ChemicalBook > CAS DataBase List > 6-IODO-PYRIDIN-2-YLAMINE

6-IODO-PYRIDIN-2-YLAMINE

Product Name
6-IODO-PYRIDIN-2-YLAMINE
CAS No.
88511-25-5
Chemical Name
6-IODO-PYRIDIN-2-YLAMINE
Synonyms
6-iodopyridin-2-aMine;6-iodo-2-pyridinamine;2-AMino-6-iodopyridine;2-PyridinaMine, 6-iodo-;6-Iodo-pyridine-2ylamine;6-IODO-PYRIDIN-2-YLAMINE
CBNumber
CB5765197
Molecular Formula
C5H5IN2
Formula Weight
220.01
MOL File
88511-25-5.mol
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6-IODO-PYRIDIN-2-YLAMINE Property

Melting point:
103-104°C
storage temp. 
under inert gas (nitrogen or Argon) at 2–8 °C
form 
solid
Appearance
White to light yellow Solid
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Safety

Hazard Codes 
Xi
HazardClass 
IRRITANT
HS Code 
2933399990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
ADE000340
Product name
6-Iodo-pyridin-2-ylamine
Purity
AldrichCPR
Packaging
1g
Price
$497
Updated
2025/07/31
TRC
Product number
B450615
Product name
6-iodopyridin-2-amine
Packaging
100mg
Price
$155
Updated
2021/12/16
Apolloscientific
Product number
OR913273
Product name
6-Iodopyridin-2-amine
Purity
95%
Packaging
250mg
Price
$55
Updated
2021/12/16
SynQuest Laboratories
Product number
3H30-H-0G
Product name
6-Iodopyridin-2-amine
Purity
95%
Packaging
250mg
Price
$88
Updated
2021/12/16
Matrix Scientific
Product number
023722
Product name
6-Iodo-pyridin-2-ylamine
Purity
98%
Packaging
250mg
Price
$125
Updated
2021/12/16
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6-IODO-PYRIDIN-2-YLAMINE Chemical Properties,Usage,Production

Synthesis

19798-81-3

88511-25-5

General procedure for the synthesis of 6-iodopyridin-2-amine from 2-amino-6-bromopyridine: 2-bromo-6-aminopyridine (519 mg), cuprous iodide (29 mg), sodium iodide (899 mg), and N,N-dimethylethylenediamine (26 mg) were dissolved in dioxane (5 mL) and heated to react for 6 hours at 110 °C in an inert atmosphere. Upon completion of the reaction, concentrated ammonia (8 mL) was added, followed by water (10 mL). The reaction mixture was extracted with dichloromethane (3 x 15 mL) and the organic phase was dried with anhydrous magnesium sulfate, filtered and concentrated. The crude product was purified by rapid chromatography on silica gel using a 0-10% methanol/dichloromethane gradient elution to afford 6-iodopyridin-2-amine as a beige solid (530 mg, 80% yield). The structure of the product was confirmed by 1H NMR (CDCl3): δ 4.60 (s, 2H), 6.41-6.44 (m, 1H), 7.00-7.08 (m, 2H); mass spectrometry (MS) showed the molecular ion peak m/z 221 (MH+).

References

[1] RSC Advances, 2013, vol. 3, # 26, p. 10296 - 10300
[2] Patent: WO2005/60970, 2005, A1. Location in patent: Page/Page column 117

6-IODO-PYRIDIN-2-YLAMINE Preparation Products And Raw materials

Raw materials

Preparation Products

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6-IODO-PYRIDIN-2-YLAMINE Suppliers

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88511-25-5, 6-IODO-PYRIDIN-2-YLAMINERelated Search:

3-BENZYLOXY-6-IODO-2-(PIPERIDIN-1-YL)-PYRIDINE 6-IODO-3,4-DIHYDRO-2H-PYRIDO[3,2-B][1,4]OXAZINE 3-HYDROXY-6-IODO-2-(4-TERT-BUTOXYCARBONYLPIPERAZIN-1-YL)-PYRIDINE 2-Iodo-3-methoxy-6-nitropyridine 3-HYDROXY-6-IODO-2-BENZYLAMINOPYRIDINE 3-BENZYLOXY-6-IODO-2-(PYRROLIDIN-1-YL)-PYRIDINE (3-BENZYLOXY-6-IODO-PYRIDIN-2-YL)-ISOPROPYL-AMINE N-(6-IODO-PYRIDIN-2-YL)-2,2-DIMETHYL-PROPIONAMIDE 3-BENZYLOXY-2-ETHYLAMINO-6-IODOPYRIDINE 3-BENZYLOXY-6-IODO-2-METHYLAMINOPYRIDINE 3-HYDROXY-6-IODO-2-METHYLAMINOPYRIDINE (6-IODO-PYRIDIN-2-YL)-CARBAMIC ACID TERT-BUTYL ESTER BENZAMIDE, 4-CHLORO-N-(6-IODO-2-PYRIDINYL)- 3-(1-ETHYLPROPOXY)-6-IODO-N-METHYLPYRIDIN-2-AMINE 6-IODO-PYRIDIN-2-YLAMINE

  • 6-iodopyridin-2-aMine
  • 6-IODO-PYRIDIN-2-YLAMINE
  • 6-Iodo-pyridine-2ylamine
  • 2-PyridinaMine, 6-iodo-
  • 2-AMino-6-iodopyridine
  • 6-iodo-2-pyridinamine
  • 88511-25-5