methyl 3-amino-5-chlorobenzoate

Product Name: methyl 3-amino-5-chlorobenzoate
CAS No.: 21961-31-9
Chemical Name: methyl 3-amino-5-chlorobenzoate
Synonyms: methyl 3-amino-5-chlorobenzoate;Methyl3-amino-5-chlorobenzoate98%;Methyl 3-amino-5-chlorobenzoate 98%;3-AMINO-5-CHLORO-BENZOIC ACID METHYL ESTER;Benzoic acid, 3-aMino-5-chloro-, Methyl ester
CBNumber: CB61561289
Molecular Formula: C8H8ClNO2
Formula Weight: 185.61
MOL File: 21961-31-9.mol

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methyl 3-amino-5-chlorobenzoate Property

Boiling point:: 329.4±22.0 °C(Predicted)
Density: 1.311±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
pka: 2.39±0.10(Predicted)
Appearance: White to yellow Solid

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Safety

HS Code: 2916399090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: M331700
Product name: Methyl3-Amino-5-chlorobenzoate
Packaging: 50mg
Price: $45
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H58-5-7E
Product name: Methyl 3-amino-5-chlorobenzoate
Purity: 98%
Packaging: 5G
Price: $576
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0044086
Product name: METHYL 3-AMINO-5-CHLOROBENZOATE
Purity: 95.00%
Packaging: 1G
Price: $925.31
Updated: 2021/12/16

AK Scientific

Product number: X6549
Product name: Methyl3-amino-5-chlorobenzoate
Packaging: 1g
Price: $124
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H58-5-7E
Product name: Methyl 3-amino-5-chlorobenzoate
Purity: 98%
Packaging: 1g
Price: $176
Updated: 2021/12/16

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methyl 3-amino-5-chlorobenzoate Chemical Properties,Usage,Production

Synthesis

36138-28-0

21961-31-9

Step 2: Synthesis of methyl 3-amino-5-chlorobenzoate A dioxane solution (0.13 M) of methyl 3-chloro-5-nitrobenzoate (from Step 1) was placed in a reaction flask and SnCl2 (3.9 equiv) was added. The reaction mixture was stirred at 70 °C for 2 hours. After completion of the reaction, it was cooled to room temperature and EtOAc and saturated aqueous NaHCO3 solution was added. The reaction mixture was filtered to remove the precipitate formed. The aqueous phase was separated and extracted with EtOAc. All organic layers were combined and dried with anhydrous Na2SO4. Evaporation of the solvent under reduced pressure afforded the title compound methyl 3-amino-5-chlorobenzoate in 88% yield as a yellow solid. Mass spectrum (ES+) m/z 186,188 (M+H)+.

References

[1] Patent: WO2007/28789, 2007, A1. Location in patent: Page/Page column 35
[2] Patent: US2010/261687, 2010, A1. Location in patent: Page/Page column 60

methyl 3-amino-5-chlorobenzoate Preparation Products And Raw materials

Raw materials

Preparation Products

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methyl 3-amino-5-chlorobenzoate Suppliers

China 51 India 3 United Kingdom 1 United States 10 Global 65

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View Lastest Price from methyl 3-amino-5-chlorobenzoate manufacturers

Career Henan Chemical Co

Product: methyl 3-amino-5-chlorobenzoate 21961-31-9
Price: US $0.01/KG
Min. Order: 1KG
Purity: 98%; 99%
Supply Ability: 500g;1kg； 25kg
Release date: 2020-01-09

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methyl 3-amino-5-chlorobenzoate

Benzoic acid, 3-aMino-5-chloro-, Methyl ester

Methyl3-amino-5-chlorobenzoate98%

3-AMINO-5-CHLORO-BENZOIC ACID METHYL ESTER

Methyl 3-amino-5-chlorobenzoate 98%

21961-31-9