3-NITROBENZENESULFONAMIDE
- Product Name
- 3-NITROBENZENESULFONAMIDE
- CAS No.
- 121-52-8
- Chemical Name
- 3-NITROBENZENESULFONAMIDE
- Synonyms
- 3-Nitrobenzolesulfamide;3-nitrophenylsulfonamide;M-NITROBENZENESULFONAMIDE;3-NITROBENZENESULFONAMIDE;3-nitro-benzenesulfonamid;m-nitrobenzenesulphonamide;3 Nito Benzene Sulfonamide;Benzenesulfonamide, m-nitro-;Benzenesulfonamide, 3-nitro-;3-nitrobenzene-1-sulfonaMide
- CBNumber
- CB5440265
- Molecular Formula
- C6H6N2O4S
- Formula Weight
- 202.19
- MOL File
- 121-52-8.mol
3-NITROBENZENESULFONAMIDE Property
- Melting point:
- 166-168 °C (lit.)
- Boiling point:
- 407.7±47.0 °C(Predicted)
- Density
- 1.505 (estimate)
- refractive index
- 1.6490 (estimate)
- storage temp.
- Sealed in dry,Room Temperature
- pka
- 9.47±0.60(Predicted)
- form
- Powder
- color
- White to off-white
- Water Solubility
- 444.8mg/L(15 ºC)
- CAS DataBase Reference
- 121-52-8(CAS DataBase Reference)
- EPA Substance Registry System
- Benzenesulfonamide, 3-nitro- (121-52-8)
Safety
- Hazard Codes
- Xi
- Risk Statements
- 36/37/38
- Safety Statements
- 26-37/39-36
- WGK Germany
- 3
- TSCA
- Yes
- HS Code
- 29350090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- 296422
- Product name
- 3-Nitrobenzenesulfonamide
- Purity
- 99%
- Packaging
- 5g
- Price
- $26
- Updated
- 2023/06/20
- Product number
- 296422
- Product name
- 3-Nitrobenzenesulfonamide
- Purity
- 99%
- Packaging
- 25g
- Price
- $69.2
- Updated
- 2023/01/07
- Product number
- N0696
- Product name
- 3-Nitrobenzenesulfonamide
- Purity
- >98.0%(HPLC)(N)
- Packaging
- 5g
- Price
- $16
- Updated
- 2025/07/31
- Product number
- N0696
- Product name
- 3-Nitrobenzenesulfonamide
- Purity
- >98.0%(HPLC)(N)
- Packaging
- 25g
- Price
- $43
- Updated
- 2025/07/31
- Product number
- CHM0023944
- Product name
- 3-NITROBENZENESULFONAMIDE
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $619.7
- Updated
- 2021/12/16
3-NITROBENZENESULFONAMIDE Chemical Properties,Usage,Production
Chemical Properties
light brown powder
Uses
3-Nitrobenzenesulfonamide may be used in chemical synthesis.
Synthesis
121-51-7
121-52-8
General procedure for the synthesis of m-nitrobenzenesulfonamide from 3-nitrobenzenesulfonyl chloride: reference to Example 53 (not the method of the present invention): synthesis of 3-[6-(2-benzyloxy-phenyl)-pyrimidin-4-ylamino]-1-benzenesulfonylimine; synthesis of 3-nitrobenzenesulfonamide. 3-Nitrobenzenesulfonyl chloride (2.0 g, 9.0 mmol) was dissolved in acetonitrile (20 mL). Concentrated ammonia (20 mL) saturated with ammonium carbonate was added to this solution and the reaction mixture was stirred vigorously for 1 hour at room temperature. Subsequently, the acetonitrile was evaporated under reduced pressure and the residue was diluted with cold water (30 mL) to induce precipitate formation. The precipitate was collected by filtration and washed sequentially with water (2 x 15 mL) and ether and finally dried. 3-Nitrobenzenesulfonamide 1.46 g (80% yield) was obtained as a beige powder. Mass spectrum (Cl MS) m/z 203 (MH+).
References
[1] Patent: WO2008/129080, 2008, A1. Location in patent: Page/Page column 156; 174
[2] Bioorganic and Medicinal Chemistry Letters, 2007, vol. 17, # 1, p. 28 - 33
[3] Collection of Czechoslovak Chemical Communications, 1984, vol. 49, # 5, p. 1182 - 1192
[4] Magnetic Resonance in Chemistry, 1987, vol. 25, p. 189 - 193
[5] Russian Journal of Organic Chemistry, 2001, vol. 37, # 1, p. 87 - 92
3-NITROBENZENESULFONAMIDE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 3-NITROBENZENESULFONAMIDE manufacturers
- Product
- 3-NITROBENZENESULFONAMIDE 121-52-8
- Price
- US $1.10/g
- Min. Order
- 1g
- Purity
- 99.9%
- Supply Ability
- 100 Tons Min
- Release date
- 2021-07-12
- Product
- 3-NITROBENZENESULFONAMIDE 121-52-8
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 200kg
- Release date
- 2020-01-02