5-methoxy-1h-isoindole-1,3(2h)-dione
Uses- Product Name
- 5-methoxy-1h-isoindole-1,3(2h)-dione
- CAS No.
- 50727-04-3
- Chemical Name
- 5-methoxy-1h-isoindole-1,3(2h)-dione
- Synonyms
- 4-MethoxyphthaliMide;5-methoxyisoindole-1,3-dione;5-methoxyisoindoline-1,3-dione;5-methoxy-1h-isoindole-1,3(2h)-dione;1H-Isoindole-1,3(2H)-dione, 5-methoxy-
- CBNumber
- CB5853700
- Molecular Formula
- C9H7NO3
- Formula Weight
- 177.16
- MOL File
- 50727-04-3.mol
5-methoxy-1h-isoindole-1,3(2h)-dione Property
- Melting point:
- 219 °C
- Density
- 1.346±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- pka
- 9.84±0.20(Predicted)
- Appearance
- White to off-white Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- M263005
- Product name
- 5-Methoxyisoindoline-1,3-dione
- Packaging
- 250mg
- Price
- $250
- Updated
- 2021/12/16
- Product number
- CHM1047205
- Product name
- 5-METHOXY-1H-ISOINDOLE-1,3(2H)-DIONE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $498.09
- Updated
- 2021/12/16
- Product number
- 2356AQ
- Product name
- 5-Methoxyisoindoline-1,3-dione
- Packaging
- 1g
- Price
- $632
- Updated
- 2021/12/16
- Product number
- CM125503
- Product name
- 5-methoxyisoindoline-1,3-dione
- Purity
- 95%+
- Packaging
- 5g
- Price
- $964
- Updated
- 2021/12/16
- Product number
- CD11114127
- Product name
- 5-Methoxyisoindoline-1,3-dione
- Purity
- 97%
- Packaging
- 5g
- Price
- $1021
- Updated
- 2021/12/16
5-methoxy-1h-isoindole-1,3(2h)-dione Chemical Properties,Usage,Production
Uses
5-Methoxyisoindoline-1,3-dione is used as a reagent in the synthesis of KUP-1, a photoreactive and fluorescent pyrethroid, which can be used as a tool for photoaffinity labelling.
Uses
5-Methoxyisoindoline-1,3-dione is used as a reagent in the synthesis of KUP-1, a photoreactive and fluorescent pyrethroid, which can be used as a tool for photoaffinity labelling.
Synthesis
5111-70-6
50727-04-3
General procedure for the synthesis of 5-methoxyisoindolane-1,3-dione from 5-methoxy-1-indanone: In a stainless steel autoclave with PTFE lining, 0.01 g of MnO2 catalyst, 0.5 mmol of 5-methoxy-1-indanone, 0.2 g of ammonia (25 wt%) and 2 g of chlorobenzene were added in sequence. The reaction temperature was raised to 110 °C by an automatic temperature controller, followed by the passage of 0.6 MPa oxygen, which was maintained at a constant pressure, and the reaction was continued for 4 hours. Upon completion of the reaction, the reaction mixture was analyzed by GC-MS and the yield of 5-methoxyisoindolidine-1,3-dione was measured to be 85%.
References
[1] Patent: CN106278990, 2017, A. Location in patent: Paragraph 0013; 0017; 0018; 0020; 0023; 0028
5-methoxy-1h-isoindole-1,3(2h)-dione Preparation Products And Raw materials
Raw materials
Preparation Products
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