Ethyl 2-chloro-6-methylpyridine-4-carboxylate, 97%
- Product Name
- Ethyl 2-chloro-6-methylpyridine-4-carboxylate, 97%
- CAS No.
- 3998-88-7
- Chemical Name
- Ethyl 2-chloro-6-methylpyridine-4-carboxylate, 97%
- Synonyms
- Ethyl 2-chloro-6-methyl-4-pyridinecarboxylate;2-Chloro-6-methylisonicotinic Acid Ethyl Ester;Ethyl 2-chloro-6-methylpyridine-4-carboxylate, 97%;Ethyl 2-chloro-6-methylpyridine-4-carboxylate, 97%;2-Chloro-6-methylpyridine-4-carboxylic acid ethyl ester;4-Pyridinecarboxylic acid, 2-chloro-6-Methyl-, ethyl ester;JR-14076, Ethyl 2-chloro-6-methylpyridine-4-carboxylate, 97%
- CBNumber
- CB61569634
- Molecular Formula
- C9H10ClNO2
- Formula Weight
- 199.63
- MOL File
- 3998-88-7.mol
Ethyl 2-chloro-6-methylpyridine-4-carboxylate, 97% Property
- Melting point:
- 65-67°C
- Boiling point:
- 107°C/1.5mm
- Density
- 1?+-.0.06 g/cm3(Predicted)
- Flash point:
- 107°C/1.5mm
- storage temp.
- Inert atmosphere,Room Temperature
- solubility
- soluble in Methanol
- form
- powder to crystal
- pka
- -0.14±0.10(Predicted)
- color
- White to Almost white
Safety
- HS Code
- 2933399990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P405Store locked up.
N-Bromosuccinimide Price
- Product number
- JRD0891
- Product name
- Ethyl 2-chloro-6-methylpyridine-4-carboxylate
- Packaging
- 1G
- Price
- $107
- Updated
- 2025/07/31
- Product number
- E1262
- Product name
- Ethyl 2-Chloro-6-methylisonicotinate
- Purity
- >98.0%(GC)
- Packaging
- 1g
- Price
- $46
- Updated
- 2025/07/31
- Product number
- E1262
- Product name
- Ethyl 2-Chloro-6-methylisonicotinate
- Purity
- >98.0%(GC)
- Packaging
- 5g
- Price
- $137
- Updated
- 2025/07/31
- Product number
- E903788
- Product name
- Ethyl2-Chloro-6-methylpyridine-4-carboxylate
- Packaging
- 500mg
- Price
- $90
- Updated
- 2021/12/16
- Product number
- OR952499
- Product name
- Ethyl2-chloro-6-methylpyridine-4-carboxylate
- Purity
- 95%
- Packaging
- 1g
- Price
- $105
- Updated
- 2021/12/16
Ethyl 2-chloro-6-methylpyridine-4-carboxylate, 97% Chemical Properties,Usage,Production
Synthesis
25462-85-5
64-17-5
3998-88-7
Step 1: Synthesis of ethyl 2-chloro-6-methylisonicotinate (97). Concentrated sulfuric acid (2 mL) was added dropwise to a stirred solution of 2-chloro-6-methylpyridine-4-carboxylic acid (7.0 g, 40.79 mmol) in ethanol (70 mL) at 0 °C. Subsequently, the reaction mixture was heated to 80 °C and kept for 12 hours. Upon completion of the reaction, the mixture was cooled to room temperature and concentrated under vacuum to remove the solvent. The concentrated residue was diluted with ethyl acetate and washed sequentially with water, sodium bicarbonate solution and saturated aqueous sodium chloride solution. The organic layer was separated, dried over anhydrous sodium sulfate, filtered and concentrated to give ethyl 2-chloro-6-methylisonicotinate (97) (7 g, 86% yield) as a white solid.
References
[1] Patent: US2010/249071, 2010, A1. Location in patent: Page/Page column 63-64
[2] Patent: WO2008/29371, 2008, A1. Location in patent: Page/Page column 41
[3] Patent: WO2009/24905, 2009, A1. Location in patent: Page/Page column 38-39; 49
[4] Patent: US2010/63108, 2010, A1. Location in patent: Page/Page column 16
[5] Patent: US2011/46170, 2011, A1. Location in patent: Page/Page column 17
Ethyl 2-chloro-6-methylpyridine-4-carboxylate, 97% Preparation Products And Raw materials
Raw materials
Preparation Products
Ethyl 2-chloro-6-methylpyridine-4-carboxylate, 97% Suppliers
- Tel
- 320-37350700
- Fax
- +32 (0)37350701
- sales@tcieurope.eu
- Country
- Europe
- ProdList
- 23671
- Advantage
- 75
View Lastest Price from Ethyl 2-chloro-6-methylpyridine-4-carboxylate, 97% manufacturers
- Product
- Ethyl 2-chloro-6-methylpyridine-4-carboxylate 3998-88-7
- Price
- US $0.00-0.00/kg
- Min. Order
- 1kg
- Purity
- 98%
- Supply Ability
- 1Ton
- Release date
- 2022-10-14
- Product
- Ethyl 2-chloro-6-methylpyridine-4-carboxylate, 97% 3998-88-7
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- Customized
- Release date
- 2019-07-03