ChemicalBook > CAS DataBase List > 3-IODO-4-METHOXY-PYRIDINE
3-IODO-4-METHOXY-PYRIDINE
- Product Name
- 3-IODO-4-METHOXY-PYRIDINE
- CAS No.
- 89640-55-1
- Chemical Name
- 3-IODO-4-METHOXY-PYRIDINE
- Synonyms
- 3-IODO-4-METHOXY-PYRIDINE;Pyridine, 3-iodo-4-methoxy-
- CBNumber
- CB6127420
- Molecular Formula
- C6H6INO
- Formula Weight
- 235.02
- MOL File
- 89640-55-1.mol
More
Less
3-IODO-4-METHOXY-PYRIDINE Property
- Melting point:
- 78 °C(Solv: ligroine (8032-32-4))
- Boiling point:
- 271.2±25.0 °C(Predicted)
- Density
- 1.825±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- pka
- 4.52±0.18(Predicted)
- form
- solid
- Appearance
- White to yellow Solid
- InChI
- InChI=1S/C6H6INO/c1-9-6-2-3-8-4-5(6)7/h2-4H,1H3
- InChIKey
- WZAPSURIRLYQEJ-UHFFFAOYSA-N
- SMILES
- C1=NC=CC(OC)=C1I
More
Less
More
Less
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
More
Less
N-Bromosuccinimide Price
Sigma-Aldrich
- Product number
- ADE000651
- Product name
- 3-Iodo-4-methoxypyridine
- Purity
- Aldrich
- Packaging
- 1g
- Price
- $817
- Updated
- 2025/07/31
American Custom Chemicals Corporation
- Product number
- HCH0030628
- Product name
- PYRIDINE, 3-IODO-4-METHOXY-
- Purity
- 95.00%
- Packaging
- 250MG
- Price
- $952.88
- Updated
- 2021/12/16
AK Scientific
- Product number
- J52664
- Product name
- 3-Iodo-4-methoxypyridine
- Packaging
- 25g
- Price
- $1050
- Updated
- 2021/12/16
AK Scientific
- Product number
- 4852AC
- Product name
- 3-Iodo-4-methoxypyridine
- Packaging
- 10g
- Price
- $721
- Updated
- 2021/12/16
Matrix Scientific
- Product number
- 048337
- Product name
- 3-Iodo-4-methoxypyridine
- Packaging
- 1mg
- Price
- $195
- Updated
- 2021/12/16
More
Less
3-IODO-4-METHOXY-PYRIDINE Chemical Properties,Usage,Production
Synthesis
620-08-6
89640-55-1
The general procedure for the synthesis of 3-iodo-4-methoxypyridine from 4-methoxypyridine was as follows: n-butyllithium (ca. 1.6 M hexane solution, 1.5 mmol) was sequentially added to a stirred solution of 2,2,6,6-tetramethylpiperidine (0.25 mL, 1.5 mmol) in tetrahydrofuran (THF, 2-3 mL) at 0 °C. After 5 min, n-butyllithium (ca. 1.6 M hexane solution, 1.5 mmol) was added. ZnCl2TMEDA complex (0.13 g, 0.50 mmol). The reaction mixture was continued to be stirred at 0 °C for 15 min and then 4-methoxypyridine (1.0 mmol) was added at 0-10 °C. After the reaction mixture was stirred for 2 h at room temperature, a THF (4 mL) solution of iodine (I2, 0.38 g, 1.5 mmol) was added. After the mixture was stirred overnight, the reaction was quenched by the addition of saturated aqueous sodium thiosulfate (Na2S2O3) solution (4 mL) and extracted with ethyl acetate (AcOEt, 320 mL). The organic layers were combined, dried with anhydrous magnesium sulfate (MgSO4), filtered and concentrated under reduced pressure. Finally, the target product, 3-iodo-4-methoxypyridine, was purified by silica gel column chromatography (eluent given in the product specification).
