7-Nitro-1,2,3,4-tetrahydroquinoline
- Product Name
- 7-Nitro-1,2,3,4-tetrahydroquinoline
- CAS No.
- 30450-62-5
- Chemical Name
- 7-Nitro-1,2,3,4-tetrahydroquinoline
- Synonyms
- 7-Nitro-1;7-Nitro-1,2,3,4-Terahydroquinoline;7-NITRO-1,2,3,4-TETRAHYDROQUINOLINE;1,2,3,4-TETRAHYDRO-7-NITROQUINOLINE;7-Nitro-1,2,3,4-tetrahydroquinoline>Quinoline, 1,2,3,4-tetrahydro-7-nitro-;7-Nitro-1,2,3,4-tetrahydroquinoline,95%;7-NITRO-1,2,3,4-TETRAHYDRO-QUINOLINE HYDROCHLORIDE;7-Nitro-1,2,3,4-tetrahydroquinoline 1,2,3,4-Tetrahydro-7-nitroquinoline
- CBNumber
- CB6246251
- Molecular Formula
- C9H10N2O2
- Formula Weight
- 178.19
- MOL File
- 30450-62-5.mol
7-Nitro-1,2,3,4-tetrahydroquinoline Property
- Melting point:
- 61.0 to 65.0 °C
- Boiling point:
- 325.2±31.0 °C(Predicted)
- Density
- 1.236±0.06 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Sealed in dry,Room Temperature
- solubility
- soluble in Methanol
- pka
- 3.44±0.20(Predicted)
- form
- Powder
- color
- Red
- CAS DataBase Reference
- 30450-62-5(CAS DataBase Reference)
N-Bromosuccinimide Price
- Product number
- MNO000018
- Product name
- 7-Nitro-1,2,3,4-tetrahydroquinoline
- Purity
- Aldrich
- Packaging
- 1g
- Price
- $70.9
- Updated
- 2024/03/01
- Product number
- N0955
- Product name
- 7-Nitro-1,2,3,4-tetrahydroquinoline
- Purity
- >98.0%(GC)(T)
- Packaging
- 5g
- Price
- $77
- Updated
- 2024/03/01
- Product number
- N0955
- Product name
- 7-Nitro-1,2,3,4-tetrahydroquinoline
- Purity
- >98.0%(GC)(T)
- Packaging
- 25g
- Price
- $249
- Updated
- 2024/03/01
- Product number
- H61612
- Product name
- 7-Nitro-1,2,3,4-tetrahydroquinoline, 95%
- Packaging
- 1g
- Price
- $41.65
- Updated
- 2024/03/01
- Product number
- H61612
- Product name
- 7-Nitro-1,2,3,4-tetrahydroquinoline, 95%
- Packaging
- 5g
- Price
- $179.65
- Updated
- 2024/03/01
7-Nitro-1,2,3,4-tetrahydroquinoline Chemical Properties,Usage,Production
Uses
7-Nitro-1,2,3,4-tetrahydroquinoline is a quinoline compound that can be used as a reagent in chemical reactions or as an intermediate in organic synthesis. It can be used to prepare 7-Aminoquinoline and 7-Nitroquinoline.
Synthesis
7-Nitro-1,2,3,4-tetrahydroquinoline is synthesised by the reaction of 1,2,3,4-tetrahydroquinoline and nitric acid in sulphuric acid solution. The specific synthesis steps are as follows:
Concentrated sulfuric acid (30.00 mL) was cooled to -10° C. with an ice/salt bath.
To this, 1,2,3,4-tetrahydro-quinoline (10.60 g, 75.60 mmol) and a solution of nitric acid (99.5percent, 4.80 g, 75.60 mmol) in sulfuric acid (15.00 mL) were added simultaneously within 1 hour, so that the temperature of the reaction mixture does not exceed 10° C.
The mixture was stirred then for 2.5 hours at -5° C., then poured over ice and treated with sodium carbonate (0.10 kg) until pH 8-9 was reached.
The solid was filtered, washing with water, then dissolved in dichloromethane.
The organic phase was washed with water, dried over magnesium sulphate and evaporated.
7-Nitro-1,2,3,4-tetrahydro-quinoline was obtained as a viscous brown oil, 13.70 g (85percent), 84percent purity.
7-Nitro-1,2,3,4-tetrahydroquinoline Preparation Products And Raw materials
Raw materials
Preparation Products
7-Nitro-1,2,3,4-tetrahydroquinoline Suppliers
- Tel
- 03-36680489
- Fax
- 03-3668-0520
- Sales-JP@TCIchemicals.com
- Country
- Japan
- ProdList
- 28387
- Advantage
- 80
View Lastest Price from 7-Nitro-1,2,3,4-tetrahydroquinoline manufacturers
- Product
- 7-Nitro-1,2,3,4-tetrahydroquinoline 30450-62-5
- Price
- US $0.00/G
- Min. Order
- 10G
- Purity
- 98%min
- Supply Ability
- 300KG/month
- Release date
- 2023-01-10
- Product
- 1,2,3,4-TETRAHYDRO-7-NITROQUINOLINE 30450-62-5
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 100KG
- Release date
- 2019-12-25