,3-DIOXOLANE;2-HydroxyMethyl-1,3-dioxolaneC4H8O3
- CBNumber
- CB5439179
- Molecular Formula
- C4H8O3
- Formula Weight
- 104.1
- MOL File
- 5694-68-8.mol
2-HYDROXYMETHYL-1,3-DIOXOLANE Property
- Boiling point:
- 97 °C
- Density
- 1.164±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- pka
- 14.83±0.10(Predicted)
- form
- liquid
- color
- Colourless to light yellow
- InChI
- InChI=1S/C4H8O3/c5-3-4-6-1-2-7-4/h4-5H,1-3H2
- InChIKey
- ZAGUSKAXELYWCE-UHFFFAOYSA-N
- SMILES
- O1CCOC1CO
Safety
- RIDADR
- UN1993
- HS Code
- 2909200090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
N-Bromosuccinimide Price
- Product number
- D495680
- Product name
- (1,3-Dioxolan-2-yl)methanol
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- 2093AL
- Product name
- 2-Hydroxymethyl-1,3-dioxolane
- Packaging
- 10g
- Price
- $512
- Updated
- 2021/12/16
- Product number
- A220670
- Product name
- (1,3-Dioxolan-2-yl)methanol
- Purity
- 95%
- Packaging
- 250mg
- Price
- $20
- Updated
- 2021/12/16
- Product number
- A220670
- Product name
- (1,3-Dioxolan-2-yl)methanol
- Purity
- 95%
- Packaging
- 1g
- Price
- $58
- Updated
- 2021/12/16
- Product number
- O33317
- Product name
- (1,3-dioxolan-2-yl)methanol
- Purity
- 97%
- Packaging
- 1G
- Price
- $100
- Updated
- 2021/12/16
2-HYDROXYMETHYL-1,3-DIOXOLANE Chemical Properties,Usage,Production
Synthesis
71516-48-8
5694-68-8
General procedure for the synthesis of 1,3-dioxane-2-methanol from the compound (CAS: 71516-48-8): (66b) Preparation of 1,3-dioxan-2-ylmethanol: To a solution of 2-((benzyloxy)methyl)-1,3-dioxan-2-ylmethanol (3.01 g, 15.5 mmol) in methanol (100 mL), obtained in the previous step (66a), was Palladium hydroxide (20 wt% Pd (dry basis) carbon, wet (up to 50% water)) (300 mg) was added. The reaction mixture was stirred at room temperature for 15 hours under hydrogen atmosphere. Upon completion of the reaction, the gas in the reaction vessel was displaced with nitrogen, the catalyst was removed by filtration through diatomaceous earth and washed with methanol. The filtrate was concentrated and dried under reduced pressure to afford 1,3-dioxane-2-methanol (1.57 g, 97.3% yield) as a light yellow oil.1H NMR (400 MHz, CDCl3) δ ppm: 1.89 (1H, br s), 3.66-3.72 (2H, m), 3.88-4.08 (4H, m), 5.01 (1H, t, J = 3 Hz).
References
[1] Patent: US2007/10542, 2007, A1. Location in patent: Page/Page column 82
2-HYDROXYMETHYL-1,3-DIOXOLANE Preparation Products And Raw materials
Raw materials
Preparation Products
2-HYDROXYMETHYL-1,3-DIOXOLANE Suppliers
- Tel
- --
- Fax
- --
- synthon@synthon-chemicals.com
- Country
- Germany
- ProdList
- 2000
- Advantage
- 65
- Tel
- --
- Fax
- --
- sales@chemos-group.com
- Country
- Germany
- ProdList
- 6350
- Advantage
- 71
View Lastest Price from 2-HYDROXYMETHYL-1,3-DIOXOLANE manufacturers
- Product
- 2-HYDROXYMETHYL-1,3-DIOXOLANE 5694-68-8
- Price
- US $0.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 10000KGS
- Release date
- 2025-03-19