References
[1] Tetrahedron, 2016, vol. 72, # 17, p. 2196 - 2205
[2] Tetrahedron, 1993, vol. 49, # 37, p. 8373 - 8380
[3] Tetrahedron Letters, 2011, vol. 52, # 36, p. 4590 - 4594
[4] Chemical Communications, 2014, vol. 50, # 85, p. 12859 - 12862
[5] Chemistry - A European Journal, 2013, vol. 19, # 24, p. 7944 - 7960
3-IODO-4-METHOXY-PYRIDINE Preparation Products And Raw materials
Raw materials
Preparation Products
More
Less
3-IODO-4-METHOXY-PYRIDINE Suppliers
- Tel
- 微信 17321281695 18019252918
- Fax
- 17321281695
- sale@amkchem.com
- Country
- China
- ProdList
- 15136
- Advantage
- 55
- Tel
- 18210857532; 18210857532
- Fax
- 86-10-82849933
- jkinfo@jkchemical.com
- Country
- China
- ProdList
- 96815
- Advantage
- 76
- Tel
- 86-027-67849912
- Fax
- 86-027-87531808
- sales@chemwish.com
- Country
- China
- ProdList
- 35896
- Advantage
- 56
- Tel
- 4009903999 13355009207
- Fax
- 0539-6365991
- 3007715519@qq.com
- Country
- China
- ProdList
- 18729
- Advantage
- 57
- Tel
- 18652989687
- Fax
- +86-25-52131256
- sales@norris-pharm.com
- Country
- China
- ProdList
- 8878
- Advantage
- 55
- Tel
- +86-28-85122536 85324413
- Fax
- +86-28-85326443
- market@astatech.cn
- Country
- China
- ProdList
- 8026
- Advantage
- 55
- Tel
- 21-33526724 18930996265
- Fax
- 37023730
- info@carlowchem.com
- Country
- China
- ProdList
- 1922
- Advantage
- 58
- Tel
- 029-86115547 17791676824
- Fax
- 02151602123
- sales@cochemical.com
- Country
- China
- ProdList
- 3014
- Advantage
- 58
- Tel
- 400-164-7117 13681763483
- Fax
- +86-21-61629029
- product02@bidepharm.com
- Country
- China
- ProdList
- 39966
- Advantage
- 60
- Tel
- 13120367189
- Fax
- 021-50315529
- mychess007@163.com
- Country
- China
- ProdList
- 1994
- Advantage
- 55
- Tel
- 18905173768
- Fax
- 025-83263139
- 52513593@qq.com
- Country
- China
- ProdList
- 2331
- Advantage
- 50
- Tel
- 021-64340559 13651849907;
- Fax
- 021- 64345308
- xinyu_shi@jwypharmlab.com.cn
- Country
- China
- ProdList
- 12000
- Advantage
- 58
- Tel
- 021-34979681; 17701870669
- Fax
- 021-34979681
- 41513101@qq.com
- Country
- China
- ProdList
- 1785
- Advantage
- 55
- Tel
- 526763801 13301653310
- Fax
- +86-21-51619052
- 526763801@qq.com
- Country
- China
- ProdList
- 9287
- Advantage
- 55
- Tel
- 021-61312847; 18021002903
- Fax
- QQ:3008007432
- 3008007409@qq.com
- Country
- China
- ProdList
- 71826
- Advantage
- 60
- Tel
- 028-83379370 13880556291
- Fax
- 028-87747383
- tcy@tcypharm.com
- Country
- China
- ProdList
- 7218
- Advantage
- 58
- Tel
- 571-89925085
- Fax
- 0086-571-89925065
- sales@amadischem.com
- Country
- China
- ProdList
- 131957
- Advantage
- 58
- Tel
- 025-87782433 18021532344
- Fax
- 025-87782433
- 1345332203@qq.com
- Country
- China
- ProdList
- 4135
- Advantage
- 58
- Tel
- 400-711-5280 86-571-81025280
- Fax
- 86-571-85806285
- sales@molcore.com
- Country
- China
- ProdList
- 9967
- Advantage
- 58
- Tel
- 025-66061636 18013972705
- Fax
- (3)02557626880
- qqyang@aikonchem.com
- Country
- China
- ProdList
- 15814
- Advantage
- 58
- Tel
- 15026866316
- 180642609@qq.com
- Country
- China
- ProdList
- 4967
- Advantage
- 58
- Tel
- 021-61469567 13482353728
- Fax
- 021-61161605
- sales@fdc-chemical.com
- Country
- China
- ProdList
- 9722
- Advantage
- 58
- Tel
- 4009004166/18616739031 18616739031
- 3007523370@qq.com
- Country
- China
- ProdList
- 52687
- Advantage
- 58
- Tel
- 021-58581007 18019463053
- Fax
- 021-50966098
- sales@coolpharm.com
- Country
