5'-BROMO-2'-HYDROXYPROPIOPHENONE 97

ChemicalBook > CAS DataBase List > 5'-BROMO-2'-HYDROXYPROPIOPHENONE 97

5'-BROMO-2'-HYDROXYPROPIOPHENONE 97

Product Name: 5'-BROMO-2'-HYDROXYPROPIOPHENONE 97
CAS No.: 17764-93-1
Chemical Name: 5'-BROMO-2'-HYDROXYPROPIOPHENONE 97
Synonyms: 5‘-Bromo-2’-hydroxypropiophene;5'-Bromo-2'-hydroxypropiophenone;5'-Bromo-2'-hydroxypropiophenone >5'-BROMO-2'-HYDROXYPROPIOPHENONE 97;1-(5-bromo-2-hydroxyphenyl)-1-propanone;1-Propanone, 1-(5-bromo-2-hydroxyphenyl)-;JRH-01104, 1-(5-Bromo-2-hydroxyphenyl)propan-1-one, 97%
CBNumber: CB5500363
Molecular Formula: C9H9BrO2
Formula Weight: 229.07
MOL File: 17764-93-1.mol

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5'-BROMO-2'-HYDROXYPROPIOPHENONE 97 Property

Melting point:: 78-79°C
Boiling point:: 156°C/21mmHg(lit.)
Density: 1.506±0.06 g/cm3(Predicted)
pka: 7.68±0.48(Predicted)
form: powder to crystal
color: White to Light yellow to Light orange

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Safety

Hazard Codes: Xn
Risk Statements: 22
RIDADR: UN 2811 6.1/PG 3
WGK Germany: 3
HS Code: 2914500090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H301Toxic if swalloed

H319Causes serious eye irritation

Precautionary statements

P301+P310IF SWALLOWED: Immediately call a POISON CENTER or doctor/physician.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 663700
Product name: 5′-Bromo-2′-hydroxypropiophenone
Purity: 97%
Packaging: 1g
Price: $49.9
Updated: 2022/05/15

Sigma-Aldrich

Product number: 663700
Product name: 5′-Bromo-2′-hydroxypropiophenone
Purity: 97%
Packaging: 10g
Price: $303
Updated: 2022/05/15

TCI Chemical

Product number: B4769
Product name: 5'-Bromo-2'-hydroxypropiophenone
Purity: >98.0%(GC)(T)
Packaging: 1g
Price: $24
Updated: 2024/03/01

TCI Chemical

Product number: B4769
Product name: 5'-Bromo-2'-hydroxypropiophenone
Purity: >98.0%(GC)(T)
Packaging: 5g
Price: $71
Updated: 2024/03/01

TRC

Product number: B997348
Product name: 5''-Bromo-2''-hydroxypropiophenone
Packaging: 2.5g
Price: $110
Updated: 2021/12/16

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5'-BROMO-2'-HYDROXYPROPIOPHENONE 97 Chemical Properties,Usage,Production

Preparation

Preparation by Fries rearrangement of 4-bromophenyl propionate with aluminium chloride at 165° for 1 h (97%), at 150–160° for 30 min or at 120° for 30–40 min (80%)
Preparation by bromination of o-hydroxypropiophenone with bromine in 80% aqueous acetic acid at r.t. (66%)
Also obtained by acylation of p-bromophenol with propionic acid in the presence of boron trifluoride in a sealed tube at 120° for 1 h (59%).

5'-BROMO-2'-HYDROXYPROPIOPHENONE 97 Preparation Products And Raw materials

Raw materials

Preparation Products

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