ChemicalBook > CAS DataBase List > 2-Pyrimidinamine, 4-chloro-5-methyl- (9CI)

2-Pyrimidinamine, 4-chloro-5-methyl- (9CI)

Product Name
2-Pyrimidinamine, 4-chloro-5-methyl- (9CI)
CAS No.
20090-58-8
Chemical Name
2-Pyrimidinamine, 4-chloro-5-methyl- (9CI)
Synonyms
4-Chloro-5-methylpyrimidin-2-amine;4-Chloro-5-methyl-2-pyrimidinamine;4-Chloro-2-amino-5-methylpyrimidine;2-Amino-4-chloro-5-methylpyrimidine;2-Pyrimidinamine, 4-chloro-5-methyl-;2-Pyrimidinamine, 4-chloro-5-methyl- (9CI);4-Chloro-5-methylpyrimidin-2-amine, 2-Amino-4-chloro-5-methyl-1,3-diazine
CBNumber
CB61081301
Molecular Formula
C5H6ClN3
Formula Weight
143.57
MOL File
20090-58-8.mol
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2-Pyrimidinamine, 4-chloro-5-methyl- (9CI) Property

Melting point:
184-185℃
Boiling point:
320.8±34.0 °C(Predicted)
Density 
1.349±0.06 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2–8 °C
form 
solid
pka
3.99±0.10(Predicted)
color 
Light yellow to yellow
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Safety

HS Code 
2933599590
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TRC
Product number
C350035
Product name
4-Chloro-5-methylpyrimidin-2-amine
Packaging
250mg
Price
$75
Updated
2021/12/16
AK Scientific
Product number
W4243
Product name
4-Chloro-5-methylpyrimidin-2-amine
Packaging
250mg
Price
$108
Updated
2021/12/16
Matrix Scientific
Product number
073828
Product name
4-Chloro-5-methylpyrimidin-2-amine
Purity
95+%
Packaging
500mg
Price
$140
Updated
2021/12/16
SynQuest Laboratories
Product number
3H30-5-Y9
Product name
2-Amino-4-chloro-5-methylpyrimidine
Packaging
250mg
Price
$175
Updated
2021/12/16
Matrix Scientific
Product number
073828
Product name
4-Chloro-5-methylpyrimidin-2-amine
Purity
95+%
Packaging
1g
Price
$215
Updated
2021/12/16
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2-Pyrimidinamine, 4-chloro-5-methyl- (9CI) Chemical Properties,Usage,Production

Synthesis

15981-91-6

20090-58-8

Step b: Synthesis of 4-chloro-2-amino-5-methylpyrimidine 5-Methylisocytosine (3 g, 24.0 mmol) was mixed with phosphorus trichloride (POCl3, 20 mL) and heated to reflux for 45 minutes. Upon completion of the reaction, the excess phosphorous trichloride was removed by distillation under reduced pressure. The residue was slowly poured into ice water and the pH was subsequently adjusted to alkaline with ammonia at 10 °C. The precipitated solid was collected by filtration and recrystallized from ethanol to afford the target compound 4-chloro-2-amino-5-methylpyrimidine (1 g, 29.0% yield). 1H NMR (400 MHz, DMSO-d6) δ: 8.11 (s, 1H, pyrimidine ring H), 6.81 (br s, 2H, NH2), 2.04 (s, 3H, CH3).

References

[1] Patent: US2009/221597, 2009, A1. Location in patent: Page/Page column 41
[2] Journal of the Chemical Society, 1947, p. 41,45

2-Pyrimidinamine, 4-chloro-5-methyl- (9CI) Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 2-Pyrimidinamine, 4-chloro-5-methyl- (9CI) manufacturers

Career Henan Chemical Co
Product
2-Pyrimidinamine, 4-chloro-5-methyl- (9CI) 20090-58-8
Price
US $3.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
100kg
Release date
2019-07-04
Hebei Jimi Trading Co., Ltd.
Product
2-Pyrimidinamine, 4-chloro-5-methyl- (9CI) 20090-58-8
Price
US $1.00/kg
Min. Order
1kg
Purity
99%
Supply Ability
500KG
Release date
2019-04-16

20090-58-8, 2-Pyrimidinamine, 4-chloro-5-methyl- (9CI)Related Search:

2-Amino-4,6-dichloro-pyrimidine-5-carbaldehyde 2-AMINO-4,6-DIHYDROXY-5-METHYLPYRIMIDINE 4-CHLORO-5-ETHYL-6-METHYL-PYRIMIDIN-2-YLAMINE 4-CHLORO-5-(4-CHLORO-BENZYL)-6-METHYL-PYRIMIDIN-2-YLAMINE 4-CHLORO-6-METHYL-5-NAPHTHALEN-1-YLMETHYL-PYRIMIDIN-2-YLAMINE CHEMBRDG-BB 4015982 4-CHLORO-5,6-DIMETHYL-PYRIMIDIN-2-YLAMINE 5-ALLYL-2-AMINO-6-CHLORO-4-PYRIMIDINOL CHEMBRDG-BB 4015981 4-CHLORO-5-(2-CHLORO-BENZYL)-6-METHYL-PYRIMIDIN-2-YLAMINE 5-ALLYL-4-CHLORO-6-METHYL-PYRIMIDIN-2-YLAMINE CHEMBRDG-BB 4015983 2-Pyrimidinamine, 4-chloro-5-methyl- (9CI) 2-AMINO-4-[BENZYL(METHYL)AMINO]-6-CHLORO-5-PYRIMIDINECARBALDEHYDE N-(4-CHLORO-6-HYDRAZINO-5-PHENYLPYRIMIDIN-2-YL)-N,N-DIMETHYLAMINE RARECHEM AN KA 0877 2-AMINO-4-CHLORO-6-PIPERIDINO-5-PYRIMIDINECARBALDEHYDE 2-PYRIMIDINAMINE, 4-CHLORO-6-METHYL-5-(PHENYLMETHYL)-

  • 2-Pyrimidinamine, 4-chloro-5-methyl- (9CI)
  • 4-Chloro-5-methylpyrimidin-2-amine
  • 2-Amino-4-chloro-5-methylpyrimidine
  • 4-Chloro-5-methylpyrimidin-2-amine, 2-Amino-4-chloro-5-methyl-1,3-diazine
  • 4-Chloro-2-amino-5-methylpyrimidine
  • 4-Chloro-5-methyl-2-pyrimidinamine
  • 2-Pyrimidinamine, 4-chloro-5-methyl-
  • 20090-58-8
  • 20090-55-8
  • PYRIMIDINE