4-CHLORO-3-IODOANILINE
- Product Name
- 4-CHLORO-3-IODOANILINE
- CAS No.
- 573764-31-5
- Chemical Name
- 4-CHLORO-3-IODOANILINE
- Synonyms
- 3-iodo-4-chloroaniline;4-CHLORO-3-IODOANILINE;4-Chloro-3-iodoaniline97%;4-Chloro-3-iodobenzenamine;4-Chloro-3-iodoaniline 97%;4-Chloro-3-iodo-phenylamine;BenzenaMine, 4-chloro-3-iodo-
- CBNumber
- CB62457259
- Molecular Formula
- C6H5ClIN
- Formula Weight
- 253.47
- MOL File
- 573764-31-5.mol
4-CHLORO-3-IODOANILINE Property
- Melting point:
- 70 °C
- Boiling point:
- 322.3±27.0 °C(Predicted)
- Density
- 2.015±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- form
- solid
- pka
- 3.00±0.10(Predicted)
- color
- Brown to very dark brown
Safety
- HS Code
- 2921420090
N-Bromosuccinimide Price
- Product number
- C368798
- Product name
- 4-Chloro-3-iodoaniline
- Packaging
- 100mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- OR46038
- Product name
- 4-Chloro-3-iodoaniline
- Purity
- 97%
- Packaging
- 250mg
- Price
- $85
- Updated
- 2021/12/16
- Product number
- 3630-M-X1
- Product name
- 4-Chloro-3-iodoaniline
- Packaging
- 250mg
- Price
- $93
- Updated
- 2021/12/16
- Product number
- 6136AJ
- Product name
- 4-Chloro-3-iodoaniline
- Packaging
- 5g
- Price
- $158
- Updated
- 2021/12/16
- Product number
- OR46038
- Product name
- 4-Chloro-3-iodoaniline
- Purity
- 97%
- Packaging
- 1g
- Price
- $170
- Updated
- 2021/12/16
4-CHLORO-3-IODOANILINE Chemical Properties,Usage,Production
Synthesis
74534-15-9
573764-31-5
2) Preparation of 4-chloro-3-iodoaniline (compounds 1-4): a mixture of compounds 1-3 (37 g, 0.13 mol), iron powder (29.3 g, 0.52 mol), and NH4Cl (7 g, 0.13 mol) was dissolved in EtOH/H2O (200 mL/100 mL) and the reaction was stirred for 3 hr at 75 °C. Upon completion of the reaction, the reaction mixture was filtered and concentrated under reduced pressure to remove most of the EtOH. the remaining mixture was extracted with ethyl acetate, washed sequentially with water and saturated saline, and the organic phase was dried with anhydrous Na2SO4. After concentration under reduced pressure, 3-iodo-4-chloroaniline (compounds 1-4) was obtained as a yellow solid (32 g, 97% yield).LCMS: m/z 254.0 [M + 1]+.1H NMR (400 MHz, CDCl3): δ 3.65 (br, 2H), 6.58 (dd, J = 8.8 Hz, 2.4 Hz, 1H), 7.15-7.17 (m, 2H).
References
[1] Patent: US2014/18368, 2014, A1. Location in patent: Paragraph 0162; 0164
[2] European Journal of Medicinal Chemistry, 2017, vol. 141, p. 721 - 733
[3] Journal of the American Chemical Society, 2007, vol. 129, # 51, p. 15919 - 15926
[4] Journal of the Chemical Society, 1951, p. 1774,1778
[5] Bioorganic and Medicinal Chemistry Letters, 2009, vol. 19, # 19, p. 5576 - 5581
4-CHLORO-3-IODOANILINE Preparation Products And Raw materials
Raw materials
Preparation Products
4-CHLORO-3-IODOANILINE Suppliers
- Tel
- tp@aladdinsci.com
- Country
- United States
- ProdList
- 57505
- Advantage
- 58
- Tel
- +1-817863-6948 +1-（817）863-6948
- sales@aceschem.com
- Country
- United States
- ProdList
- 19632
- Advantage
- 58
- Tel
- --
- Fax
- --
- info@synthonix.com
- Country
- United States
- ProdList
- 6872
- Advantage
- 58
- Tel
- --
- Fax
- --
- sales@combi-blocks.com
- Country
- United States
- ProdList
- 6618
- Advantage
- 69
- Tel
- --
- Fax
- --
- info@synquestlabs.com
- Country
- United States
- ProdList
- 6871
- Advantage
- 62
- Tel
- --
- Fax
- --
- sales@matrixscientific.com
- Country
- United States
- ProdList
- 6632
- Advantage
- 80
View Lastest Price from 4-CHLORO-3-IODOANILINE manufacturers
- Product
- 4-chloro-3-iodoaniline 573764-31-5
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 200kg
- Release date
- 2018-12-25