2-AMINO-N-(2-METHYLPHENYL)BENZAMIDE
- Product Name
- 2-AMINO-N-(2-METHYLPHENYL)BENZAMIDE
- CAS No.
- 4943-85-5
- Chemical Name
- 2-AMINO-N-(2-METHYLPHENYL)BENZAMIDE
- Synonyms
- OTAVA-BB 1133397;2-Amino-benzoesaeure-o-toluidid;N-(2-Aminobenzoyl)-2-methylaniline;2-AMINO-N-(2-METHYLPHENYL)BENZAMIDE;BENZAMIDE, 2-AMINO-N-(2-METHYLPHENYL)-
- CBNumber
- CB6238085
- Molecular Formula
- C14H14N2O
- Formula Weight
- 226.27
- MOL File
- 4943-85-5.mol
2-AMINO-N-(2-METHYLPHENYL)BENZAMIDE Property
- Melting point:
- 104-105 °C
- Boiling point:
- 320.2±35.0 °C(Predicted)
- Density
- 1.210±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- pka
- 13.25±0.70(Predicted)
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- R702153
- Product name
- 2-AMINO-N-(2-METHYLPHENYL)BENZAMIDE
- Purity
- AldrichCPR
- Packaging
- 25MG
- Price
- $30.7
- Updated
- 2025/07/31
- Product number
- 6693AB
- Product name
- 2-Amino-N-(o-tolyl)benzamide
- Packaging
- 1g
- Price
- $10
- Updated
- 2021/12/16
- Product number
- 6693AB
- Product name
- 2-Amino-N-(o-tolyl)benzamide
- Packaging
- 5g
- Price
- $25
- Updated
- 2021/12/16
- Product number
- CS-0038876
- Product name
- 2-Amino-N-(2-methylphenyl)benzamide
- Packaging
- 25g
- Price
- $56
- Updated
- 2021/12/16
- Product number
- 157206
- Product name
- 2-Amino-N-(2-methylphenyl)benzamide
- Packaging
- 0.500g
- Price
- $120
- Updated
- 2021/12/16
2-AMINO-N-(2-METHYLPHENYL)BENZAMIDE Chemical Properties,Usage,Production
Synthesis
2385-25-3
4943-85-5
Nitrobenzene (0.6 mmol) was used as a feedstock and mixed with 5 wt% Pd/C (0.5 mol%, 0.003 mmol), H2O (10 eq, 6.0 mmol), B2(OH)4 (3.3 eq, 2.0 mmol) and CH3CN (1.0 mL) in a 10 mL reaction tube. The reaction mixture was stirred at 50 °C for 24 hours. The reaction progress was monitored by TLC. After completion of the reaction, the mixture was cooled to room temperature. Water (5 mL) was added and extracted with EtOAc (3 x 5 mL). The organic phases were combined, dried with anhydrous Na2SO4, filtered and concentrated under reduced pressure. The residue was purified by silica gel column chromatography to afford the target product 2-amino-N-(o-toluene)benzamide (55 mg, 99% yield).
References
[1] Tetrahedron, 2017, vol. 73, # 27-28, p. 3898 - 3904
[2] Journal of Medicinal Chemistry, 2008, vol. 51, # 8, p. 2400 - 2411
[3] RSC Advances, 2016, vol. 6, # 33, p. 27378 - 27387
[4] Synlett, 2018, vol. 29, # 13, p. 1765 - 1768
[5] Journal of Medicinal Chemistry, 1986, vol. 29, # 8, p. 1534 - 1537
2-AMINO-N-(2-METHYLPHENYL)BENZAMIDE Preparation Products And Raw materials
Raw materials
Preparation Products
2-AMINO-N-(2-METHYLPHENYL)BENZAMIDE Suppliers
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View Lastest Price from 2-AMINO-N-(2-METHYLPHENYL)BENZAMIDE manufacturers
- Product
- N-(2-Aminobenzoyl)-2-methylaniline 4943-85-5
- Price
- US $1.00-2.10/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 20000KG
- Release date
- 2024-08-14
- Product
- 2-AMINO-N-(2-METHYLPHENYL)BENZAMIDE 4943-85-5
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- Customized
- Release date
- 2019-12-20