3-IODOPHENYL ACETATE
- Product Name
- 3-IODOPHENYL ACETATE
- CAS No.
- 42861-71-2
- Chemical Name
- 3-IODOPHENYL ACETATE
- Synonyms
- Phenol, 3-iodo-, 1-acetate;Acetic acid 3-iodo-phenyl ester
- CBNumber
- CB61010383
- Molecular Formula
- C8H7IO2
- Formula Weight
- 262.04
- MOL File
- 42861-71-2.mol
3-IODOPHENYL ACETATE Property
- storage temp.
- 2-8°C(protect from light)
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- A145040
- Product name
- AceticAcid3-Iodo-phenylEster
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- HCH0352036
- Product name
- 3-IODOPHENYL ACETATE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $500.05
- Updated
- 2021/12/16
- Product number
- 3855CU
- Product name
- 3-Iodophenylacetate
- Packaging
- 250mg
- Price
- $91
- Updated
- 2021/12/16
- Product number
- CC00-2012
- Product name
- Aceticacid3-iodo-phenylester
- Purity
- ＞97%
- Packaging
- 10g
- Price
- $200
- Updated
- 2021/12/16
- Product number
- A115515
- Product name
- 3-Iodophenylacetate
- Purity
- 95+%
- Packaging
- 5g
- Price
- $202
- Updated
- 2021/12/16
3-IODOPHENYL ACETATE Chemical Properties,Usage,Production
Synthesis
626-02-8
75-36-5
42861-71-2
a) Synthesis of 3-iodophenyl acetate 3-Iodophenol (3 g, 13.6 mmol), acetyl chloride (2.9 ml, 40.9 mmol) and potassium carbonate (9.42 g, 68.2 mmol) were dissolved in N,N-dimethylformamide (75 ml) and the reaction was stirred for 16 hours at room temperature. After completion of the reaction, the mixture was partitioned between water and ethyl acetate. The organic layer was washed with 1N NaOH solution, dried over anhydrous magnesium sulfate and subsequently concentrated under reduced pressure. The crude product was purified by silica gel column chromatography using 20% ethyl acetate/hexane as eluent to give 2.3 g (65% yield) of 3-iodophenyl acetate. Nuclear magnetic resonance hydrogen spectroscopy (1H NMR, CDCl3) data were as follows: δ 7.57 (1H, m), 7.46 (1H, m), 7.08 (2H, m), 2.29 (3H, s).
References
[1] Bioorganic and Medicinal Chemistry, 2004, vol. 12, # 9, p. 2079 - 2098
[2] Journal of Medicinal Chemistry, 2005, vol. 48, # 4, p. 926 - 934
[3] Journal of Medicinal Chemistry, 1997, vol. 40, # 23, p. 3804 - 3819
[4] Patent: US2003/18064, 2003, A1
[5] Patent: WO2012/49460, 2012, A1. Location in patent: Page/Page column 43
3-IODOPHENYL ACETATE Preparation Products And Raw materials
Raw materials
Preparation Products
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