N-(4-Bromobenzyl)-2-butyl-4-chloro-1H-imidazole-5-carboxyaldehyde

Product Name: N-(4-Bromobenzyl)-2-butyl-4-chloro-1H-imidazole-5-carboxyaldehyde
CAS No.: 143722-29-6
Chemical Name: N-(4-Bromobenzyl)-2-butyl-4-chloro-1H-imidazole-5-carboxyaldehyde
Synonyms: Butanoicacid,4-chloro-6-oxo-;1-(1H-1,3-BENZODIAZOL-2-YL)-1H-PYRAZOL-7-AMINE;1-(4-bromobenzyl)-2-butyl-4-chloro-1H-imidazole-5-carbaldehyde;N-(4-Bromobenzyl)-2-butyl-4-chloro-1H-imidazole-5-carboxyaldehyde;3-[(4-Bromophenyl)methyl]-2-butyl-5-chloroimidazole-4-carbaldehyde;1-[(4-BroMophenyl)Methyl]-2-butyl-4-chloro-1H-iMidazole-5-carboxaldehyde;1H-Imidazole-5-carboxaldehyde, 1-[(4-bromophenyl)methyl]-2-butyl-4-chloro-
CBNumber: CB62503134
Molecular Formula: C15H16BrClN2O
Formula Weight: 355.66
MOL File: 143722-29-6.mol

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N-(4-Bromobenzyl)-2-butyl-4-chloro-1H-imidazole-5-carboxyaldehyde Property

storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
solubility: soluble in Chloroform, Dichloromethane, Ethyl Acetate, Methanol

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B680195
Product name: N-(4-Bromobenzyl)-2-butyl-4-chloro-1H-imidazole-5-carboxyaldehyde
Packaging: 50mg
Price: $155
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB19202
Product name: N-(4-Bromobenzyl)-2-butyl-4-chloro-1H-imidazole-5-carboxyaldehyde
Packaging: 50mg
Price: $254.5
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB19202
Product name: N-(4-Bromobenzyl)-2-butyl-4-chloro-1H-imidazole-5-carboxyaldehyde
Packaging: 100mg
Price: $462
Updated: 2021/12/16

AK Scientific

Product number: 2808AQ
Product name: 1-(4-Bromobenzyl)-2-butyl-4-chloro-1H-imidazole-5-carbaldehyde
Packaging: 1g
Price: $622.4
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB19202
Product name: N-(4-Bromobenzyl)-2-butyl-4-chloro-1H-imidazole-5-carboxyaldehyde
Packaging: 250mg
Price: $840
Updated: 2021/12/16

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N-(4-Bromobenzyl)-2-butyl-4-chloro-1H-imidazole-5-carboxyaldehyde Chemical Properties,Usage,Production

Uses

Intermediate in the production of Sartan derivatives

Synthesis

83857-96-9

589-15-1

143722-29-6

Example 14 Synthesis of 1-(4-bromobenzyl)-2-butyl-4-chloro-1H-imidazole-5-carbaldehyde 2-n-butyl-4-chloro-1H-imidazole-5-carboxaldehyde (111.9 g, 0.6 mol), p-bromobenzyl bromide (153.02 g, 0.6 mol), anhydrous potassium carbonate (103.5 g, 0.75 mol), and dry N,N-dimethylacetamide (900 mL) were mixed and the reaction was stirred for 4 hours at room temperature. After completion of the reaction, the reaction mixture was diluted with toluene (1.2 L) and water (1.8 L) and stirring was continued for 30 min. After standing and stratifying, the organic layer was separated and washed twice with 900 mL of water. The organic layer was dried with magnesium sulfate and filtered to remove the desiccant. The filtrate was concentrated and the residue was dried by vacuum pump overnight to give 191.71 g of the target product in 89.9% yield.

References

[1] Patent: US5310928, 1994, A
[2] Patent: US5130439, 1992, A

N-(4-Bromobenzyl)-2-butyl-4-chloro-1H-imidazole-5-carboxyaldehyde Preparation Products And Raw materials

Raw materials

Preparation Products

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N-(4-Bromobenzyl)-2-butyl-4-chloro-1H-imidazole-5-carboxyaldehyde Suppliers

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143722-29-6, N-(4-Bromobenzyl)-2-butyl-4-chloro-1H-imidazole-5-carboxyaldehydeRelated Search:

1H-Imidazole-5-carboxaldehyde, 1-[(4-bromophenyl)methyl]-2-butyl-4-chloro-

N-(4-Bromobenzyl)-2-butyl-4-chloro-1H-imidazole-5-carboxyaldehyde

1-[(4-BroMophenyl)Methyl]-2-butyl-4-chloro-1H-iMidazole-5-carboxaldehyde

1-(4-bromobenzyl)-2-butyl-4-chloro-1H-imidazole-5-carbaldehyde

3-[(4-Bromophenyl)methyl]-2-butyl-5-chloroimidazole-4-carbaldehyde

Butanoicacid,4-chloro-6-oxo-

1-(1H-1,3-BENZODIAZOL-2-YL)-1H-PYRAZOL-7-AMINE

143722-29-6

C15H16BrClN2O

Aromatics

Heterocycles

Intermediates