cycloheptanecarboxamide
- Product Name
- cycloheptanecarboxamide
- CAS No.
- 1459-39-8
- Chemical Name
- cycloheptanecarboxamide
- Synonyms
- cycloheptanecarboxamide
- CBNumber
- CB61259078
- Molecular Formula
- C8H15NO
- Formula Weight
- 141.21
- MOL File
- 1459-39-8.mol
cycloheptanecarboxamide Property
- Melting point:
- 193-194 °C(Solv: ethanol (64-17-5))
- Boiling point:
- 295.2±7.0 °C(Predicted)
- Density
- 0.990±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- pka
- 16.76±0.20(Predicted)
Safety
- HS Code
- 2924297099
N-Bromosuccinimide Price
- Product number
- 114843
- Product name
- Cycloheptanecarboxamide
- Purity
- 97%
- Packaging
- 1g
- Price
- $529
- Updated
- 2021/12/16
- Product number
- 1459398
- Product name
- Cycloheptanecarboxamide
- Packaging
- 5g
- Price
- $545.49
- Updated
- 2021/12/16
- Product number
- CD13022405
- Product name
- Cycloheptanecarboxamide
- Purity
- 97%
- Packaging
- 5g
- Price
- $546
- Updated
- 2021/12/16
- Product number
- 61-11751
- Product name
- Cycloheptanecarboxamide
- Purity
- 95-98%
- Packaging
- 5g
- Price
- $660
- Updated
- 2021/12/16
- Product number
- A127425
- Product name
- Cycloheptanecarboxamide
- Purity
- 97%
- Packaging
- 100mg
- Price
- $49
- Updated
- 2021/12/16
cycloheptanecarboxamide Chemical Properties,Usage,Production
Synthesis
32730-85-1
1459-39-8
General procedure for the synthesis of cycloheptanamide from cycloheptanecarbonitrile: To a solution of nitromethane (1 mL) containing cycloheptanecarbonitrile (1.00 g, 8.12 mmol) was added sequentially, at room temperature, water (1 mL), DBU (2.47 g, 16.2 mmol), copper(I) iodide (309 mg, 1.62 mmol), and caesium carbonate(I) (1.32 g, 4.06 mmol). The reaction mixture was heated to 90°C and maintained for 8 hours. After completion of the reaction, the mixture was poured into water (50 mL) and the organic layer was separated. The aqueous layer was extracted with chloroform (CHCl3), the organic layers were combined and dried with anhydrous magnesium sulfate (MgSO4). The solvent was removed by concentration under reduced pressure and the resulting brown solid was washed with hexane to give the final cycloheptanamide (499 mg, 44% yield) with a melting point of 192-194 °C.
References
[1] Synlett, 2018, vol. 29, # 15, p. 2061 - 2065
cycloheptanecarboxamide Preparation Products And Raw materials
Raw materials
Preparation Products
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