ChemicalBook > CAS DataBase List > 2-BROMO-6-CHLOROBENZYL BROMIDE

2-BROMO-6-CHLOROBENZYL BROMIDE

Product Name: 2-BROMO-6-CHLOROBENZYL BROMIDE
CAS No.: 75002-98-1
Chemical Name: 2-BROMO-6-CHLOROBENZYL BROMIDE
Synonyms: -3-chlorobenzene;1-Bromo-2-(bromomethyl);2-bromo-6-chlorobromobenzyl;2-BROMO-6-CHLOROBENZYL BROMIDE;2-Bromo-6-chlorobenzyl bromide 97%;1-BroMo-2-(broMoMethyl)-3-chlorobenzene;Benzene, 1-bromo-2-(bromomethyl)-3-chloro-;1-Bromo-2-(bromomethyl)-3-chlorobenzene, 2-Chloro-alpha,6-dibromotoluene
CBNumber: CB6259907
Molecular Formula: C7H5Br2Cl
Formula Weight: 284.38
MOL File: Mol file

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2-BROMO-6-CHLOROBENZYL BROMIDE Property

Melting point:: 62-64°C
Boiling point:: 283.4±25.0 °C(Predicted)
Density: 1.93g/ml
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
Appearance: Light brown to off-white Solid

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Safety

RIDADR: UN1759
HazardClass: 8
HS Code: 2903998090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word: Danger
Hazard statements: H314Causes severe skin burns and eye damage
Precautionary statements: P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

Oakwood

Product number: 019489
Product name: 2-Bromo-6-chlorobenzylbromide
Purity: 98%
Packaging: 5g
Price: $225
Updated: 2021/12/16

SynQuest Laboratories

Product number: 1700-D-04
Product name: 2-Bromo-6-chlorobenzyl bromide
Purity: 97%
Packaging: 1g
Price: $240
Updated: 2021/12/16

Oakwood

Product number: 019489
Product name: 2-Bromo-6-chlorobenzylbromide
Purity: 98%
Packaging: 1g
Price: $75
Updated: 2021/12/16

AK Scientific

Product number: 1665AC
Product name: 1-Bromo-2-(bromomethyl)-3-chlorobenzene
Packaging: 250mg
Price: $77
Updated: 2021/12/16

SynQuest Laboratories

Product number: 1700-D-04
Product name: 2-Bromo-6-chlorobenzyl bromide
Purity: 97%
Packaging: 5G
Price: $600
Updated: 2021/12/16

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2-BROMO-6-CHLOROBENZYL BROMIDE Chemical Properties,Usage,Production

Synthesis

62356-27-8

75002-98-1

General procedure for the synthesis of 2-bromo-6-chlorobenzyl bromide (compound [5-2]) from 2-bromo-6-chlorotoluene: 2-bromo-6-chlorotoluene (1.58 g) was dissolved in 15 mL of carbon tetrachloride, and N-bromosuccinimide (1.63 g) and 2,2'-azino-bis (isobutyronitrile) (125 mg) were added. The reaction mixture was heated to reflux for 24 hours. After completion of the reaction, the reaction was quenched with water and the mixture was extracted with chloroform. The organic layers were combined, dried over anhydrous sodium sulfate, filtered and the filtrate concentrated under reduced pressure. The resulting residue was purified by silica gel column chromatography to afford 2-bromo-6-chlorobenzyl bromide (2.16 g) as a white solid.1H-NMR (400 MHz, CDCl3) δ: 7.51 (1H, d, J = 8.1 Hz), 7.37 (1H, d, J = 8.1 Hz), 7.11 (1H, d, J = 8.1 Hz), 4.80 (2H, s) .

References

[1] Organic and Biomolecular Chemistry, 2012, vol. 10, # 31, p. 6404 - 6409
[2] Journal of Medicinal Chemistry, 1981, vol. 24, # 4, p. 382 - 389
[3] Patent: US4259349, 1981, A
[4] Journal of the American Chemical Society, 2008, vol. 130, # 45, p. 15157 - 15166
[5] Journal of the American Chemical Society, 2011, vol. 133, # 24, p. 9282 - 9285

2-BROMO-6-CHLOROBENZYL BROMIDE Preparation Products And Raw materials

Raw materials

Preparation Products

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75002-98-1, 2-BROMO-6-CHLOROBENZYL BROMIDERelated Search:

2-Bromo-6-chlorobenzyl bromide 97%

2-BROMO-6-CHLOROBENZYL BROMIDE

1-BroMo-2-(broMoMethyl)-3-chlorobenzene

1-Bromo-2-(bromomethyl)-3-chlorobenzene, 2-Chloro-alpha,6-dibromotoluene

1-Bromo-2-(bromomethyl)

Benzene, 1-bromo-2-(bromomethyl)-3-chloro-

2-bromo-6-chlorobromobenzyl

-3-chlorobenzene

75002-98-1

C7H5Br2Cl