1H-PYRROLO[2,3-C]PYRIDINE-2-CARBOXYLIC ACID ETHYL ESTER

Uses

Product Name: 1H-PYRROLO[2,3-C]PYRIDINE-2-CARBOXYLIC ACID ETHYL ESTER
CAS No.: 24334-19-8
Chemical Name: 1H-PYRROLO[2,3-C]PYRIDINE-2-CARBOXYLIC ACID ETHYL ESTER
Synonyms: Ethyl 6-azaindole-2-carbo...;Ethyl 6-azaindole-2-carboxylate;1H-pyrrolo[2,3-c]pyridine-2-carboxylate;6-azaindole-2-carboxylic acid ethyl ester;(E)-ethyl 3-(3-aminopyridin-4-yl)acrylate;ethyl 1H-pyrrolo[2,3-c]pyridine-2-carboxylate;ethyl 1H-pyrrolo[2,3-c]pyridine-2-carbo×ylate;ETHYL 1H-PYRR0L0E2, 3- C]PYRIDINE-2-CARB0XYLATE;1H-PYRROLO[2,3-C]PYRIDINE-2-CARBOXYLIC ACID ETHYL ESTER
CBNumber: CB62458357
Molecular Formula: C10H10N2O2
Formula Weight: 190.2
MOL File: 24334-19-8.mol

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1H-PYRROLO[2,3-C]PYRIDINE-2-CARBOXYLIC ACID ETHYL ESTER Property

Melting point:: 207-208 °C
Boiling point:: 371.8±22.0 °C(Predicted)
Density: 1.272±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 12.67±0.40(Predicted)
Appearance: White to off-white Solid

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Safety

HS Code: 2933998090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P312Call a POISON CENTER or doctor/physician if you feel unwell.

P321Specific treatment (see … on this label).

P330Rinse mouth.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

P403+P233Store in a well-ventilated place. Keep container tightly closed.

P405Store locked up.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC

Product number: E927680
Product name: Ethyl1H-Pyrrolo[2,3-c]pyridine-2-carboxylate
Packaging: 100mg
Price: $65
Updated: 2021/12/16

Apolloscientific

Product number: OR922142
Product name: Ethyl1H-pyrrolo[2,3-c]pyridine-2-carboxylate
Purity: 95%
Packaging: 250mg
Price: $225
Updated: 2021/12/16

AK Scientific

Product number: 1795AB
Product name: Ethyl1H-pyrrolo[2,3-c]pyridine-2-carboxylate
Packaging: 1g
Price: $351
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H58-1-J2
Product name: Ethyl 6-azaindole-2-carboxylate
Packaging: 1g
Price: $375
Updated: 2021/12/16

Apolloscientific

Product number: OR922142
Product name: Ethyl1H-pyrrolo[2,3-c]pyridine-2-carboxylate
Purity: 95%
Packaging: 1g
Price: $555
Updated: 2021/12/16

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1H-PYRROLO[2,3-C]PYRIDINE-2-CARBOXYLIC ACID ETHYL ESTER Chemical Properties,Usage,Production

Uses

Ethyl 1H-pyrrolo[2,3-c]pyridine-2-carboxylate is a useful research chemical.

Synthesis

95-92-1

180253-66-1

24334-19-8

1. tert-Butyl (4-methylpyridin-3-yl)carbamate (3.5 g, 16.8 mmol) was dissolved in anhydrous THF (30 ml) and cooled to -40 °C under argon protection. 2. tert-butyl lithium (20.7 ml, 1.7 M pentane solution, 35.2 mmol) was added slowly and the reaction mixture was kept stirred at -40 °C for 1 hour. 3. A solution of diethyl oxalate (2.5 ml, 18.5 mmol) in THF (30 ml) was added dropwise over 15 min. 4. the reaction mixture was warmed to 0 °C and stirring was continued for 2 h. The reaction mixture was then slowly warmed to room temperature and stirred for 19 h. The reaction mixture was then stirred for 1 h. The reaction mixture was then slowly warmed to room temperature. 5. 2N HCl (110 ml) was carefully added to the reaction mixture and heated to reflux for 2 hours. 6. After cooling, the organic phase was extracted by adding dichloromethane (100 ml) and the aqueous phase pH was adjusted to 8 and the organic phase was separated. 7. The aqueous phase was washed with dichloromethane (2 x 50 ml), the organic layers were combined, dried with magnesium sulfate and concentrated to give a light brown solid. 8. The solid was ground with ethyl acetate and the beige solid product (586 mg, 18%) was collected by filtration. LCMS (Method B): RT = 1.89min, M + H + = 190.

