3-Ethynylpiperidine hydrochloride
- Product Name
- 3-Ethynylpiperidine hydrochloride
- CAS No.
- 959918-19-5
- Chemical Name
- 3-Ethynylpiperidine hydrochloride
- Synonyms
- 3-ETHYNYLPIPERIDINE HCL;3-Ethynylpiperidine hydrochloride;Piperidine, 3-ethynyl-, hydrochloride (1:1)
- CBNumber
- CB62490050
- Molecular Formula
- C7H12ClN
- Formula Weight
- 145.63
- MOL File
- 959918-19-5.mol
3-Ethynylpiperidine hydrochloride Property
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- Appearance
- White to yellow Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P321Specific treatment (see … on this label).
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
N-Bromosuccinimide Price
- Product number
- E939510
- Product name
- 3-Ethynylpiperidinehydrochloride
- Packaging
- 50mg
- Price
- $110
- Updated
- 2021/12/16
- Product number
- Y6534
- Product name
- 3-Ethynyl-piperidinehydrochloride
- Packaging
- 100mg
- Price
- $149
- Updated
- 2021/12/16
- Product number
- Y6534
- Product name
- 3-Ethynyl-piperidinehydrochloride
- Packaging
- 250mg
- Price
- $192
- Updated
- 2021/12/16
- Product number
- AS40990
- Product name
- 3-Ethynylpiperidine HCl
- Purity
- 95%
- Packaging
- 250mg
- Price
- $229
- Updated
- 2021/12/16
- Product number
- 119218
- Product name
- 3-Ethynylpiperidine hydrochloride
- Purity
- 95+%
- Packaging
- 250mg
- Price
- $389
- Updated
- 2021/12/16
3-Ethynylpiperidine hydrochloride Chemical Properties,Usage,Production
Synthesis
664362-16-7
959918-19-5
General procedure for the synthesis of 3-ethynylpiperidine hydrochloride from 3-ethynylpiperidine-1-carboxylic acid tert-butyl ester: Preparation of Intermediate 35 (Method V); Synthesis of 3-ethynylpiperidine hydrochloride: to Intermediate 33 (1.50 g, 7.18 mmol) was added a dioxane solution (50 mL) of 4 M HCl. The reaction mixture was stirred at room temperature for 16 hours. After completion of the reaction, the mixture was concentrated in vacuum. The residue was ground with ether (Et2O) to give 3-alkynylpiperidine hydrochloride (0.91 g, 86% yield).1H NMR (DMSO-d6) δ: 9.02 (2H, br.s), 3.38-3.24 (1H, m), 3.21-3.08 (2H, m), 2.94-2.76 (3H, m), 2.00-1.87 (1H, m), 1.83-1.73 (1H, m), 1.73-1.60 (1H, m), 1.60-1.48 (1H, m).
References
[1] Patent: WO2007/141504, 2007, A1. Location in patent: Page/Page column 59
[2] Bioorganic and Medicinal Chemistry Letters, 2016, vol. 26, # 8, p. 1993 - 1996
3-Ethynylpiperidine hydrochloride Preparation Products And Raw materials
Raw materials
Preparation Products
3-Ethynylpiperidine hydrochloride Suppliers
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View Lastest Price from 3-Ethynylpiperidine hydrochloride manufacturers
- Product
- 3-Ethynylpiperidine hydrochloride 959918-19-5
- Price
- US $1.00/g
- Min. Order
- 1g
- Purity
- 99%
- Supply Ability
- 200kg
- Release date
- 2019-12-26