Uses
ChemicalBook > CAS DataBase List > 1,3-DIBROMO-5-IODOBENZENE

1,3-DIBROMO-5-IODOBENZENE

Uses
Product Name
1,3-DIBROMO-5-IODOBENZENE
CAS No.
19752-57-9
Chemical Name
1,3-DIBROMO-5-IODOBENZENE
Synonyms
SKL670;3,5-DIBROMOIODOBENZENE;3-DIBROMO-5-IODOBENZENE;3,5-Dibromophenyl iodide;1-Iodo-3,5-dibromobenzene;1,3-DIBROMO-5-IODOBENZENE;Benzene,1,3-dibromo-5-iodo-;1,3-Dibromo-5-iodobenzene>1,3-DIBROMO-5-IODOBENZENE 25G;1,3-Dibromo-5-iodobenzene 98%
CBNumber
CB5752502
Molecular Formula
C6H3Br2I
Formula Weight
361.8
MOL File
19752-57-9.mol
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1,3-DIBROMO-5-IODOBENZENE Property

Melting point:
124.4-124.7℃
Boiling point:
302.7±32.0 °C(Predicted)
Density 
2.514±0.06 g/cm3 (20 ºC 760 Torr)
storage temp. 
Keep in dark place,Sealed in dry,Room Temperature
form 
powder to crystal
color 
Light yellow to Brown
InChI
InChI=1S/C6H3Br2I/c7-4-1-5(8)3-6(9)2-4/h1-3H
InChIKey
KARUMYWDGQTPFL-UHFFFAOYSA-N
SMILES
C1(Br)=CC(I)=CC(Br)=C1
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Safety

HS Code 
2903998090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

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N-Bromosuccinimide Price

TCI Chemical
Product number
D4691
Product name
1,3-Dibromo-5-iodobenzene
Packaging
1G
Price
$42
Updated
2025/07/31
TCI Chemical
Product number
D4691
Product name
1,3-Dibromo-5-iodobenzene
Packaging
5G
Price
$156
Updated
2025/07/31
TRC
Product number
B426233
Product name
1,3-Dibromo-5-iodobenzene
Packaging
10mg
Price
$45
Updated
2021/12/16
TRC
Product number
B426233
Product name
1,3-Dibromo-5-iodobenzene
Packaging
50mg
Price
$60
Updated
2021/12/16
Matrix Scientific
Product number
092113
Product name
1,3-Dibromo-5-iodobenzene
Purity
95+%
Packaging
1g
Price
$30
Updated
2021/12/16
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1,3-DIBROMO-5-IODOBENZENE Chemical Properties,Usage,Production

Uses

1,3-Dibromo-5-iodobenzene is an important organic intermediate widely used in the fields of dyes, pigments, pharmaceuticals and pesticides.

Chemical Properties

Reddish brown powder

Synthesis

10527-69-2

19752-57-9

The general procedure for the synthesis of 1,3-dibromo-5-iodobenzene from 2,6-dibromo-4-iodoaniline is as follows: 1. Preparation of 3,5-dibromoiodobenzene: 188.4 g of 2,6-dibromo-4-iodoaniline and 600 g of hypophosphorous acid were added to the reaction vessel at room temperature and stirred well. Subsequently, a solution formed by dissolving 34.5 g of sodium nitrite in 60 ml of water was added dropwise. The reaction is violently exothermic and the reaction temperature needs to be controlled at 20-25°C by means of a water bath. After the dropwise addition was completed, the reaction was continued for about 3 hours until a large white solid precipitate was observed. The reaction was continued at this temperature for 1 hour. The progress of the reaction was monitored by HPLC and stopped when the raw material 2,6-dibromo-4-iodoaniline completely disappeared. The crude product was collected by filtration. 2. Purification of the crude product: the crude product was dispersed in three 1000 ml flasks, 700 ml of anhydrous ethanol was added to each flask, and the product was heated to reflux (ca. 80 °C) to completely dissolve the product. Subsequently, it was cooled to 20-25 °C, the crystals were collected by filtration and dried under reduced pressure at 60 °C to obtain white needle-like crystals of 136 g. The purity of the product, 3,5-dibromo-2-iodobenzene, was 99.72% by HPLC analysis and the reaction yield was 75.2%.

