4-Ethylsulfonylbenzaldehyde

Product Name: 4-Ethylsulfonylbenzaldehyde
CAS No.: 50899-03-1
Chemical Name: 4-Ethylsulfonylbenzaldehyde
Synonyms: 4-Ethylsulfonylbenzaldehyde;Benzaldehyde, 4-(ethylsulfonyl)-
CBNumber: CB61115574
Molecular Formula: C9H10O3S
Formula Weight: 198.24
MOL File: Mol file

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4-Ethylsulfonylbenzaldehyde Property

Melting point:: 108～110℃
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C

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Safety

HS Code: 2913000090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

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N-Bromosuccinimide Price

ChemScene

Product number: CS-0061668
Product name: 4-ethylsulfonylbenzaldehyde
Packaging: 1g
Price: $208
Updated: 2021/12/16

SynQuest Laboratories

Product number: 6663-1-04
Product name: 4-(Ethylsulfonyl)benzaldehyde
Purity: 97%
Packaging: 1g
Price: $240
Updated: 2021/12/16

Matrix Scientific

Product number: 024873
Product name: 4-Ethylsulfonylbenzaldehyde
Packaging: 1g
Price: $268
Updated: 2021/12/16

ChemScene

Product number: CS-0061668
Product name: 4-ethylsulfonylbenzaldehyde
Packaging: 100mg
Price: $62
Updated: 2021/12/16

ChemScene

Product number: CS-0061668
Product name: 4-ethylsulfonylbenzaldehyde
Packaging: 250mg
Price: $104
Updated: 2021/12/16

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4-Ethylsulfonylbenzaldehyde Chemical Properties,Usage,Production

Synthesis

84211-94-9

50899-03-1

4-(Ethylthio)benzaldehyde (2.46 g, 14.8 mmol) was dissolved in dichloromethane (100 mL) at 0 °C and m-chloroperoxybenzoic acid (m-CPBA, 7 g, 31.1 mmol) was added in batches with stirring. The reaction mixture was stirred continuously at 0 °C for 1 hour. Subsequently, 1M sodium hydroxide solution (35 mL) was added and stirring was continued for 10 minutes. Upon completion of the reaction, the reaction mixture was extracted with dichloromethane and the organic layer was washed with saturated brine and subsequently concentrated under reduced pressure. Unreacted m-CPBA was found to remain in the reaction by 1H NMR analysis, so the crude product was redissolved in ethyl acetate and washed five times with 1 M sodium hydroxide solution to completely remove the residual m-CPBA. finally, the organic layer was concentrated under reduced pressure to afford 2.16 g of 4-(ethylsulfonyl)benzaldehyde in 74% yield. The structure of the product was confirmed by 1H NMR (D6-DMSO): δ 10.20 (1H, s), 8.24-8.15 (4H, m), 3.44 (2H, q, J=7.4Hz), 1.16 (3H, t, J=7.4Hz).

References

[1] Patent: US2010/305120, 2010, A1. Location in patent: Page/Page column 53
[2] Annali di Chimica (Rome, Italy), 1951, vol. 41, p. 139,143, 146
[3] Annali di Chimica (Rome, Italy), 1951, vol. 41, p. 139,143, 146

4-Ethylsulfonylbenzaldehyde Preparation Products And Raw materials

Raw materials

Preparation Products

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