2,6-DICHLORO-4-NITROANISOLE
- Product Name
- 2,6-DICHLORO-4-NITROANISOLE
- CAS No.
- 17742-69-7
- Chemical Name
- 2,6-DICHLORO-4-NITROANISOLE
- Synonyms
- NSC 212118;4-Nitro-2,6-dichloroanisole;2,6-DICHLORO-4-NITROANISOLE;1,3-Dichloro-2-Methoxy-5-Nitro;2,6-Dichloro-4-nitroanisole>2,6-DICHLORO-4-NITROANISOLE 99%;2,6-Dichloro-4-nitroanisole, 98%;3,5-Dichloro-4-methoxynitrobenzene;2.6-Dichlor-4-nitro-1-Methoxy-benzol;1,3-Dichloro-5-Methoxy-2-nitrobenzene
- CBNumber
- CB6121226
- Molecular Formula
- C7H5Cl2NO3
- Formula Weight
- 222.03
- MOL File
- 17742-69-7.mol
2,6-DICHLORO-4-NITROANISOLE Property
- Melting point:
- 97-100 °C
- Boiling point:
- 305.6±37.0 °C(Predicted)
- Density
- 1.5223 (rough estimate)
- refractive index
- 1.6140 (estimate)
- Flash point:
- 160 °C
- storage temp.
- Sealed in dry,Room Temperature
- solubility
- DMSO (Sparingly), Chloroform (Slightly)
- form
- Solid
- color
- Pale Yellow to Yellow
- CAS DataBase Reference
- 17742-69-7(CAS DataBase Reference)
Safety
- Hazard Codes
- N-T,T,N
- Risk Statements
- 51/53-25
- Safety Statements
- 61-45-36/37
- RIDADR
- 2811
- Hazard Note
- Toxic
- HazardClass
- IRRITANT
- PackingGroup
- III
- HS Code
- 29049095
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H301Toxic if swalloed
H341Suspected of causing genetic defects
H411Toxic to aquatic life with long lasting effects
- Precautionary statements
-
P201Obtain special instructions before use.
P202Do not handle until all safety precautions have been read and understood.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P273Avoid release to the environment.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P308+P313IF exposed or concerned: Get medical advice/attention.
P391Collect spillage. Hazardous to the aquatic environment
P405Store locked up.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- D2872
- Product name
- 2,6-Dichloro-4-nitroanisole
- Purity
- >98.0%(GC)
- Packaging
- 1g
- Price
- $53
- Updated
- 2025/07/31
- Product number
- D2872
- Product name
- 2,6-Dichloro-4-nitroanisole
- Purity
- >98.0%(GC)
- Packaging
- 5g
- Price
- $158
- Updated
- 2025/07/31
- Product number
- D438480
- Product name
- 2,6-Dichloro-4-nitroanisole
- Packaging
- 500mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- 4654-5-X4
- Product name
- 2,6-Dichloro-4-nitroanisole
- Purity
- 98%
- Packaging
- 1g
- Price
- $28
- Updated
- 2021/12/16
- Product number
- FD33375
- Product name
- 2,6-Dichloro-4-nitroanisole
- Packaging
- 500mg
- Price
- $45
- Updated
- 2021/12/16
2,6-DICHLORO-4-NITROANISOLE Chemical Properties,Usage,Production
Chemical Properties
slightly beige crystals
Uses
2,6-Dichloro-4-nitroanisole can be used for thyroid hormone receptor agonists.
Synthesis Reference(s)
The Journal of Organic Chemistry, 28, p. 1656, 1963 DOI: 10.1021/jo01041a056
Synthesis
618-80-4
74-88-4
17742-69-7
GENERAL STEPS: To a stirred solution of 2,6-dichloro-4-nitrophenol (6.0 g, 28.84 mmol) in anhydrous DMF (60 mL) was added anhydrous K2CO3 (15.9 g, 115.36 mmol) and iodomethane (8.18 g, 57.69 mmol). The reaction mixture was stirred at 0°C and then gradually warmed up to 60°C and kept for 6 hours. After completion of the reaction, the mixture was cooled to room temperature and slowly poured into ice water to quench the reaction. The precipitated solid was collected by filtration and dried under vacuum to obtain the crude product. The crude product was purified by column chromatography using petroleum ether: ethyl acetate (85:15) as eluent to give 2.5 g (39.0% yield) of 1,3-dichloro-2-methoxy-5-nitrobenzene as an off-white solid. The structure of the product was confirmed by 1H NMR (400 MHz, CDCl3): δ 8.22 (s, 2H), 4.01 (s, 3H).
References
[1] Patent: WO2017/117239, 2017, A1. Location in patent: Page/Page column 42
[2] Journal of Organic Chemistry, 1963, vol. 28, p. 1656 - 1662
[3] Bulletin of the Chemical Society of Japan, 1994, vol. 67, # 10, p. 2639 - 2646
2,6-DICHLORO-4-NITROANISOLE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2,6-DICHLORO-4-NITROANISOLE manufacturers
- Product
- 2,6-DICHLORO-4-NITROANISOLE 17742-69-7
- Price
- US $1.00/ASSAYS
- Min. Order
- 1ASSAYS
- Purity
- 98%min
- Supply Ability
- G/KG/T
- Release date
- 2019-12-23