6-IODO-PYRIDIN-2-YLAMINE

Product Name: 6-IODO-PYRIDIN-2-YLAMINE
CAS No.: 88511-25-5
Chemical Name: 6-IODO-PYRIDIN-2-YLAMINE
Synonyms: 6-iodopyridin-2-aMine;6-iodo-2-pyridinamine;2-AMino-6-iodopyridine;2-PyridinaMine, 6-iodo-;6-Iodo-pyridine-2ylamine;6-IODO-PYRIDIN-2-YLAMINE
CBNumber: CB5765197
Molecular Formula: C5H5IN2
Formula Weight: 220.01
MOL File: 88511-25-5.mol

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6-IODO-PYRIDIN-2-YLAMINE Property

Melting point:: 103-104°C
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
form: solid
Appearance: White to light yellow Solid

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Safety

Hazard Codes: Xi
HazardClass: IRRITANT
HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: ADE000340
Product name: 6-Iodo-pyridin-2-ylamine
Purity: AldrichCPR
Packaging: 1g
Price: $497
Updated: 2025/07/31

TRC

Product number: B450615
Product name: 6-iodopyridin-2-amine
Packaging: 100mg
Price: $155
Updated: 2021/12/16

SynQuest Laboratories

Product number: 3H30-H-0G
Product name: 6-Iodopyridin-2-amine
Purity: 95%
Packaging: 1g
Price: $200
Updated: 2021/12/16

Matrix Scientific

Product number: 023722
Product name: 6-Iodo-pyridin-2-ylamine
Purity: 98%
Packaging: 250mg
Price: $125
Updated: 2021/12/16

Apolloscientific

Product number: OR913273
Product name: 6-Iodopyridin-2-amine
Purity: 95%
Packaging: 1g
Price: $125
Updated: 2021/12/16

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6-IODO-PYRIDIN-2-YLAMINE Chemical Properties,Usage,Production

Synthesis

19798-81-3

88511-25-5

General procedure for the synthesis of 6-iodopyridin-2-amine from 2-amino-6-bromopyridine: 2-bromo-6-aminopyridine (519 mg), cuprous iodide (29 mg), sodium iodide (899 mg), and N,N-dimethylethylenediamine (26 mg) were dissolved in dioxane (5 mL) and heated to react for 6 hours at 110 °C in an inert atmosphere. Upon completion of the reaction, concentrated ammonia (8 mL) was added, followed by water (10 mL). The reaction mixture was extracted with dichloromethane (3 x 15 mL) and the organic phase was dried with anhydrous magnesium sulfate, filtered and concentrated. The crude product was purified by rapid chromatography on silica gel using a 0-10% methanol/dichloromethane gradient elution to afford 6-iodopyridin-2-amine as a beige solid (530 mg, 80% yield). The structure of the product was confirmed by 1H NMR (CDCl3): δ 4.60 (s, 2H), 6.41-6.44 (m, 1H), 7.00-7.08 (m, 2H); mass spectrometry (MS) showed the molecular ion peak m/z 221 (MH+).

References

[1] RSC Advances, 2013, vol. 3, # 26, p. 10296 - 10300
[2] Patent: WO2005/60970, 2005, A1. Location in patent: Page/Page column 117

6-IODO-PYRIDIN-2-YLAMINE Preparation Products And Raw materials

Raw materials

Preparation Products

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6-IODO-PYRIDIN-2-YLAMINE Suppliers

China 55 India 2 United Kingdom 1 United States 7 Global 65

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88511-25-5, 6-IODO-PYRIDIN-2-YLAMINERelated Search:

3-BENZYLOXY-6-IODO-2-(PIPERIDIN-1-YL)-PYRIDINE 6-IODO-3,4-DIHYDRO-2H-PYRIDO[3,2-B][1,4]OXAZINE 3-HYDROXY-6-IODO-2-(4-TERT-BUTOXYCARBONYLPIPERAZIN-1-YL)-PYRIDINE 2-Iodo-3-methoxy-6-nitropyridine 3-HYDROXY-6-IODO-2-BENZYLAMINOPYRIDINE 3-BENZYLOXY-6-IODO-2-(PYRROLIDIN-1-YL)-PYRIDINE (3-BENZYLOXY-6-IODO-PYRIDIN-2-YL)-ISOPROPYL-AMINE N-(6-IODO-PYRIDIN-2-YL)-2,2-DIMETHYL-PROPIONAMIDE 3-BENZYLOXY-2-ETHYLAMINO-6-IODOPYRIDINE 3-BENZYLOXY-6-IODO-2-METHYLAMINOPYRIDINE 3-HYDROXY-6-IODO-2-METHYLAMINOPYRIDINE (6-IODO-PYRIDIN-2-YL)-CARBAMIC ACID TERT-BUTYL ESTER BENZAMIDE, 4-CHLORO-N-(6-IODO-2-PYRIDINYL)- 3-(1-ETHYLPROPOXY)-6-IODO-N-METHYLPYRIDIN-2-AMINE 6-IODO-PYRIDIN-2-YLAMINE

6-iodopyridin-2-aMine

6-IODO-PYRIDIN-2-YLAMINE

6-Iodo-pyridine-2ylamine

2-PyridinaMine, 6-iodo-

2-AMino-6-iodopyridine

6-iodo-2-pyridinamine

88511-25-5