ChemicalBook > CAS DataBase List > 2,3-difluoro-4-nitro-Phenol

2,3-difluoro-4-nitro-Phenol

Product Name
2,3-difluoro-4-nitro-Phenol
CAS No.
123173-60-4
Chemical Name
2,3-difluoro-4-nitro-Phenol
Synonyms
2,3-difluoro-4-nitro-Phenol;Phenol, 2,3-difluoro-4-nitro-
CBNumber
CB62582520
Molecular Formula
C6H3F2NO3
Formula Weight
175.09
MOL File
123173-60-4.mol
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2,3-difluoro-4-nitro-Phenol Property

Boiling point:
307.4±42.0 °C(Predicted)
Density 
1.619
storage temp. 
2-8°C
pka
4.98±0.24(Predicted)
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Safety

HS Code 
2908990000
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H317May cause an allergic skin reaction

H318Causes serious eye damage

H410Very toxic to aquatic life with long lasting effects

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P272Contaminated work clothing should not be allowed out of the workplace.

P273Avoid release to the environment.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P333+P313IF SKIN irritation or rash occurs: Get medical advice/attention.

P391Collect spillage. Hazardous to the aquatic environment

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC
Product number
D452758
Product name
2,3-Difluoro-4-nitrophenol
Packaging
50mg
Price
$45
Updated
2021/12/16
TRC
Product number
D452758
Product name
2,3-Difluoro-4-nitrophenol
Packaging
100mg
Price
$90
Updated
2021/12/16
AK Scientific
Product number
X0147
Product name
2,3-Difluoro-4-nitrophenol
Packaging
5g
Price
$481
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0362579
Product name
2,3-DIFLUORO-4-NITROPHENOL
Purity
95.00%
Packaging
5MG
Price
$504.93
Updated
2021/12/16
AK Scientific
Product number
J98479
Product name
2,3-Difluoro-4-nitrophenol
Packaging
10g
Price
$600
Updated
2021/12/16
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2,3-difluoro-4-nitro-Phenol Chemical Properties,Usage,Production

Synthesis

6418-38-8

123173-60-4

General procedure for the synthesis of 2,3-difluoro-4-nitrophenol from 2,3-difluorophenol: Step a: Nitration reaction To a solution of 2,3-difluorophenol (52.0 g, 400.0 mmol) in dichloromethane (DCM, 500.0 mL) was slowly added 70% nitric acid (HNO3, 28.0 mL, 400.0 mmol) dropwise at 0 °C. The reaction mixture was gradually warmed to room temperature and stirring was continued at 0 °C for 30 min. Upon completion of the reaction, the precipitate was collected by filtration, washed with deionized water and subsequently dried under vacuum to afford 20 g of the target product 2,3-difluoro-4-nitrophenol (white solid) in 29% yield.

References

[1] Patent: WO2012/178015, 2012, A2. Location in patent: Page/Page column 138-139

2,3-difluoro-4-nitro-Phenol Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 2,3-difluoro-4-nitro-Phenol manufacturers

Career Henan Chemical Co
Product
2,3-difluoro-4-nitro-Phenol 123173-60-4
Price
US $1.00/KG
Min. Order
1KG
Purity
97%
Supply Ability
100kg
Release date
2020-02-01

123173-60-4, 2,3-difluoro-4-nitro-PhenolRelated Search:


  • 2,3-difluoro-4-nitro-Phenol
  • Phenol, 2,3-difluoro-4-nitro-
  • 123173-60-4