ChemicalBook > CAS DataBase List > 2-AMINO-5-BROMO-3-METHOXYBENZOIC ACID

2-AMINO-5-BROMO-3-METHOXYBENZOIC ACID

Product Name
2-AMINO-5-BROMO-3-METHOXYBENZOIC ACID
CAS No.
864293-44-7
Chemical Name
2-AMINO-5-BROMO-3-METHOXYBENZOIC ACID
Synonyms
2-AMino-5-broMo-3-Methoxybenzoic;5-Bromo-3-methoxyanthranilic Acid;2-AMINO-5-BROMO-3-METHOXYBENZOIC ACID;Benzoic acid, 2-amino-5-bromo-3-methoxy-;2-Amino-5-bromo-3-(methyloxy)benzoic acid
CBNumber
CB62455891
Molecular Formula
C8H8BrNO3
Formula Weight
246.06
MOL File
864293-44-7.mol
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2-AMINO-5-BROMO-3-METHOXYBENZOIC ACID Property

Boiling point:
356.0±42.0 °C(Predicted)
Density 
1.703±0.06 g/cm3(Predicted)
storage temp. 
Keep in dark place,Sealed in dry,Room Temperature
pka
4.43±0.10(Predicted)
Appearance
Off-white to light yellow Solid
InChI
InChI=1S/C8H8BrNO3/c1-13-6-3-4(9)2-5(7(6)10)8(11)12/h2-3H,10H2,1H3,(H,11,12)
InChIKey
YSBGYQUUOKRQAT-UHFFFAOYSA-N
SMILES
C(O)(=O)C1=CC(Br)=CC(OC)=C1N
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Safety

HS Code 
2916399090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P321Specific treatment (see … on this label).

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

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N-Bromosuccinimide Price

Biosynth Carbosynth
Product number
FA141359
Product name
2-Amino-5-bromo-3-methoxybenzoic acid
Packaging
100mg
Price
$83
Updated
2021/12/16
Biosynth Carbosynth
Product number
FA141359
Product name
2-Amino-5-bromo-3-methoxybenzoic acid
Packaging
250mg
Price
$165
Updated
2021/12/16
Biosynth Carbosynth
Product number
FA141359
Product name
2-Amino-5-bromo-3-methoxybenzoic acid
Packaging
500mg
Price
$290
Updated
2021/12/16
Biosynth Carbosynth
Product number
FA141359
Product name
2-Amino-5-bromo-3-methoxybenzoic acid
Packaging
1g
Price
$500
Updated
2021/12/16
SynQuest Laboratories
Product number
4657-9-10
Product name
2-Amino-5-bromo-3-methoxybenzoic acid
Packaging
500mg
Price
$584
Updated
2021/12/16
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2-AMINO-5-BROMO-3-METHOXYBENZOIC ACID Chemical Properties,Usage,Production

Synthesis

3177-80-8

864293-44-7

General procedure for the synthesis of 2-amino-5-bromo-3-methoxybenzoic acid from 2-amino-3-methoxybenzoic acid: 2-amino-3-methoxybenzoic acid (10.0 g, 59.8 mmol, 1.0 eq.) was dissolved in dichloromethane (DCM, 150 mL), followed by addition of N-bromosuccinimide (NBS, 10.6 g, 59.8 mmol 1.0 eq.). The reaction mixture was stirred at room temperature for 2 hours. Upon completion of the reaction, the solid product was collected by filtration and washed with dichloromethane (100 mL x 2) to give the final 2-amino-5-bromo-3-methoxybenzoic acid as a gray solid (12.1 g, 82.2% yield).

References

[1] Patent: US2009/203657, 2009, A1. Location in patent: Page/Page column 50
[2] Patent: US2009/203677, 2009, A1. Location in patent: Page/Page column 53
[3] Patent: US2009/197871, 2009, A1. Location in patent: Page/Page column 52-53
[4] Patent: WO2009/100169, 2009, A1. Location in patent: Page/Page column 131
[5] Journal of Medicinal Chemistry, 2018, vol. 61, # 14, p. 6087 - 6109

2-AMINO-5-BROMO-3-METHOXYBENZOIC ACID Preparation Products And Raw materials

Raw materials

Preparation Products

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2-AMINO-5-BROMO-3-METHOXYBENZOIC ACID Suppliers

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View Lastest Price from 2-AMINO-5-BROMO-3-METHOXYBENZOIC ACID manufacturers

Career Henan Chemical Co
Product
2-AMINO-5-BROMO-3-METHOXYBENZOIC ACID 864293-44-7
Price
US $1.00/g
Min. Order
1g
Purity
98%
Supply Ability
100KG
Release date
2020-01-12

864293-44-7, 2-AMINO-5-BROMO-3-METHOXYBENZOIC ACIDRelated Search:

3-BROMO-5-BENZYLOXY-2,6-DINITROBENZOIC ACID BENZYL ESTER 3-BROMO-5-METHOXY-2,6-DINITRO-BENZOIC ACID METHYL ESTER (2-AMINO-5-BROMO-3-METHOXYPHENYL)METHANOL 2-AMINO-5-BROMO-3-METHOXYBENZOIC ACID

  • 2-AMINO-5-BROMO-3-METHOXYBENZOIC ACID
  • 2-AMino-5-broMo-3-Methoxybenzoic
  • 2-Amino-5-bromo-3-(methyloxy)benzoic acid
  • Benzoic acid, 2-amino-5-bromo-3-methoxy-
  • 5-Bromo-3-methoxyanthranilic Acid
  • 864293-44-7