- China
- ProdList
- 12878
- Advantage
- 58
- Tel
- 025-58867862 18751812725
- Fax
- 02558867862
- sales@ace-pharm.com
- Country
- China
- ProdList
- 1985
- Advantage
- 58
- Tel
- zhiqianbio@126.com
- Country
- China
- ProdList
- 19778
- Advantage
- 58
- Tel
- +86-0571-88938639 +8617705817739
- Fax
- +86-571-88938652，+86-571- 88492614
- info@dycnchem.com
- Country
- China
- ProdList
- 52846
- Advantage
- 58
- Tel
- 15221000252
- 278450236@qq.com
- Country
- China
- ProdList
- 203
- Advantage
- 58
- Tel
- 18151111370
- 1046215251@qq.com
- Country
- China
- ProdList
- 5999
- Advantage
- 58
- Tel
- +86-0371-86658258 +8613203830695
- Fax
- 0086-371-86658258
- factory@coreychem.com
- Country
- China
- ProdList
- 29798
- Advantage
- 58
- Tel
- 0519-68985668 13685222090
- Fax
- qq735434464
- sales@kechem.cn
- Country
- China
- ProdList
- 26028
- Advantage
- 58
- Tel
- 15221000252
- 278450236@qq.com
- Country
- China
- ProdList
- 370
- Advantage
- 58
- Tel
- 021-51816796-820 13611835272
- Fax
- 021-5161 3951
- sales2@sunwaypharm.com
- Country
- China
- ProdList
- 44119
- Advantage
- 58
- Tel
- 029-81124267 17392282731
- Fax
- 029-88380327
- 1073@dideu.com
- Country
- China
- ProdList
- 9992
- Advantage
- 58
- Tel
- 400-8210725 4008210725
- malulu@leyan.com
- Country
- China
- ProdList
- 40000
- Advantage
- 58
- Tel
- 400-6005915
- sales@picasso-e.com
- Country
- China
- ProdList
- 39653
- Advantage
- 58
- Tel
- +86(21)5895 0110 19945755304
- sales@chemany.com
- Country
- China
- ProdList
- 9984
- Advantage
- 58
- Tel
- 13356901049
- mark@sklnchem.cn
- Country
- China
- ProdList
- 7997
- Advantage
- 58
- Tel
- 19171595131
- 3168392538@qq.com
- Country
- China
- ProdList
- 490
- Advantage
- 58
- Tel
- 18455579438
- Country
- China
- ProdList
- 16684
- Advantage
- 58
- Tel
- 010-50973130 17801761073
- Gsiyu@solarbio.com
- Country
- China
- ProdList
- 50464
- Advantage
- 58
- Tel
- 021-57520305 13795461237
- zhuruyan@jskchem.com
- Country
- China
- ProdList
- 49234
- Advantage
- 58
- Tel
- 4000255188
- marketing@pharmablock.com
- Country
- China
- ProdList
- 9126
- Advantage
- 58
- Tel
- 400-0628126 18736790110;
- sales-team@aobchem.com.cn
- Country
- China
- ProdList
- 50000
- Advantage
- 58
- Tel
- 021-54306202 18917919676
- info@hanhongsci.com
- Country
- China
- ProdList
- 29995
- Advantage
- 58
- Tel
- 021-50795510 4000665055
- syeu@accelachem.com
- Country
- China
- ProdList
- 11015
- Advantage
- 58
- Tel
- 0635-893290 18663513896;
- 28698871@qq.com
- Country
- China
- ProdList
- 8022
- Advantage
- 58
- Tel
- 029-15596886083 15596886083
- 739383595@qq.com
- Country
- China
- ProdList
- 4073
- Advantage
- 58
- Tel
- 400-6206333 13167063860
- anhua.mao@aladdin-e.com
- Country
- China
- ProdList
- 48457
- Advantage
- 58
- Tel
- 17717618050
- zllg@gh-reagent.com
- Country
- China
- ProdList
- 10420
- Advantage
- 58
More
Less
View Lastest Price from 3-IODO-4-METHOXY-PYRIDINE manufacturers
Career Henan Chemical Co
- Product
- 3-Iodo-4-methoxypyridine 89640-55-1
- Price
- US $9.80/KG
- Min. Order
- 1KG
- Purity
- ≥98%
- Supply Ability
- 20 tons
- Release date
- 2020-01-02
89640-55-1, 3-IODO-4-METHOXY-PYRIDINERelated Search:
4-ETHOXY-3,5-DIIODOPYRIDINE
TERT-BUTYL5-IODO-4-METHOXYPYRIDIN-2-YLCARBAMATE
N-(3-IODO-4-METHOXY-PYRIDIN-2-YL)-2,2-DIMETHYL-PROPIONAMIDE
3,5-diiodo-4-methoxypyridine
3-IODO-4-METHOXY-PYRIDIN-2-YLAMINE
4-(2-HYDROXYETHOXY)-3-IODO PYRIDINE
3-IODO-4-METHOXY-PYRIDINE