ChemicalBook > CAS DataBase List > (4-BENZOYL-PHENOXY)-ACETIC ACID

(4-BENZOYL-PHENOXY)-ACETIC ACID

Product Name: (4-BENZOYL-PHENOXY)-ACETIC ACID
CAS No.: 6322-83-4
Chemical Name: (4-BENZOYL-PHENOXY)-ACETIC ACID
Synonyms: 105380;2-(4-benzoylphenoxy)acetic acid;Acetic acid, (4-benzoylphenoxy)-;Acetic acid, 2-(4-benzoylphenoxy)-
CBNumber: CB61491229
Molecular Formula: C15H12O4
Formula Weight: 256.25
MOL File: 6322-83-4.mol

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(4-BENZOYL-PHENOXY)-ACETIC ACID Property

storage temp.: Sealed in dry,Room Temperature
Appearance: White to off-white Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B208653
Product name: (4-Benzoyl-phenoxy)-aceticacid
Packaging: 25mg
Price: $45
Updated: 2021/12/16

TRC

Product number: B208653
Product name: (4-Benzoyl-phenoxy)-aceticacid
Packaging: 100mg
Price: $65
Updated: 2021/12/16

TRC

Product number: B208653
Product name: (4-Benzoyl-phenoxy)-aceticacid
Packaging: 250mg
Price: $75
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0015489
Product name: (4-BENZOYL-PHENOXY)-ACETIC ACID
Purity: 95.00%
Packaging: 1G
Price: $794.34
Updated: 2021/12/16

Matrix Scientific

Product number: 120853
Product name: 2-(4-Benzoylphenoxy)aceticacid
Purity: 97%
Packaging: 5g
Price: $1072
Updated: 2021/12/16

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(4-BENZOYL-PHENOXY)-ACETIC ACID Chemical Properties,Usage,Production

Synthesis

51848-56-7

6322-83-4

General procedure for the synthesis of (4-benzoylphenoxy)-acetic acid from ethyl 2-(4-benzoylphenoxy)acetate: 1N NaOH solution (3.9 mmol) was added to an ethanol (20 mL) solution of ethyl 2-(4-benzoylphenoxy)acetate (3.0 mmol) and the reaction mixture was stirred for 10-15 h at room temperature. Upon completion of the reaction, the solvent was removed by distillation under reduced pressure and the residue was dissolved in water (20 mL) and acidified with concentrated HCl at 0 °C. Subsequently, the aqueous layer was extracted with dichloromethane (3 x 20 mL), the organic layers were combined and dried with anhydrous Na2SO4. After drying, the organic layer was concentrated under reduced pressure to give the crude product. Finally, the crude product was purified by crystallization from cyclohexane or chloroform to afford the target compound (4-benzoylphenoxy)-acetic acid in good yield.

References

[1] Medicinal Chemistry, 2014, vol. 10, # 1, p. 59 - 65
[2] Anales de la Real Sociedad Espanola de Fisica y Quimica, vol. 24, p. 88
[3] Chem. Zentralbl., 1926, vol. 97, # II, p. 21
[4] Tetrahedron Letters, 2004, vol. 45, # 10, p. 2239 - 2241
[5] Journal of Peptide Science, 2010, vol. 16, # 10, p. 551 - 557

(4-BENZOYL-PHENOXY)-ACETIC ACID Preparation Products And Raw materials

Raw materials

Preparation Products

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Acetic acid, (4-benzoylphenoxy)-

2-(4-benzoylphenoxy)acetic acid

105380

Acetic acid, 2-(4-benzoylphenoxy)-

6322-83-4