Ethyl 3-oxocyclohexane-1-carboxylate

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Ethyl 3-oxocyclohexane-1-carboxylate

Product Name: Ethyl 3-oxocyclohexane-1-carboxylate
CAS No.: 33668-25-6
Chemical Name: Ethyl 3-oxocyclohexane-1-carboxylate
Synonyms: ETHYL 3-OXOCYCLOHEXANECARBOXYLATE;Ethyl 3-oxo-cyclohexane formate;Ethyl Cyclohexanone-β-carboxylate;ETHYL 3-OXOCYCLOHEXANE-l-CARBOXYLATE;ETHYL 3-OXOCYCLOHEXANE-1-CARBOXYLATE;Ethyl 3-oxocyclohexane-1-carboxylate 97+%;3-Cyclohexanonecarboxylic acid ethyl ester;3-Oxocyclohexanecarboxylic acid ethyl ester;3-Oxocyclohexane-1-carboxylic acid ethyl ester;Cyclohexanecarboxylic acid, 3-oxo-, ethyl ester
CBNumber: CB6265528
Molecular Formula: C9H14O3
Formula Weight: 170.21
MOL File: 33668-25-6.mol

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Ethyl 3-oxocyclohexane-1-carboxylate Property

Boiling point:: 249℃
Density: 1.083
Flash point:: 104℃
storage temp.: 2-8°C
InChI: InChI=1S/C9H14O3/c1-2-12-9(11)7-4-3-5-8(10)6-7/h7H,2-6H2,1H3
InChIKey: YLRVJPQVDQQBOX-UHFFFAOYSA-N
SMILES: C1(C(OCC)=O)CCCC(=O)C1

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Safety

Hazard Codes: Xi
Risk Statements: 41
Safety Statements: 26-39
Hazard Note: Irritant
HS Code: 2918199890

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: E908940
Product name: EthylCyclohexanone-β-carboxylate
Packaging: 2.5g
Price: $250
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0003534
Product name: ethyl 3-oxocyclohexane-1-carboxylate
Purity: 95.00%
Packaging: 1G
Price: $941.33
Updated: 2021/12/16

Rieke Metals

Product number: 7591
Product name: ethyl 3-oxocyclohexane-1-carboxylate
Purity: 97%
Packaging: 5g
Price: $1514
Updated: 2021/12/16

SynQuest Laboratories

Product number: 2229-1-X3
Product name: Ethyl 3-oxocyclohexane-1-carboxylate
Packaging: 100mg
Price: $31
Updated: 2021/12/16

Oakwood

Product number: 067079
Product name: Ethyl3-Oxocyclohexanecarboxylate
Purity: 98%
Packaging: 250mg
Price: $40
Updated: 2021/12/16

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Ethyl 3-oxocyclohexane-1-carboxylate Chemical Properties,Usage,Production

Uses

Ethyl Cyclohexanone-β-carboxylate is an intermediate used to prepare carbazole-carboxamides with selective JAK2 inhibitory activities.

Synthesis Reference(s)

Journal of the American Chemical Society, 110, p. 2565, 1988 DOI: 10.1021/ja00216a033

Synthesis

To a round bottom flask was added 3-oxo-1-cyclohexanecarboxylic acid (3.85 g, 27.1 mmol), ethanol (7.91 mL), p-toluenesulfonic acid (0.097 g, 0.56 mmol) and toluene (65.9 mL). The mixture was refluxed with a Dean-star trap overnight. The reaction mixture was cooled down and concentrated under reduced pressure to afford 4.61 g (100 %) of the title compound, 3-oxo-cyclohexanecarboxylic acid ethyl ester (Ethyl 3-oxocyclohexane-1-carboxylate), as a yellow oil.

Ethyl 3-oxocyclohexane-1-carboxylate Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from Ethyl 3-oxocyclohexane-1-carboxylate manufacturers

Shanghai Yongzeng Technology Co.,Ltd

Product: ethyl-3-oxocyclohexanecarboxylate 33668-25-6
Price: US $0.00/gm
Min. Order: 100gm
Purity: 96%min
Supply Ability: 100kgs
Release date: 2024-09-10

Shaanxi Dideu Medichem Co. Ltd

Product: ETHYL 3-OXOCYCLOHEXANE-1-CARBOXYLATE 33668-25-6
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 20T
Release date: 2024-08-15

Zhuozhou Wenxi import and Export Co., Ltd

Product: Ethyl 3-oxocyclohexane-1-carbo xylate 33668-25-6
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-07-10

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33668-25-6

Esters

Ring Systems