2-(6-methylpyridin-3-yl)acetic acid

Product Name: 2-(6-methylpyridin-3-yl)acetic acid
CAS No.: 19733-96-1
Chemical Name: 2-(6-methylpyridin-3-yl)acetic acid
Synonyms: 2-(6-Methylpyridin-3-yl);6-Methyl-3-pyridineacetic acid;3-Pyridineacetic acid, 6-methyl-;2-(6-Methyl-3-pyridyl)acetic Acid;2-(6-methylpyridin-3-yl)acetic acid
CBNumber: CB62534862
Molecular Formula: C8H9NO2
Formula Weight: 151.16
MOL File: 19733-96-1.mol

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2-(6-methylpyridin-3-yl)acetic acid Property

Melting point:: 73-74 °C
Boiling point:: 125-127 °C
Density: 1.196±0.06 g/cm3(Predicted)
storage temp.: Inert atmosphere,Room Temperature
pka: 3.68±0.10(Predicted)
Appearance: Off-white to light yellow Solid
InChI: InChI=1S/C8H9NO2/c1-6-2-3-7(5-9-6)4-8(10)11/h2-3,5H,4H2,1H3,(H,10,11)
InChIKey: DWTRPWLHNATUPX-UHFFFAOYSA-N
SMILES: C1=NC(C)=CC=C1CC(O)=O

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Safety

Hazard Codes: Xn
Risk Statements: 22
HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: M341175
Product name: 2-(6-Methylpyridin-3-yl)aceticacid
Packaging: 50mg
Price: $65
Updated: 2021/12/16

Apolloscientific

Product number: OR952061
Product name: 2-(6-Methylpyridin-3-yl)aceticacid
Purity: 95%
Packaging: 250mg
Price: $130
Updated: 2021/12/16

Matrix Scientific

Product number: 082453
Product name: (6-Methylpyridin-3-yl)acetic acid
Purity: 97%
Packaging: 500mg
Price: $181
Updated: 2021/12/16

Matrix Scientific

Product number: 082453
Product name: (6-Methylpyridin-3-yl)acetic acid
Purity: 97%
Packaging: 1g
Price: $278
Updated: 2021/12/16

Apolloscientific

Product number: OR952061
Product name: 2-(6-Methylpyridin-3-yl)aceticacid
Purity: 95%
Packaging: 1g
Price: $345
Updated: 2021/12/16

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2-(6-methylpyridin-3-yl)acetic acid Chemical Properties,Usage,Production

Synthesis

19733-95-0

19733-96-1

Example 3: Preparation of 2-methyl-5-pyridylacetic acid; 2-(6-methylpyridin-3-yl)morpholinoethylthione (25 g) was dissolved in 200 mL of ethanol, followed by addition of a 60% aqueous NaOH solution (21 g NaOH dissolved in 25 mL of water). The reaction mixture was heated to 80 °C and refluxed for 17 hours. After completion of the reaction, it was cooled to room temperature and the solvent was removed by rotary evaporation. A small amount of water was added to dissolve the residue and the pH was adjusted with concentrated hydrochloric acid to 2. The insoluble material was removed by filtration and the filtrate was extracted twice with ether, the ether layers were combined and washed once with distilled water. The aqueous layer was retained and set aside. The water in the solvent was removed by rotary evaporation and the product was dried in a vacuum drying oven for 24 h to give 2-methyl-5-pyridylacetic acid (11 g) in about 70% yield. The product was characterized by 1H-NMR (400 MHz, DMSO-d6): δ 2.43 (3H, s, CH3); 3.57 (2H, s, CH2); 7.17-7.19 (1H, d, ArH); 7.53-7.56 (1H, dd, ArH); 8.30-8.31 (1H, d, ArH); 12.42 (1H, s , COOH).

References

[1] Patent: EP2417973, 2012, A1. Location in patent: Page/Page column 6-8; 16
[2] Patent: US2012/122914, 2012, A1. Location in patent: Page/Page column 5
[3] Patent: WO2010/67085, 2010, A2. Location in patent: Page/Page column 60-61

2-(6-methylpyridin-3-yl)acetic acid Preparation Products And Raw materials

Raw materials

Preparation Products

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2-(6-methylpyridin-3-yl)acetic acid Suppliers

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19733-96-1, 2-(6-methylpyridin-3-yl)acetic acidRelated Search:

2-(6-Methylpyridin-3-yl)

2-(6-methylpyridin-3-yl)acetic acid

6-Methyl-3-pyridineacetic acid

2-(6-Methyl-3-pyridyl)acetic Acid

3-Pyridineacetic acid, 6-methyl-

19733-96-1