ChemicalBook > CAS DataBase List > 2-ACETYL-4-CYANOPHENOL

2-ACETYL-4-CYANOPHENOL

Product Name
2-ACETYL-4-CYANOPHENOL
CAS No.
35794-84-4
Chemical Name
2-ACETYL-4-CYANOPHENOL
Synonyms
RARECHEM BW GA 0369;2-ACETYL-4-CYANOPHENOL;4'-Cyano-2'-hydroxyacetophenone;Benzonitrile, 3-acetyl-4-hydroxy-;Benzonitrile, 3-acetyl-4-hydroxy- (6CI,7CI,9CI);4'-Cyano-2'-hydroxyacetophenone[2-acetyl-4-cyanophenol]
CBNumber
CB5691407
Molecular Formula
C9H7NO2
Formula Weight
161.16
MOL File
35794-84-4.mol
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2-ACETYL-4-CYANOPHENOL Property

Melting point:
103 °C
Boiling point:
313.5±32.0 °C(Predicted)
Density 
1.26±0.1 g/cm3(Predicted)
storage temp. 
Inert atmosphere,Room Temperature
solubility 
DMSO (Slightly), Methanol (Slightly)
form 
Solid
pka
8.04±0.18(Predicted)
color 
Off-White to Pale Yellow
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Safety

HS Code 
2926907090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
A172093
Product name
2-Acetyl-4-cyanophenol
Packaging
250mg
Price
$50
Updated
2021/12/16
Biosynth Carbosynth
Product number
FA139653
Product name
3-Acetyl-4-hydroxybenzonitrile
Packaging
500mg
Price
$70
Updated
2021/12/16
AK Scientific
Product number
W5730
Product name
2-Acetyl-4-cyanophenol
Packaging
1g
Price
$110
Updated
2021/12/16
Biosynth Carbosynth
Product number
FA139653
Product name
3-Acetyl-4-hydroxybenzonitrile
Packaging
1g
Price
$125
Updated
2021/12/16
Biosynth Carbosynth
Product number
FA139653
Product name
3-Acetyl-4-hydroxybenzonitrile
Packaging
2g
Price
$218
Updated
2021/12/16
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2-ACETYL-4-CYANOPHENOL Chemical Properties,Usage,Production

Preparation

Obtained by heating a mixture of 4-cyanophenyl acetate and aluminium chloride at 180–185° for 2 h (58%).

Synthesis

13031-41-9

35794-84-4

The general procedure for the synthesis of 2-acetyl-p-cyanophenol from 4-cyanophenyl acetate by Fries rearrangement reaction was as follows: phenyl acetate was heated and reacted with aluminum chloride for 3 h at 180-185 °C for Fries rearrangement. After completion of the reaction, the target product 2-acetyl-p-cyanophenol was isolated in 45% yield.

References

[1] ChemMedChem, 2013, vol. 8, # 6, p. 914 - 918
[2] Patent: US2007/117823, 2007, A1. Location in patent: Page/Page column 7
[3] Patent: WO2007/54580, 2007, A1. Location in patent: Page/Page column 15
[4] Letters in Drug Design and Discovery, 2010, vol. 7, # 6, p. 415 - 420
[5] Medicinal Chemistry Research, 2015, vol. 24, # 7, p. 3008 - 3020

2-ACETYL-4-CYANOPHENOL Preparation Products And Raw materials

Raw materials

Preparation Products

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2-ACETYL-4-CYANOPHENOL Suppliers

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View Lastest Price from 2-ACETYL-4-CYANOPHENOL manufacturers

Career Henan Chemical Co
Product
3-acetyl-4-hydroxybenzonitrile 35794-84-4
Price
US $1.00/KG
Min. Order
1KG
Purity
98% HPLC
Supply Ability
10 tons
Release date
2020-02-14

35794-84-4, 2-ACETYL-4-CYANOPHENOLRelated Search:

4-Cyanophenol AURORA KA-6181 5-ACETYL-2-AMINO-4-HYDROXYBENZONITRILE AURORA KA-6265 2-ACETYL-4-CYANOPHENOL AURORA KA-6182

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