2-ISOPROPYL-4-NITROPHENOL

Product Name: 2-ISOPROPYL-4-NITROPHENOL
CAS No.: 60515-72-2
Chemical Name: 2-ISOPROPYL-4-NITROPHENOL
Synonyms: 4-nitro-2-isopropylphenol;2-ISOPROPYL-4-NITROPHENOL;4-nitro-2-propan-2-ylphenol;Phenol, 2-(1-methylethyl)-4-nitro-
CBNumber: CB61507980
Molecular Formula: C9H11NO3
Formula Weight: 181.19
MOL File: 60515-72-2.mol

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2-ISOPROPYL-4-NITROPHENOL Property

Melting point:: 86 °C
Boiling point:: 294.3±33.0 °C(Predicted)
Density: 1.209±0.06 g/cm3(Predicted)
storage temp.: Inert atmosphere,Room Temperature
pka: 7.62±0.22(Predicted)
Appearance: Brown to black Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: I872808
Product name: 2-Isopropyl-4-nitrophenol
Packaging: 2mg
Price: $60
Updated: 2021/12/16

AK Scientific

Product number: 9023AB
Product name: 2-Isopropyl-4-nitrophenol
Packaging: 5g
Price: $300
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0098205
Product name: 2-ISOPROPYL-4-NITROPHENOL
Purity: 95.00%
Packaging: 5MG
Price: $503.11
Updated: 2021/12/16

Crysdot

Product number: CD12056519
Product name: 2-Isopropyl-4-nitrophenol
Purity: 95+%
Packaging: 25g
Price: $534
Updated: 2021/12/16

Alichem

Product number: 60515722
Product name: 2-Isopropyl-4-nitrophenol
Packaging: 25g
Price: $555.36
Updated: 2021/12/16

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2-ISOPROPYL-4-NITROPHENOL Chemical Properties,Usage,Production

Synthesis

88-69-7

141-78-6

60515-72-2

To a solution of acetic acid (30 mL) containing 2-isopropylphenol (4.1 mL), 69% nitric acid (4 mL) was slowly added under ice bath conditions, keeping the reaction temperature constant with constant stirring for 30 minutes. Upon completion of the reaction, the reaction was quenched by the addition of ice water and subsequently extracted with tert-butyl methyl ether. The organic phase was washed sequentially with water and saturated saline, dried over anhydrous sodium sulfate and filtered. The filtrate was concentrated under reduced pressure to obtain the crude product. The crude product was purified by silica gel column chromatography, and the eluent was a mixed solvent of hexane/ethyl acetate in the ratio of 4:1, v/v. The target compound 2-isopropyl-4-nitrophenol (2.66 g, 49% yield) was finally obtained as a yellow solid. The structure of the product was confirmed by 1H NMR (400 MHz, CDCl3): δ 1.3 (6H, d, J = 7.0 Hz), 3.25 (1H, m), 6.82 (1H, d, J = 9.0 Hz), 8.01 (1H, dd, J = 9.0, 2.5 Hz), 8.13 (1H, d, J = 2.5 Hz).

References

[1] Patent: US6555556, 2003, B1

2-ISOPROPYL-4-NITROPHENOL Preparation Products And Raw materials

Raw materials

Preparation Products

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2-ISOPROPYL-4-NITROPHENOL Suppliers

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2-ISOPROPYL-4-NITROPHENOL

4-nitro-2-isopropylphenol

4-nitro-2-propan-2-ylphenol

Phenol, 2-(1-methylethyl)-4-nitro-

60515-72-2