Pyridine, 5-bromo-2-(chloromethyl)- (9CI)

Product Name: Pyridine, 5-bromo-2-(chloromethyl)- (9CI)
CAS No.: 168823-76-5
Chemical Name: Pyridine, 5-bromo-2-(chloromethyl)- (9CI)
Synonyms: RSYY(Vorapaxar Sulfatet)-53;5-bromo-2-(chloromethyl)pyridine;Pyridine, 5-bromo-2-(chloromethyl)-;Pyridine, 5-bromo-2-(chloromethyl)- (9CI)
CBNumber: CB61055926
Molecular Formula: C6H5BrClN
Formula Weight: 206.47
MOL File: 168823-76-5.mol

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Pyridine, 5-bromo-2-(chloromethyl)- (9CI) Property

Boiling point:: 243.4±25.0 °C(Predicted)
Density: 1.631±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
pka: 1.35±0.22(Predicted)
Appearance: Light brown to yellow Liquid

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC

Product number: B614080
Product name: 5-Bromo-2-(chloromethyl)pyridine
Packaging: 10mg
Price: $45
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0366823
Product name: 5-BROMO-2-(CHLOROMETHYL)PYRIDINE
Purity: 95.00%
Packaging: 5MG
Price: $495.07
Updated: 2021/12/16

Ambeed

Product number: A142230
Product name: 5-Bromo-2-(chloromethyl)pyridine
Purity: 97%
Packaging: 5g
Price: $844
Updated: 2021/12/16

Chemenu

Product number: CM127652
Product name: 5-bromo-2-(chloromethyl)pyridine
Purity: 97%
Packaging: 5g
Price: $847
Updated: 2021/12/16

Crysdot

Product number: CD11240133
Product name: 5-Bromo-2-(chloromethyl)pyridine
Purity: 97%
Packaging: 5g
Price: $897
Updated: 2021/12/16

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Pyridine, 5-bromo-2-(chloromethyl)- (9CI) Chemical Properties,Usage,Production

Synthesis

88139-91-7

168823-76-5

Part B: 5-Bromo-2-hydroxymethylpyridine (500 mg, 2.7 mmol) was dissolved in dichloromethane (5 mL) and cooled in an ice bath to 0°C. Thionyl chloride (480 mg, 4.05 mmol) was added slowly dropwise, and after completion of the dropwise addition, the reaction mixture was transferred to room temperature and stirred for 3 hours. After completion of the reaction, the reaction was quenched with saturated sodium bicarbonate solution. The organic layer was separated, dried over anhydrous sodium sulfate and concentrated under reduced pressure to give 5-bromo-2-chloromethylpyridine (510 mg, 92% yield).

References

[1] Journal of Porphyrins and Phthalocyanines, 2010, vol. 14, # 6, p. 469 - 480
[2] Patent: WO2007/84451, 2007, A1. Location in patent: Page/Page column 147
[3] Chemistry - A European Journal, 2011, vol. 17, # 38, p. 10670 - 10681
[4] Journal of Organic Chemistry, 2004, vol. 69, # 2, p. 250 - 262
[5] Patent: WO2006/76415, 2006, A2. Location in patent: Page/Page column 46

Pyridine, 5-bromo-2-(chloromethyl)- (9CI) Preparation Products And Raw materials

Raw materials

Preparation Products

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Pyridine, 5-bromo-2-(chloromethyl)- (9CI) Suppliers

China 51 Europe 1 United States 3 Global 55

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View Lastest Price from Pyridine, 5-bromo-2-(chloromethyl)- (9CI) manufacturers

ZHENGZHOU JIUYI TIME NEW MATERIALS CO,.LTD

Product: 5-Bromo-2-(chloromethyl)pyridine 168823-76-5
Price: US $2.00-6.00/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: 100kg
Release date: 2025-08-07

Career Henan Chemica Co

Product: Pyridine, 5-bromo-2-(chloromethyl)- (9CI) 168823-76-5
Price: US $0.37/g
Min. Order: 1g
Purity: 99%min cherry@coreychem.com
Supply Ability: 1kg/10kg
Release date: 2020-11-29

168823-76-5, Pyridine, 5-bromo-2-(chloromethyl)- (9CI)Related Search:

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168823-76-5

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