2,2-dimethyl-2H-pyrido[3,2-b]-1,4-oxazin-3(4H)-one

Product Name: 2,2-dimethyl-2H-pyrido[3,2-b]-1,4-oxazin-3(4H)-one
CAS No.: 20348-21-4
Chemical Name: 2,2-dimethyl-2H-pyrido[3,2-b]-1,4-oxazin-3(4H)-one
Synonyms: Einecs 243-753-2;2,2-Dimethyl-2H-pyrido[3,2-b][1,4]oxazin-3(4H);2,2-dimethyl-4H-pyrido[2,3-e][1,4]oxazin-3-one;2,2-dimethyl-4H-pyrido[3,2-b][1,4]oxazin-3-one;2,2-dimethyl-2H-pyrido[3,2-b]-1,4-oxazin-3(4H)-one;2,2-DIMETHYL-2H-PYRIDO(3,2-B)(1,4)OXAZINE-3(4H)-ONE;2H-Pyrido[3,2-b]-1,4-oxazin-3(4H)-one, 2,2-diMethyl-;2,2-diMethyl-2H,3H,4H-pyrido[3,2-b][1,4]oxazin-3-one
CBNumber: CB5909443
Molecular Formula: C9H10N2O2
Formula Weight: 178.19
MOL File: 20348-21-4.mol

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2,2-dimethyl-2H-pyrido[3,2-b]-1,4-oxazin-3(4H)-one Property

Boiling point:: 352.5±37.0 °C(Predicted)
Density: 1.176±0.06 g/cm3 (20 ºC 760 Torr)
storage temp.: Store at room temperature
pka: 11.13±0.40(Predicted)
form: solid
Appearance: White to off-white Solid
InChI: InChI=1S/C9H10N2O2/c1-9(2)8(12)11-7-6(13-9)4-3-5-10-7/h3-5H,1-2H3,(H,10,11,12)
InChIKey: DMLNXUUGRSBBBR-UHFFFAOYSA-N
SMILES: O1C(C)(C)C(=O)NC2=NC=CC=C12

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Safety

HS Code: 2934999090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word: Warning
Hazard statements: H302Harmful if swallowed

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: PHB00083
Product name: 2,2-Dimethyl-2H-pyrido[3,2-b][1,4]oxazin-3(4H)-one
Purity: AldrichCPR
Packaging: 1G
Price: $201
Updated: 2023/06/20

TRC

Product number: D479888
Product name: 2,2-Dimethyl-2H-pyrido[3,2-b][1,4]oxazin-3(4H)-one
Packaging: 50mg
Price: $45
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H56-1-MB
Product name: 2,2-Dimethyl-2H-pyrido[3,2-b][1,4]oxazin-3(4H)-one
Packaging: 1g
Price: $75
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FD126905
Product name: 2,2-Dimethyl-2H-pyrido[3,2-b][1,4]oxazin-3(4H)-one
Packaging: 250mg
Price: $85
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FD126905
Product name: 2,2-Dimethyl-2H-pyrido[3,2-b][1,4]oxazin-3(4H)-one
Packaging: 500mg
Price: $150
Updated: 2021/12/16

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2,2-dimethyl-2H-pyrido[3,2-b]-1,4-oxazin-3(4H)-one Chemical Properties,Usage,Production

Synthesis

16867-03-1

600-00-0

20348-21-4

Step - (i): Synthesis of 2,2-dimethyl-2H-pyrido[3,2-B][1,4]oxazin-3(4H)-one (18.1) 2-Amino-3-hydroxypyridine (5 g, 45.45 mmol) was dissolved in acetone (50 mL) at 20-35 °C and stirred to form a solution. Subsequently K2CO3 (25.09g, 181.81mmol) was added followed by dropwise addition of ethyl 2-bromo-2-methylpropionate (13.29g, 68.18mmol). The reaction mixture was stirred at 70 °C for 16 hours. After completion of the reaction, the mixture was cooled to 20-35 °C and diluted with ice water. The resulting solid was collected by filtration and washed with water to afford the target compound as a white solid (5g, 97% yield). 1H NMR (400MHz, DMSO-d6): [specific NMR data should be added here].

References

[1] Patent: WO2015/71780, 2015, A1. Location in patent: Page/Page column 22
[2] Tetrahedron Letters, 2010, vol. 51, # 14, p. 1852 - 1855
[3] Acta Chemica Scandinavica (1947-1973), 1969, vol. 23, p. 2322 - 2324

2,2-dimethyl-2H-pyrido[3,2-b]-1,4-oxazin-3(4H)-one Preparation Products And Raw materials

Raw materials

Preparation Products

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2,2-dimethyl-2H-pyrido[3,2-b]-1,4-oxazin-3(4H)-one Suppliers

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View Lastest Price from 2,2-dimethyl-2H-pyrido[3,2-b]-1,4-oxazin-3(4H)-one manufacturers

Shanghai Rlavie Technology Co ltd

Product: 2,2-dimethyl-2H,3H,4H-pyrido[3,2-b][1,4]oxazin-3-one 20348-21-4
Price: US $0.00-0.00/KG
Min. Order: 1g
Purity: 98%min
Supply Ability: 100kgs/month
Release date: 2021-11-20

Career Henan Chemical Co

Product: 2,2-dimethyl-2H-pyrido[3,2-b]-1,4-oxazin-3(4H)-one 20348-21-4
Price: US $0.00/KG
Min. Order: 1KG
Purity: 90%-99.9%
Supply Ability: 500kg
Release date: 2019-07-05

20348-21-4, 2,2-dimethyl-2H-pyrido[3,2-b]-1,4-oxazin-3(4H)-oneRelated Search:

2,2-dimethyl-2H-pyrido[3,2-b]-1,4-oxazin-3(4H)-one

Einecs 243-753-2

2,2-dimethyl-4H-pyrido[3,2-b][1,4]oxazin-3-one

2,2-diMethyl-2H,3H,4H-pyrido[3,2-b][1,4]oxazin-3-one

2H-Pyrido[3,2-b]-1,4-oxazin-3(4H)-one, 2,2-diMethyl-

2,2-dimethyl-4H-pyrido[2,3-e][1,4]oxazin-3-one

2,2-Dimethyl-2H-pyrido[3,2-b][1,4]oxazin-3(4H)

2,2-DIMETHYL-2H-PYRIDO(3,2-B)(1,4)OXAZINE-3(4H)-ONE

20348-21-4