Ethyl-2-fluoro-5-iodobenzoate
- Product Name
- Ethyl-2-fluoro-5-iodobenzoate
- CAS No.
- 773136-66-6
- Chemical Name
- Ethyl-2-fluoro-5-iodobenzoate
- Synonyms
- Ethyl-2-fluoro-5-iodobenzoate;Benzoic acid, 2-fluoro-5-iodo-, ethyl ester
- CBNumber
- CB61114537
- Molecular Formula
- C9H8FIO2
- Formula Weight
- 294.06
- MOL File
- 773136-66-6.mol
Ethyl-2-fluoro-5-iodobenzoate Property
- storage temp.
- 2-8°C(protect from light)
- Appearance
- Colorless to light yellow Liquid
Safety
- HS Code
- 2916399090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H226Flammable liquid and vapour
- Precautionary statements
-
P210Keep away from heat/sparks/open flames/hot surfaces. — No smoking.
P233Keep container tightly closed.
P240Ground/bond container and receiving equipment.
P241Use explosion-proof electrical/ventilating/lighting/…/equipment.
P242Use only non-sparking tools.
P243Take precautionary measures against static discharge.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.
P370+P378In case of fire: Use … for extinction.
P403+P235Store in a well-ventilated place. Keep cool.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- HCH0014154
- Product name
- ETHYL-2-FLUORO-5-IODOBENZOATE
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $720.37
- Updated
- 2021/12/16
- Product number
- HCH0014154
- Product name
- ETHYL-2-FLUORO-5-IODOBENZOATE
- Purity
- 95.00%
- Packaging
- 5G
- Price
- $1285.52
- Updated
- 2021/12/16
- Product number
- A179873
- Product name
- Ethyl2-Fluoro-5-iodobenzoate
- Purity
- 95+%
- Packaging
- 250mg
- Price
- $22
- Updated
- 2021/12/16
- Product number
- A179873
- Product name
- Ethyl2-Fluoro-5-iodobenzoate
- Purity
- 95+%
- Packaging
- 1g
- Price
- $50
- Updated
- 2021/12/16
- Product number
- MB-16775
- Product name
- ethyl2-fluoro-5-iodobenzoate
- Purity
- 97%
- Packaging
- 1g
- Price
- $110
- Updated
- 2021/12/16
Ethyl-2-fluoro-5-iodobenzoate Chemical Properties,Usage,Production
Synthesis
64-17-5
124700-41-0
773136-66-6
General procedure for the synthesis of ethyl 2-fluoro-5-iodobenzoate from ethanol and 2-fluoro-5-iodobenzoic acid: 2-Fluoro-5-iodobenzoic acid (Oakwood, 0.99 g, 3.72 mmol) and H2SO4 (198 μL, 3.72 mmol) were added to EtOH (7.4 mL). The reaction mixture was stirred at 100 °C overnight. After completion of the reaction, the mixture was concentrated in vacuum. The crude product was purified by fast column chromatography (gradient of 0 to 10% EtOAc/hexane) to afford the title compound ethyl 2-fluoro-5-iodobenzoate (916 mg, 84%) as a colorless oil. 1H NMR (CDCl3) δ 8.24 (dd, J = 6.8, 2.4 Hz, 1H), 7.81 (ddd, J = 8.8, 4.5, 2.4 Hz, 1H), 6.93 (dd, J = 10.3, 8.6 Hz, 1H), 4.41 (q, J = 7.0 Hz, 2H), 1.42 (t, J = 7.2 Hz, 3H).
References
[1] Patent: WO2012/162365, 2012, A1. Location in patent: Page/Page column 173-174
Ethyl-2-fluoro-5-iodobenzoate Preparation Products And Raw materials
Raw materials
Preparation Products
Ethyl-2-fluoro-5-iodobenzoate Suppliers
- Tel
- --
- Fax
- --
- vernam@fluorochem.co.uk
- Country
- United Kingdom
- ProdList
- 6375
- Advantage
- 65