4-(3-HYDROXY-PROPYL)-BENZONITRILE
- Product Name
- 4-(3-HYDROXY-PROPYL)-BENZONITRILE
- CAS No.
- 83101-12-6
- Chemical Name
- 4-(3-HYDROXY-PROPYL)-BENZONITRILE
- Synonyms
- 4-(3-HYDROXY-PROPYL)-BENZONITRILE;Benzonitrile, 4-(3-hydroxypropyl)-
- CBNumber
- CB5840948
- Molecular Formula
- C10H11NO
- Formula Weight
- 161.2
- MOL File
- 83101-12-6.mol
4-(3-HYDROXY-PROPYL)-BENZONITRILE Property
- storage temp.
- 2-8°C
- Appearance
- Colorless to light yellow Liquid
Safety
- HS Code
- 2926907090
N-Bromosuccinimide Price
- Product number
- A425510
- Product name
- 4-(3-Hydroxypropyl)benzonitrile
- Packaging
- 50mg
- Price
- $110
- Updated
- 2021/12/16
- Product number
- A425510
- Product name
- 4-(3-Hydroxypropyl)benzonitrile
- Packaging
- 100mg
- Price
- $175
- Updated
- 2021/12/16
- Product number
- Z5162
- Product name
- 4-(3-Hydroxypropyl)benzonitrile
- Packaging
- 1g
- Price
- $386
- Updated
- 2021/12/16
- Product number
- CHM0138377
- Product name
- 4-(3-HYDROXYPROPYL)BENZONITRILE
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $918.06
- Updated
- 2021/12/16
- Product number
- 83101126
- Product name
- 4-(3-Hydroxypropyl)benzonitrile
- Packaging
- 500mg
- Price
- $980
- Updated
- 2021/12/16
4-(3-HYDROXY-PROPYL)-BENZONITRILE Chemical Properties,Usage,Production
Synthesis
42287-94-5
83101-12-6
4) Synthesis of 3-(4-cyanophenyl)propanol Borane-tetrahydrofuran complex (1.0 M, 33.0 mL, 33.0 mmol, dissolved in tetrahydrofuran) was slowly added dropwise to a stirred tetrahydrofuran solution (50 mL) of 3-(4-cyanophenyl)propanoic acid (4.40 g, 25.1 mmol). The reaction mixture was stirred continuously for 14 hours at room temperature. Upon completion of the reaction, water (50 mL) and potassium carbonate (10.0 g, 72.4 mmol) were added to the mixture. Subsequently, the mixture was extracted with ethyl acetate, and the combined organic phases were washed with saturated brine, dried over anhydrous magnesium sulfate, and concentrated under reduced pressure to afford 3-(4-cyanophenyl)propanol as a yellow oil (3.20 g, 79% yield). 1H-NMR (200 MHz, CDCl3) δ: 7.58 (2H, d, J = 8.2 Hz), 7.31 (2H, d, J = 8.2 Hz), 3.68 (2H, t, J = 6.2 Hz), 2.79 (2H, t, J = 7.8 Hz), 2.00-1.75 (2H, m). IR (pure): 3319, 2943, 2229, 1608, 1505, 1415, 1054, 854, 817 cm-1.
References
[1] Patent: US6235731, 2001, B1
4-(3-HYDROXY-PROPYL)-BENZONITRILE Preparation Products And Raw materials
Raw materials
Preparation Products
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