References

[1] Patent: US2010/216768, 2010, A1. Location in patent: Page/Page column 16-17

1H-PYRROLO[2,3-C]PYRIDINE-2-CARBOXYLIC ACID ETHYL ESTER Preparation Products And Raw materials

Raw materials

Preparation Products

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1H-PYRROLO[2,3-C]PYRIDINE-2-CARBOXYLIC ACID ETHYL ESTER Suppliers

China 82 India 4 Switzerland 1 United Kingdom 1 United States 11 Global 99

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View Lastest Price from 1H-PYRROLO[2,3-C]PYRIDINE-2-CARBOXYLIC ACID ETHYL ESTER manufacturers

Career Henan Chemical Co

Product: 1H-PYRROLO[2,3-C]PYRIDINE-2-CARBOXYLIC ACID ETHYL ESTER 24334-19-8
Price: US $8.00/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: 10tons
Release date: 2018-12-24

24334-19-8, 1H-PYRROLO[2,3-C]PYRIDINE-2-CARBOXYLIC ACID ETHYL ESTERRelated Search:

6-AZAINDOLE-3-CARBOXYLIC ACID METHYL 1H-PYRROLO[3,2-B]PYRIDINE-5-CARBOXYLATE 1H-Pyrrolo[3,2-b]pyridine-3-aceticacid(8CI,9CI) 1H-Pyrido[2,3-b][1,4]oxazin-2(3H)-one(9CI) 1H-Pyrrolo[3,2-c]pyridine-2-carboxylic acid, Methyl ester 1H-Pyrrolo[2,3-b]pyridine-3-carboxylic acid, methyl ester METHYL 1H-PYRROLO[3,2-B]PYRIDINE-2-CARBOXYLATE 1H-pyrrolo[3,2-b]pyridine-3-carboxylic acid 1H-Pyrrolo[3,2-c]pyridine-3-ethanamine 1,5-Dihydropyrrolo[3,2-a]pyrimidine-2,4-dion (1H-Pyrrolo[2,3-c]pyridin-3-yl)MethanaMine methyl 1H-pyrrolo[3,2-b]pyridine-3-carboxylate 2-b]pyridin-3-aMine dihydrochloride 3-Cyano-4-azaindole Methyl 6-azaindole-3-carboxylate 1H-PYRROLO[3,2-B]PYRIDINE-2-CARBOXYLIC ACID 1H-PYRROLO[3,2-B]PYRIDINE-2-CARBALDEHYDE 1H-PYRAZOLO[3,4-B]PYRAZIN-3-AMINE

1H-PYRROLO[2,3-C]PYRIDINE-2-CARBOXYLIC ACID ETHYL ESTER

ethyl 1H-pyrrolo[2,3-c]pyridine-2-carboxylate

Ethyl 6-azaindole-2-carboxylate

Ethyl 6-azaindole-2-carbo...

ethyl 1H-pyrrolo[2,3-c]pyridine-2-carbo×ylate

(E)-ethyl 3-(3-aminopyridin-4-yl)acrylate

1H-pyrrolo[2,3-c]pyridine-2-carboxylate

6-azaindole-2-carboxylic acid ethyl ester

ETHYL 1H-PYRR0L0E2, 3- C]PYRIDINE-2-CARB0XYLATE

24334-19-8