3-IODOPHENYL ACETATE

Product Name: 3-IODOPHENYL ACETATE
CAS No.: 42861-71-2
Chemical Name: 3-IODOPHENYL ACETATE
Synonyms: Phenol, 3-iodo-, 1-acetate;Acetic acid 3-iodo-phenyl ester
CBNumber: CB61010383
Molecular Formula: C8H7IO2
Formula Weight: 262.04
MOL File: 42861-71-2.mol

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3-IODOPHENYL ACETATE Property

storage temp.: 2-8°C(protect from light)

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: A145040
Product name: AceticAcid3-Iodo-phenylEster
Packaging: 50mg
Price: $45
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0352036
Product name: 3-IODOPHENYL ACETATE
Purity: 95.00%
Packaging: 5MG
Price: $500.05
Updated: 2021/12/16

AK Scientific

Product number: 3855CU
Product name: 3-Iodophenylacetate
Packaging: 250mg
Price: $91
Updated: 2021/12/16

Chemcia Scientific

Product number: CC00-2012
Product name: Aceticacid3-iodo-phenylester
Purity: ＞97%
Packaging: 10g
Price: $200
Updated: 2021/12/16

Ambeed

Product number: A115515
Product name: 3-Iodophenylacetate
Purity: 95+%
Packaging: 5g
Price: $202
Updated: 2021/12/16

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3-IODOPHENYL ACETATE Chemical Properties,Usage,Production

Synthesis

626-02-8

75-36-5

42861-71-2

a) Synthesis of 3-iodophenyl acetate 3-Iodophenol (3 g, 13.6 mmol), acetyl chloride (2.9 ml, 40.9 mmol) and potassium carbonate (9.42 g, 68.2 mmol) were dissolved in N,N-dimethylformamide (75 ml) and the reaction was stirred for 16 hours at room temperature. After completion of the reaction, the mixture was partitioned between water and ethyl acetate. The organic layer was washed with 1N NaOH solution, dried over anhydrous magnesium sulfate and subsequently concentrated under reduced pressure. The crude product was purified by silica gel column chromatography using 20% ethyl acetate/hexane as eluent to give 2.3 g (65% yield) of 3-iodophenyl acetate. Nuclear magnetic resonance hydrogen spectroscopy (1H NMR, CDCl3) data were as follows: δ 7.57 (1H, m), 7.46 (1H, m), 7.08 (2H, m), 2.29 (3H, s).

References

[1] Bioorganic and Medicinal Chemistry, 2004, vol. 12, # 9, p. 2079 - 2098
[2] Journal of Medicinal Chemistry, 2005, vol. 48, # 4, p. 926 - 934
[3] Journal of Medicinal Chemistry, 1997, vol. 40, # 23, p. 3804 - 3819
[4] Patent: US2003/18064, 2003, A1
[5] Patent: WO2012/49460, 2012, A1. Location in patent: Page/Page column 43

3-IODOPHENYL ACETATE Preparation Products And Raw materials

Raw materials

Preparation Products

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3-IODOPHENYL ACETATE Suppliers

China 18 India 1 United States 3 Global 22

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42861-71-2, 3-IODOPHENYL ACETATERelated Search:

3-(DIACETOXYIODO)TOLUENE SALOR-INT L134899-1EA 5-IODO-6-AMINO-1,2-BENZOPYRONE IODOMESITYLENE DIACETATE 3-IODOPHENYL ACETATE

Acetic acid 3-iodo-phenyl ester

Phenol, 3-iodo-, 1-acetate

42861-71-2