2-Pyrimidinamine, 4-chloro-5-methyl- (9CI)

Product Name: 2-Pyrimidinamine, 4-chloro-5-methyl- (9CI)
CAS No.: 20090-58-8
Chemical Name: 2-Pyrimidinamine, 4-chloro-5-methyl- (9CI)
Synonyms: 4-Chloro-5-methylpyrimidin-2-amine;4-Chloro-5-methyl-2-pyrimidinamine;4-Chloro-2-amino-5-methylpyrimidine;2-Amino-4-chloro-5-methylpyrimidine;2-Pyrimidinamine, 4-chloro-5-methyl-;2-Pyrimidinamine, 4-chloro-5-methyl- (9CI);4-Chloro-5-methylpyrimidin-2-amine, 2-Amino-4-chloro-5-methyl-1,3-diazine
CBNumber: CB61081301
Molecular Formula: C5H6ClN3
Formula Weight: 143.57
MOL File: 20090-58-8.mol

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2-Pyrimidinamine, 4-chloro-5-methyl- (9CI) Property

Melting point:: 184-185℃
Boiling point:: 320.8±34.0 °C(Predicted)
Density: 1.349±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
form: solid
pka: 3.99±0.10(Predicted)
color: Light yellow to yellow

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Safety

HS Code: 2933599590

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TRC

Product number: C350035
Product name: 4-Chloro-5-methylpyrimidin-2-amine
Packaging: 250mg
Price: $75
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0025575
Product name: 4-CHLORO-5-METHYL-PYRIMIDIN-2-YLAMINE
Purity: 95.00%
Packaging: 250MG
Price: $284.55
Updated: 2021/12/16

AK Scientific

Product number: W4243
Product name: 4-Chloro-5-methylpyrimidin-2-amine
Packaging: 250mg
Price: $108
Updated: 2021/12/16

Matrix Scientific

Product number: 073828
Product name: 4-Chloro-5-methylpyrimidin-2-amine
Purity: 95+%
Packaging: 500mg
Price: $140
Updated: 2021/12/16

SynQuest Laboratories

Product number: 3H30-5-Y9
Product name: 2-Amino-4-chloro-5-methylpyrimidine
Packaging: 250mg
Price: $175
Updated: 2021/12/16

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2-Pyrimidinamine, 4-chloro-5-methyl- (9CI) Chemical Properties,Usage,Production

Synthesis

15981-91-6

20090-58-8

Step b: Synthesis of 4-chloro-2-amino-5-methylpyrimidine 5-Methylisocytosine (3 g, 24.0 mmol) was mixed with phosphorus trichloride (POCl3, 20 mL) and heated to reflux for 45 minutes. Upon completion of the reaction, the excess phosphorous trichloride was removed by distillation under reduced pressure. The residue was slowly poured into ice water and the pH was subsequently adjusted to alkaline with ammonia at 10 °C. The precipitated solid was collected by filtration and recrystallized from ethanol to afford the target compound 4-chloro-2-amino-5-methylpyrimidine (1 g, 29.0% yield). 1H NMR (400 MHz, DMSO-d6) δ: 8.11 (s, 1H, pyrimidine ring H), 6.81 (br s, 2H, NH2), 2.04 (s, 3H, CH3).

References

[1] Patent: US2009/221597, 2009, A1. Location in patent: Page/Page column 41
[2] Journal of the Chemical Society, 1947, p. 41,45

2-Pyrimidinamine, 4-chloro-5-methyl- (9CI) Preparation Products And Raw materials

Raw materials

Preparation Products

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2-Pyrimidinamine, 4-chloro-5-methyl- (9CI) Suppliers

China 87 Europe 1 India 2 Switzerland 1 United Kingdom 2 United States 6 Global 99

Shanghai Hanhong Scientific Co.,Ltd.

Tel: 021-54306202 13764082696
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Shanghai Sunway Pharmaceutical Technology Co., Ltd

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Amber MolTech LLC

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Shanghai Topbiochem Technology Co., Ltd

Tel: 021-58170097
Email: info@topbiochem.com
Country: China
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Shanghai potentpharm CO.,Ltd

Tel: (86) 21 51969655
Fax: (86) 21 51969655， QQ：33109286， 263541193
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SuZhou ShiYa Biopharmaceuticals, Inc.

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9ding chemical ( Shanghai) Limited

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SynAsst Chemical.

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Shanghai Raise Chemical Technology Co.,Ltd

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EnliPharma Technology Co., Ltd

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View Lastest Price from 2-Pyrimidinamine, 4-chloro-5-methyl- (9CI) manufacturers

Career Henan Chemical Co

Product: 2-Pyrimidinamine, 4-chloro-5-methyl- (9CI) 20090-58-8
Price: US $3.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100kg
Release date: 2019-07-04

Hebei Jimi Trading Co., Ltd.

Product: 2-Pyrimidinamine, 4-chloro-5-methyl- (9CI) 20090-58-8
Price: US $1.00/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: 500KG
Release date: 2019-04-16

20090-58-8, 2-Pyrimidinamine, 4-chloro-5-methyl- (9CI)Related Search:

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2-Pyrimidinamine, 4-chloro-5-methyl- (9CI)

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