ChemicalBook > CAS DataBase List > 1-BENZYL-3-OXOAZEPANE

1-BENZYL-3-OXOAZEPANE

Product Name
1-BENZYL-3-OXOAZEPANE
CAS No.
146407-32-1
Chemical Name
1-BENZYL-3-OXOAZEPANE
Synonyms
-azepan-3-one;1-Benzyl-3-azepanone;1-BENZYL-3-OXOAZEPANE;Hexahydro-1-(phenylmethyl)-3H-azepin-3-one;3H-Azepin-3-one, hexahydro-1-(phenylmethyl)-
CBNumber
CB61519169
Molecular Formula
C13H17NO
Formula Weight
203.28
MOL File
146407-32-1.mol
More
Less

1-BENZYL-3-OXOAZEPANE Property

Boiling point:
312.6±35.0 °C(Predicted)
Density 
1.069±0.06 g/cm3(Predicted)
storage temp. 
2-8°C
pka
6.50±0.20(Predicted)
Appearance
Colorless to light yellow Liquid
More
Less

Safety

HS Code 
2933998090
More
Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

More
Less

N-Bromosuccinimide Price

TRC
Product number
B230805
Product name
1-Benzyl-azepan-3-one
Packaging
50mg
Price
$75
Updated
2021/12/16
Matrix Scientific
Product number
101755
Product name
1-Benzyl-azepan-3-one
Purity
95%
Packaging
500mg
Price
$262
Updated
2021/12/16
AK Scientific
Product number
4461AD
Product name
1-Benzyl-azepan-3-one
Packaging
1g
Price
$404
Updated
2021/12/16
Matrix Scientific
Product number
101755
Product name
1-Benzyl-azepan-3-one
Purity
95%
Packaging
1g
Price
$420
Updated
2021/12/16
SynQuest Laboratories
Product number
4H17-1-3U
Product name
1-Benzyl-azepan-3-one
Packaging
1g
Price
$517
Updated
2021/12/16
More
Less

1-BENZYL-3-OXOAZEPANE Chemical Properties,Usage,Production

Synthesis

765940-56-5

146407-32-1

The general procedure for the synthesis of 1-benzyl-azepan-3-one from the compound (CAS: 765940-56-5) is as follows: potassium tert-butoxide (336 mg) was suspended in toluene (2.5 mL) and heated under reflux conditions for 10 min. Subsequently, 5-(benzyl-ethoxycarbonylmethyl-amino)-pentanoic acid (695 mg) dissolved in toluene (1 mL) was slowly added to the suspension, and the addition process lasted for 5 hours, after which the reaction was continued at reflux. Upon completion of the reaction, it was cooled to room temperature and acidified by the addition of 25% hydrochloric acid (1 mL). The organic phase was separated and washed with 25% hydrochloric acid (4 x 1 mL). The aqueous hydrochloric acid phase was combined and heated under reflux conditions for 5 hours. After cooling to room temperature, the pH was adjusted to 11 with 2N sodium hydroxide solution to make the solution basic, followed by extraction with ethyl acetate. The organic phases were combined, dried with sodium sulfate and the solvent was evaporated. The resulting residue was purified by silica gel column chromatography (eluent: ethyl acetate/heptane, 1:5) to afford the target product 1-benzyl-azepan-3-one (197 mg) in 45% yield. Ref: Bull. Chem. Soc. Jpn. 1956, 29, 631-632; DE2206385.

