Ethanone, 1-[3-(1-methylethyl)phenyl]- (9CI)

Product Name: Ethanone, 1-[3-(1-methylethyl)phenyl]- (9CI)
CAS No.: 40428-87-3
Chemical Name: Ethanone, 1-[3-(1-methylethyl)phenyl]- (9CI)
Synonyms: 1-[3-(1-Methylethyl)phenyl]ethanone;Ethanone, 1-[3-(1-methylethyl)phenyl]-;Ethanone, 1-[3-(1-methylethyl)phenyl]- (9CI)
CBNumber: CB61064311
Molecular Formula: C11H14O
Formula Weight: 162.23
MOL File: 40428-87-3.mol

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Ethanone, 1-[3-(1-methylethyl)phenyl]- (9CI) Property

Boiling point:: 84-90 °C(Press: 0.2 Torr)
Density: 0.948±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

AK Scientific

Product number: 5442AB
Product name: 1-(3-Isopropylphenyl)ethanone
Packaging: 100mg
Price: $172
Updated: 2021/12/16

AK Scientific

Product number: 5442AB
Product name: 1-(3-Isopropylphenyl)ethanone
Packaging: 250mg
Price: $244
Updated: 2021/12/16

Rieke Metals

Product number: AC0307
Product name: 1-(3-Isopropylphenyl)ethanone
Packaging: 1g
Price: $294
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0309552
Product name: 1-(3-ISOPROPYLPHENYL)ETHANONE
Purity: 95.00%
Packaging: 5MG
Price: $500.98
Updated: 2021/12/16

Rieke Metals

Product number: AC0307
Product name: 1-(3-Isopropylphenyl)ethanone
Packaging: 5g
Price: $701
Updated: 2021/12/16

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Ethanone, 1-[3-(1-methylethyl)phenyl]- (9CI) Chemical Properties,Usage,Production

Synthesis

5433-01-2

78191-00-1

40428-87-3

A THF solution (250 mL) of 1-bromo-3-(propan-2-yl)benzene (5.0 g, 25.11 mmol, 1.00 eq.) was added to a 500 mL round-bottomed flask protected by an inert N2 atmosphere. The reaction system was cooled to -60 °C and n-butyllithium (20 mL, 2.00 eq.) was slowly added dropwise under stirring. After the dropwise addition, stirring was continued at -60 °C for 30 min. Subsequently, the reaction system was warmed to -30 °C and N-methoxy-N-methylacetamide (3.9 g, 37.82 mmol, 1.50 eq.) was added slowly dropwise under stirring. After completion of the dropwise addition, the reaction mixture was continued to be stirred in a liquid nitrogen bath at -30 °C for 3 hours. At the end of the reaction, the reaction was quenched by adding 20 mL of water. The reaction mixture was diluted with 200 mL of ethyl acetate, washed sequentially with 2 x 100 mL of brine, and the organic phase was dried over anhydrous Na2SO4 and concentrated under reduced pressure. The residue was purified by silica gel column chromatography with ethyl acetate/petroleum ether (1:10) as eluent to give 2.7 g (66% yield) of the target product 1-(3-isopropylphenyl)ethanone as a colorless oil.

References

[1] Patent: WO2016/201426, 2016, A1. Location in patent: Paragraph 0243
[2] Patent: WO2013/78233, 2013, A1. Location in patent: Page/Page column 62
[3] Patent: WO2013/78240, 2013, A1. Location in patent: Page/Page column 57
[4] Patent: WO2017/214505, 2017, A1. Location in patent: Paragraph 000505; 000506

Ethanone, 1-[3-(1-methylethyl)phenyl]- (9CI) Preparation Products And Raw materials

Raw materials

Preparation Products

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40428-87-3, Ethanone, 1-[3-(1-methylethyl)phenyl]- (9CI)Related Search:

Ethanone, 1-[3-(1-methylethyl)phenyl]- (9CI)

Ethanone, 1-[3-(1-methylethyl)phenyl]-

1-[3-(1-Methylethyl)phenyl]ethanone

40428-87-3

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