Dibutylurea
- Product Name
- Dibutylurea
- CAS No.
- 1792-17-2
- Chemical Name
- Dibutylurea
- Synonyms
- DIBUTYLUREA;Dibutylurea,98%;1,3-DIBUTYLUREA;N,N'-DIBUTYLUREA;urea,1,3-dibutyl-;N,N'-Di-n-butylurea;TIMTEC-BB SBB007953;N,N'-DI-N-BUTYLUREA;Urea, N,N'-dibutyl-;n,n’-dibutylurea(asimpurity)
- CBNumber
- CB5710788
- Molecular Formula
- C9H20N2O
- Formula Weight
- 172.27
- MOL File
- 1792-17-2.mol
Dibutylurea Property
- Melting point:
- 65-75 °C
- Boiling point:
- 115°C 0,03mm
- Density
- 0.9845 (rough estimate)
- refractive index
- 1.5800 (estimate)
- Flash point:
- 115°C/0.03mm
- storage temp.
- Sealed in dry,Room Temperature
- solubility
- Chloroform (Slightly), Methanol (Slightly)
- form
- Solid
- pka
- 14.44±0.46(Predicted)
- color
- White to Off-White
- BRN
- 1704165
- CAS DataBase Reference
- 1792-17-2(CAS DataBase Reference)
- NIST Chemistry Reference
- 1,3-Dibutylurea(1792-17-2)
- EPA Substance Registry System
- N,N'-Dibutylurea (1792-17-2)
Safety
- Safety Statements
- 24/25
N-Bromosuccinimide Price
- Product number
- S546577
- Product name
- 1,3-DIBUTYLUREA
- Purity
- Aldrich
- Packaging
- 1g
- Price
- $179
- Updated
- 2024/03/01
- Product number
- L06165
- Product name
- N,N'-Di-n-butylurea, 98%
- Packaging
- 5g
- Price
- $57.65
- Updated
- 2024/03/01
- Product number
- L06165
- Product name
- N,N'-Di-n-butylurea, 98%
- Packaging
- 25g
- Price
- $184.65
- Updated
- 2024/03/01
- Product number
- D429575
- Product name
- N,N''-Dibutylurea
- Packaging
- 25g
- Price
- $875
- Updated
- 2021/12/16
- Product number
- CHM0313606
- Product name
- N,N'-DIBUTYLUREA
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $495.52
- Updated
- 2021/12/16
Dibutylurea Chemical Properties,Usage,Production
Chemical Properties
white to pink or light beige crystalline powder
Uses
N,N'-Dibutylurea is a degradation product of Benomyl, the active ingredient in Benlate fungicides.
Uses
N,N''-Dibutylurea is a degradation product of Benomyl, the active ingredient in Benlate fungicides.
Preparation
The reactions under CO2 pressured conditions were carried out in a stainless steel reactor (SUS 304, 30 mL, TVS-5 type). Thus, butylamine (2.9 g, 40 mmol), Ph3SbO (370 mg, 1.0 mmol), P4S10 (890 mg, 2.0 mmol), and benzene (20 mL) were charged into the reactor, and then CO2 was introduced at a pressure of 4.9 MPa (50 kg cm-2, ca. 65 mmol) at room temperature. The reactor was heated at 80 ℃ in a temperature-regulated incubator for 12 h. When a reaction temperature higher than 100 ℃ was necessary, an oil bath was used. After the heating, the reactor was cooled and carefully decompressed. The contents were treated with hot benzene (3×20 mL) and filtered to remove an insoluble residue containing the catalyst and phosphoric acid derivatives. The collected benzene solution was then concentrated to dryness in vacuo with cooling. Pure 1,3-dibutylurea was isolated by recrystallization from ligroin (yield 2.99 g, 88%).
Synthesis Reference(s)
Synthetic Communications, 21, p. 1923, 1991 DOI: 10.1080/00397919108021783
Dibutylurea Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from Dibutylurea manufacturers
- Product
- Dibutylurea 1792-17-2
- Price
- US $8.80/KG
- Min. Order
- 1KG
- Purity
- 97%-99%
- Supply Ability
- 100kg
- Release date
- 2019-07-04