References

[1] Patent: WO2004/83218, 2004, A1. Location in patent: Page 58

1-BENZYL-3-OXOAZEPANE Preparation Products And Raw materials

Raw materials

Preparation Products

More
Less

1-BENZYL-3-OXOAZEPANE Suppliers

China 44 Germany 1 India 1 United Kingdom 1 United States 8 Global 55
Tetranov Biopharm
Tel
13526569071
Email
sales@leadmedpharm.com
Country
China
ProdList
7892
Advantage
64
Aemon Chemical
Tel
0086-755-86198205
Email
acinfo@aemonchem.com
Country
China
ProdList
1931
Advantage
57
Chem-Stone Co.,Ltd.
Tel
020-82185713,82185709 13418171485
Fax
020-82185696
Email
sales@chem-stone.com
Country
China
ProdList
744
Advantage
56
Mashilabs (Shanghai) Co.,Ltd.
Tel
19916721580
Fax
QQ：3154870176
Email
mafarm@126.com
Country
China
ProdList
4542
Advantage
58
ShangHai AmK Pharmaceutical Technology Co., Ltd.
Tel
微信 17321281695 18019252918
Fax
17321281695
Email
sale@amkchem.com
Country
China
ProdList
15136
Advantage
55
JW & Y Pharmlab Co., Ltd.
Tel
021-64340559 13651849907;
Fax
021- 64345308
Email
xinyu_shi@jwypharmlab.com.cn
Country
China
ProdList
12000
Advantage
58
Suzhou Crst Pharmatech Co., Ltd.
Tel
0512-62910395 17751098781
Fax
0512-62910396
Email
sales@crstpharma.com
Country
China
ProdList
499
Advantage
58
Amadis Chemical Company Limited
Tel
571-89925085
Fax
0086-571-89925065
Email
sales@amadischem.com
Country
China
ProdList
131957
Advantage
58
Capot Chemical Co.,Ltd.
Tel
+86-（0）57185586718; +8613336195806
Fax
+86-571-85864795
Email
sales@capot.com
Country
China
ProdList
29735
Advantage
60
Aikon International Limited
Tel
025-66061636 18013972705
Fax
(3)02557626880
Email
qqyang@aikonchem.com
Country
China
ProdList
15814
Advantage
58
Rhawn Reagent
Tel
400-400-1332688 18019345275
Fax
400-133-2688
Email
amy@rhawn.cn
Country
China
ProdList
14948
Advantage
58
Nanjing SynTitan Pharmaceutical Co., Ltd.
Tel
025-57027686 17372956142
Fax
025-57027686
Email
li_lan@syntitan.com
Country
China
ProdList
9998
Advantage
58
Shanghai Vigor Biotechnology Co., Ltd.
Tel
021-18017654 18017654809
Fax
2271705492
Email
sales@vigorchem.cn
Country
China
ProdList
958
Advantage
58
Cool Pharm, Ltd
Tel
021-58581007 18019463053
Fax
021-50966098
Email
sales@coolpharm.com
Country
China
ProdList
12878
Advantage
58
Shanghai zhigan biotechnology co., LTD
Tel
Email
zhiqianbio@126.com
Country
China
ProdList
19778
Advantage
58
Suzhou Rovathin Foreign Trade Co.,Ltd
Tel
0512-65816829 18662214788
Fax
0512-65816829
Email
info@rovathin.com.cn
Country
China
ProdList
9987
Advantage
58
Hubei Ipure Biology Co., Ltd
Tel
+8613367258412
Fax
18062427325
Email
ada@ipurechemical.com
Country
China
ProdList
10237
Advantage
58
Dayang Chem (Hangzhou) Co.,Ltd.
Tel
+86-0571-88938639 +8617705817739
Fax
+86-571-88938652，+86-571- 88492614
Email
info@dycnchem.com
Country
China
ProdList
52846
Advantage
58
Hefei Hirisun Pharmatech Co., Ltd
Tel
+8615056975894
Fax
86-0551-62678551
Email
shawn@hirisunpharm.com
Country
CHINA
ProdList
9911
Advantage
58
Accela ChemBio Co.,Ltd.
Tel
021-50795510 4000665055
Email
sales@accelachem.com
Country
China
ProdList
10467
Advantage
58
career henan chemical co
Tel
+86-0371-86658258 +8613203830695
Fax
0086-371-86658258
Email
factory@coreychem.com
Country
China
ProdList
29798
Advantage
58
Antai Fine Chemical Technology Co.,Limited
Tel
18503026267
Email
info@antaichem.com
Country
CHINA
ProdList
9636
Advantage
58
Energy Chemical
Tel
021-58432009 400-005-6266
Fax
021-58436166
Email