References

[1] Atti della Accademia Nazionale dei Lincei, Classe di Scienze Fisiche, Matematiche e Naturali, Rendiconti, 1913, vol. <5> 22 I, p. 823
[2] Atti della Accademia Nazionale dei Lincei, Classe di Scienze Fisiche, Matematiche e Naturali, Rendiconti, 1914, vol. <5> 23 I, p. 283 Anm.
[3] Journal of the American Chemical Society, 2002, vol. 124, # 29, p. 8661 - 8666
[4] Journal of Organic Chemistry, 2015, vol. 80, # 2, p. 882 - 896
[5] Patent: CN105523884, 2016, A. Location in patent: Paragraph 0014; 0016; 0017

1,3-DIBROMO-5-IODOBENZENE Preparation Products And Raw materials

Raw materials

Preparation Products

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1,3-DIBROMO-5-IODOBENZENE Suppliers

PureChemland Co.,Ltd.
Tel
13540909846 13882008651
Email
3848291069@qq.com
Country
China
ProdList
3001
Advantage
58
TCI (Shanghai) Development Co., Ltd.
Tel
021-67121386
Fax
021-67121385
Email
Sales-CN@TCIchemicals.com
Country
China
ProdList
24529
Advantage
81
Energy Chemical
Tel
021-021-58432009 400-005-6266
Fax
021-58436166
Email
sales8178@energy-chemical.com
Country
China
ProdList
44801
Advantage
61
Shijiazhuang Sdyano Fine Chemical Co., Ltd.
Tel
0311-89250318 031166536426
Fax
4000311741
Email
master@sjzsdyn.com
Country
China
ProdList
2809
Advantage
65
Accela ChemBio Co.,Ltd.
Tel
021-50795510 4000665055
Fax
021-50795055
Email
sales@accelachem.com
Country
China
ProdList
11035
Advantage
64
Nanjing Chemlin Chemical Co., Ltd
Tel
025-83697070
Fax
+86-25-83453306
Email
info@chemlin.com.cn
Country
China
ProdList
15883
Advantage
64
Shanghai Hanhong Scientific Co.,Ltd.
Tel
021-54306202 13764082696
Email
info@hanhongsci.com
Country
China
ProdList
42934
Advantage
64
Beijing Eternalchem Co,. Ltd.
Tel
010-59484199 18611897322
Email
sales@eternalchem.com
Country
China
ProdList
4383
Advantage
60
Springchem New Material Technology Co.,Limited
Tel
+86-021-62885108 +8613917661608
Email
info@spring-chem.com
Country
China
ProdList
2068
Advantage
57
Wuhan ariel chemical Co., LTD.
Tel
18986259541
Fax
027-87840182
Email
sales@3stc.com
Country
China
ProdList
3764
Advantage
58
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View Lastest Price from 1,3-DIBROMO-5-IODOBENZENE manufacturers

Shenzhen Nexcon Pharmatechs Ltd.
Product
1,3-DIBROMO-5-IODOBENZENE 19752-57-9
Price
US $0.00-0.00/KG
Min. Order
1KG
Purity
98%
Supply Ability
2000
Release date
2025-04-17
Hebei Chuanghai Biotechnology Co., Ltd
Product
1,3-DIBROMO-5-IODOBENZENE 19752-57-9
Price
US $30.00-10.00/KG
Min. Order
50KG
Purity
99%
Supply Ability
500000kg
Release date
2024-10-24
Hebei Yanxi Chemical Co., Ltd.
Product
1,3-DIBROMO-5-IODOBENZENE 19752-57-9
Price
US $0.00/kg
Min. Order
1kg
Purity
0.99
Supply Ability
20 tons
Release date
2023-11-22

19752-57-9, 1,3-DIBROMO-5-IODOBENZENERelated Search:


  • Benzene,1,3-dibromo-5-iodo-
  • 1,3-DIBROMO-5-IODOBENZENE 25G
  • 1,3-DIBROMO-5-IODOBENZENE
  • 3,5-DIBROMOIODOBENZENE
  • 1-Iodo-3,5-dibromobenzene
  • 3,5-Dibromophenyl iodide
  • 1,3-Dibromo-5-iodobenzene&gt
  • 1,3-DIBROMO-5-IODOBENZENE ISO 9001:2015 REACH
  • 3-DIBROMO-5-IODOBENZENE
  • SKL670
  • 1,3-Dibromo-5-iodobenzene 98%
  • 19752-57-9
  • C6H3Br2I
  • organic chemicals and derivatives/others
  • OLED