2-AMINO-5-BROMO-3-METHOXYBENZOIC ACID

Product Name: 2-AMINO-5-BROMO-3-METHOXYBENZOIC ACID
CAS No.: 864293-44-7
Chemical Name: 2-AMINO-5-BROMO-3-METHOXYBENZOIC ACID
Synonyms: 2-AMino-5-broMo-3-Methoxybenzoic;5-Bromo-3-methoxyanthranilic Acid;2-AMINO-5-BROMO-3-METHOXYBENZOIC ACID;Benzoic acid, 2-amino-5-bromo-3-methoxy-;2-Amino-5-bromo-3-(methyloxy)benzoic acid
CBNumber: CB62455891
Molecular Formula: C8H8BrNO3
Formula Weight: 246.06
MOL File: 864293-44-7.mol

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2-AMINO-5-BROMO-3-METHOXYBENZOIC ACID Property

Boiling point:: 356.0±42.0 °C(Predicted)
Density: 1.703±0.06 g/cm3(Predicted)
storage temp.: Keep in dark place,Sealed in dry,Room Temperature
pka: 4.43±0.10(Predicted)
Appearance: Off-white to light yellow Solid
InChI: InChI=1S/C8H8BrNO3/c1-13-6-3-4(9)2-5(7(6)10)8(11)12/h2-3H,10H2,1H3,(H,11,12)
InChIKey: YSBGYQUUOKRQAT-UHFFFAOYSA-N
SMILES: C(O)(=O)C1=CC(Br)=CC(OC)=C1N

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Safety

HS Code: 2916399090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P321Specific treatment (see … on this label).

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

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N-Bromosuccinimide Price

Biosynth Carbosynth

Product number: FA141359
Product name: 2-Amino-5-bromo-3-methoxybenzoic acid
Packaging: 250mg
Price: $165
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FA141359
Product name: 2-Amino-5-bromo-3-methoxybenzoic acid
Packaging: 500mg
Price: $290
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FA141359
Product name: 2-Amino-5-bromo-3-methoxybenzoic acid
Packaging: 1g
Price: $500
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4657-9-10
Product name: 2-Amino-5-bromo-3-methoxybenzoic acid
Packaging: 500mg
Price: $584
Updated: 2021/12/16

AK Scientific

Product number: 3538AC
Product name: 2-Amino-5-bromo-3-methoxybenzoicacid
Packaging: 10g
Price: $655
Updated: 2021/12/16

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2-AMINO-5-BROMO-3-METHOXYBENZOIC ACID Chemical Properties,Usage,Production

Synthesis

3177-80-8

864293-44-7

General procedure for the synthesis of 2-amino-5-bromo-3-methoxybenzoic acid from 2-amino-3-methoxybenzoic acid: 2-amino-3-methoxybenzoic acid (10.0 g, 59.8 mmol, 1.0 eq.) was dissolved in dichloromethane (DCM, 150 mL), followed by addition of N-bromosuccinimide (NBS, 10.6 g, 59.8 mmol 1.0 eq.). The reaction mixture was stirred at room temperature for 2 hours. Upon completion of the reaction, the solid product was collected by filtration and washed with dichloromethane (100 mL x 2) to give the final 2-amino-5-bromo-3-methoxybenzoic acid as a gray solid (12.1 g, 82.2% yield).

References

[1] Patent: US2009/203657, 2009, A1. Location in patent: Page/Page column 50
[2] Patent: US2009/203677, 2009, A1. Location in patent: Page/Page column 53
[3] Patent: US2009/197871, 2009, A1. Location in patent: Page/Page column 52-53
[4] Patent: WO2009/100169, 2009, A1. Location in patent: Page/Page column 131
[5] Journal of Medicinal Chemistry, 2018, vol. 61, # 14, p. 6087 - 6109

2-AMINO-5-BROMO-3-METHOXYBENZOIC ACID Preparation Products And Raw materials

Raw materials

Preparation Products

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2-AMINO-5-BROMO-3-METHOXYBENZOIC ACID Suppliers

China 59 India 1 United Kingdom 2 United States 8 Global 70

Weifang Yuda Pharmaceutical Technology Co., Ltd.

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View Lastest Price from 2-AMINO-5-BROMO-3-METHOXYBENZOIC ACID manufacturers

Career Henan Chemical Co

Product: 2-AMINO-5-BROMO-3-METHOXYBENZOIC ACID 864293-44-7
Price: US $1.00/g
Min. Order: 1g
Purity: 98%
Supply Ability: 100KG
Release date: 2020-01-12

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2-AMINO-5-BROMO-3-METHOXYBENZOIC ACID

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864293-44-7