marketing1@energy-chemical.com
Country
China
ProdList
44894
Advantage
58
Zhengzhou convergence chemical co., LTD
Tel
0371-0371-55153829 18003835034
Email
2853979819@qq.com
Country
China
ProdList
9998
Advantage
58
Shanghai Aizikang Pharmaceutical Research Co., Ltd
Tel
18721109360
Email
306685371@qq.com
Country
China
ProdList
1944
Advantage
58
Shanghai Haohong Pharmaceutical Co., Ltd.
Tel
400-8210725 4008210725
Email
malulu@leyan.com
Country
China
ProdList
40000
Advantage
58
Bide Pharmatech Ltd.
Tel
400-1647117 13681763483
Email
product02@bidepharm.com
Country
China
ProdList
59936
Advantage
58
Bide Pharmatech Ltd.
Tel
400-6005915
Email
sales@picasso-e.com
Country
China
ProdList
39653
Advantage
58
Beijing Solarbio Science & Tecnology Co., Ltd.
Tel
010-50973130 17801761073
Email
Gsiyu@solarbio.com
Country
China
ProdList
50751
Advantage
58
Shanghai Jieshikai Biotechnology Co. , Ltd.
Tel
021-57520305 13795461237
Email
zhuruyan@jskchem.com
Country
China
ProdList
49234
Advantage
58
Shanghai Zunlijia Life Technology Co., Ltd
Tel
021-34045219 13062664914
Email
huji@zunlijia.com
Country
China
ProdList
10027
Advantage
58
Pushan Industry (Shaanxi) Co., Ltd
Tel
029-81310890 18165209495
Email
2929288192@qq.com
Country
China
ProdList
9729
Advantage
58
Santa Cruz Biotechnology Inc
Tel
021-60936350
Email
scbt@scbt.com
Country
China
ProdList
6594
Advantage
58
Changzhou AniKare Pharmatech Co., Ltd.
Tel
+86-0519-8359-8696 +8618018249389
Email
sales@anikare.com
Country
China
ProdList
9941
Advantage
58
Wuhan Konberd Biotech Co., Ltd
Tel
+undefined18986093962
Email
admin@konberdbio.com
Country
China
ProdList
1379
Advantage
58
GIHI CHEMICALS CO.,LIMITED
Tel
+8618058761490
Email
info@gihichemicals.com
Country
China
ProdList
49934
Advantage
58
PT CHEM GROUP LIMITED
Tel
+86-85511178;
Email
peter68@ptchemgroup.com
Country
China
ProdList
35425
Advantage
58
Nanjing Doge Biomedical Technology Co., Ltd
Tel
+86-25-58227606 +86-15305155328
Email
sales@dogechemical.com
Country
China
ProdList
4128
Advantage
58
Shanghai Sunway Pharmaceutical Technology Co., Ltd
Tel
--
Fax
--
Email
sales@sunwaypharm.com
Country
China
ProdList
6536
Advantage
58
Guangzhou Weike Biotechnology Co., Ltd.
Tel
15902098758
Country
CHINA
ProdList
133
Advantage
58
Guangzhou Aoz Biotechnology Co., Ltd.
Tel
18022383332
Country
CHINA
ProdList
0
Advantage
58
Absin Bioscience Inc.
Tel
--
Fax
--
Email
chenjw@absin.cn
Country
CHINA
ProdList
6208
Advantage
58
Shanghai Hao Zhun Biological Technology Co., Ltd.
Tel
--
Fax
--
Email
info@zzsrm.com
Country
CHINA
ProdList
6650
Advantage
58
Wuhan Konberd Biotech Co., Ltd.
Tel
--
Fax
--
Email
admin@konberdbio.com
Country
China
ProdList
1310
Advantage
50
More
Less

View Lastest Price from 1-BENZYL-3-OXOAZEPANE manufacturers

Zhuozhou Wenxi import and Export Co., Ltd
Product
1-Benzyl-3-oxoazepane 146407-32-1
Price
US $15.00-10.00/KG
Min. Order
1KG
Purity
99%+ HPLC
Supply Ability
Monthly supply of 1 ton
Release date
2021-06-27
Career Henan Chemical Co
Product
1-BENZYL-3-OXOAZEPANE 146407-32-1
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
100KG
Release date
2019-12-20

146407-32-1, 1-BENZYL-3-OXOAZEPANERelated Search:

ETHANE 1-BENZYL-3-OXOAZEPANE

  • 1-BENZYL-3-OXOAZEPANE
  • 1-Benzyl-3-azepanone
  • Hexahydro-1-(phenylmethyl)-3H-azepin-3-one
  • 3H-Azepin-3-one, hexahydro-1-(phenylmethyl)-
  • -azepan-3-one
  • 146407-32-1
  • Morpholines/Thiomorpholines ,Isoxazoles ,Indazoles