ChemicalBook > CAS DataBase List > 5-Bromo-1,3-difluoro-2-nitrobenzene

5-Bromo-1,3-difluoro-2-nitrobenzene

Product Name
5-Bromo-1,3-difluoro-2-nitrobenzene
CAS No.
147808-42-2
Chemical Name
5-Bromo-1,3-difluoro-2-nitrobenzene
Synonyms
Vandetanib Impurity 12;4-BroMo-2,6-difluoronitrobenzene;1-Bromo-3,5-difluoro-4-nitrobenzene;5-bromo-1,3-difluoro-2-nitrobenzene;3,5-Difluoro-4-nitrobromobenzene 98%;Benzene, 5-bromo-1,3-difluoro-2-nitro-;5-Bromo-1,3-difluoro-2-nitrobenzene, 4-Bromo-2,6-difluoronitrobenzene
CBNumber
CB61563485
Molecular Formula
C6H2BrF2NO2
Formula Weight
237.99
MOL File
147808-42-2.mol
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5-Bromo-1,3-difluoro-2-nitrobenzene Property

Boiling point:
266 °C
Density 
1.890
Flash point:
114 °C
storage temp. 
2-8°C
form 
powder
color 
Faint yellow to orange
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Safety

HS Code 
2904990090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P260Do not breathe dust/fume/gas/mist/vapours/spray.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TRC
Product number
B690333
Product name
5-Bromo-1,3-difluoro-2-nitrobenzene
Packaging
250mg
Price
$55
Updated
2021/12/16
SynQuest Laboratories
Product number
4654-9-X1
Product name
3,5-Difluoro-4-nitrobromobenzene
Packaging
5G
Price
$56
Updated
2021/12/16
ChemScene
Product number
CS-W009157
Product name
5-Bromo-1,3-difluoro-2-nitrobenzene
Purity
99.94%
Packaging
10g
Price
$72
Updated
2021/12/16
Apolloscientific
Product number
PC57010
Product name
3,5-Difluoro-4-nitrobromobenzene
Purity
98%
Packaging
10g
Price
$74
Updated
2021/12/16
AK Scientific
Product number
J94539
Product name
5-Bromo-1,3-difluoro-2-nitrobenzene
Packaging
10g
Price
$85
Updated
2021/12/16
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5-Bromo-1,3-difluoro-2-nitrobenzene Chemical Properties,Usage,Production

Synthesis

Sodium perborate tetrahydrate (18.5 g, 0.12 mol, 5.0 eq) was suspended in glacial acetic acid (125 mL) and heated to 65 °C. 4-Bromo-2,6-difluoroanilline(5.0 g, 24.0 mmol, 1.0 eq) dissolved in glacial acetic acid (50 mL) was added slowly through a funnel over 4 h. After the addition, the reaction mixture was heated for 3 h additional hours before a second portion of NaBO3·4H2O (6.0 g, 30.0 mmol) was added. Then, the mixture was stirred for 14 h, and a third portion of oxidating agent (9.0 g, 45.0 mmol) was added. 9 h after the third addition full consumption of the starting material was indicated by TLC. After cooling the mixture to room temperature, the formed solid was removed by filtration. The filtrate was poured into ice-cold water (300 mL). The precipitated solid was filtered off and dried to give the product 5-Bromo-1,3-difluoro-2-nitrobenzene as a yellow solid (3.40 g 60percent).

5-Bromo-1,3-difluoro-2-nitrobenzene Preparation Products And Raw materials

Raw materials

Preparation Products

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5-Bromo-1,3-difluoro-2-nitrobenzene Suppliers

Wuxi Kehua Biological Technology Co., Ltd.
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0510-0510-86838766
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2258830676@qq.com
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China
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4546
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DILICHEM
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0519-0519-81238123 18014346496
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shichaojun@126.com
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China
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Shandong Bourne Pharmaceutical Co. , Ltd.
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15865694623
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1825792389@qq.com
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China
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Jia Xing Isenchem Co.,Ltd
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0573-85285100 18627885956
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0573-85285100
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isenchem@163.com
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China
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Accela ChemBio Co.,Ltd.
Tel
021-50795510 4000665055
Fax
021-50795055
Email
sales@accelachem.com
Country
China
ProdList
11655
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Shanghai Harvest Chemical Industrial Co., Ltd.
Tel
21-31038972 15721252604
Fax
+86-21-51385350
Email
ammyzuo@harvest-chem.com
Country
China
ProdList
2540
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Nanjing Chemlin Chemical Co., Ltd
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025-83697070
Fax
+86-25-83453306
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info@chemlin.com.cn
Country
China
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19172
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Shanghai Hanhong Scientific Co.,Ltd.
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021-54306202 13764082696
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info@hanhongsci.com
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China
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Beijing Eternalchem Co,. Ltd.
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010-59484199 18611897322
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sales@eternalchem.com
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China
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Chemsky(shanghai)International Co.,Ltd.
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021-50135380
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shchemsky@sina.com
Country
China
ProdList
32321
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50
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View Lastest Price from 5-Bromo-1,3-difluoro-2-nitrobenzene manufacturers

Shaanxi Dideu Medichem Co. Ltd
Product
5-Bromo-1,3-difluoro-2-nitrobenzene 147808-42-2
Price
US $0.00-0.00/KG
Min. Order
10mg
Purity
99%HPLC
Supply Ability
2000tons
Release date
2020-01-19
Career Henan Chemical Co
Product
5-Bromo-1,3-difluoro-2-nitrobenzene 147808-42-2
Price
US $1.00/KG
Min. Order
1KG
Purity
96%-98%
Supply Ability
1000KGS
Release date
2019-12-18

147808-42-2, 5-Bromo-1,3-difluoro-2-nitrobenzeneRelated Search:


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