(3-BroMo-4-Methylphenyl)Methanol
- Product Name
- (3-BroMo-4-Methylphenyl)Methanol
- CAS No.
- 68120-35-4
- Chemical Name
- (3-BroMo-4-Methylphenyl)Methanol
- Synonyms
- 3-Bromo-4-methylbenzyl alcohol;3-Bromo-4-methylbenzenemethanol;(3-BroMo-4-Methylphenyl)Methanol;Benzenemethanol, 3-bromo-4-methyl-
- CBNumber
- CB62672814
- Molecular Formula
- C8H9BrO
- Formula Weight
- 201.06
- MOL File
- 68120-35-4.mol
(3-BroMo-4-Methylphenyl)Methanol Property
- Melting point:
- 38-42°C
- Boiling point:
- 283.4±25.0 °C(Predicted)
- Density
- 1.481±0.06 g/cm3(Predicted)
- Flash point:
- >110℃
- storage temp.
- Sealed in dry,Room Temperature
- form
- powder
- pka
- 14.29±0.10(Predicted)
- Appearance
- White to off-white Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- 759732
- Product name
- 3-Bromo-4-methylbenzyl alcohol
- Purity
- 97%
- Packaging
- 1g
- Price
- $49.2
- Updated
- 2023/01/07
- Product number
- B678453
- Product name
- (3-Bromo-4-methylphenyl)methanol
- Packaging
- 100mg
- Price
- $75
- Updated
- 2021/12/16
- Product number
- FB160845
- Product name
- (3-Bromo-4-methylphenyl) methanol
- Packaging
- 1g
- Price
- $90
- Updated
- 2021/12/16
- Product number
- Z0777
- Product name
- 3-Bromo-4-methylbenzyl alcohol
- Packaging
- 1g
- Price
- $101
- Updated
- 2021/12/16
- Product number
- FB160845
- Product name
- (3-Bromo-4-methylphenyl) methanol
- Packaging
- 500mg
- Price
- $50
- Updated
- 2021/12/16
(3-BroMo-4-Methylphenyl)Methanol Chemical Properties,Usage,Production
Synthesis
7697-26-9
68120-35-4
GENERAL METHODS: 3-Bromo-4-methylbenzoic acid (20.70 g, 81.82 mmol) was dissolved in tetrahydrofuran (THF, 250 mL) and the solution was cooled to 0°C. Borane-THF complex (1.0 M in THF, 164 mL) was slowly added under stirring. The reaction mixture was gradually warmed to room temperature and stirring was continued for 2 hours. Upon completion of the reaction, the reaction was quenched with saturated sodium carbonate solution (Na2CO3, 100 mL). Subsequently, the reaction mixture was extracted with ethyl acetate (EtOAc, 3 x 100 mL). The organic layers were combined, dried with anhydrous magnesium sulfate (MgSO4), filtered and concentrated under reduced pressure to give the crude product as a colorless liquid. The crude product was further purified by distillation under reduced pressure (0.8 mbar) and the fractions distilled at 90 °C were collected to give 3-bromo-4-methylbenzyl alcohol (16.30 g, 99%) as a colorless liquid.
References
[1] Journal of Medicinal Chemistry, 2013, vol. 56, # 21, p. 8432 - 8454
[2] Synlett, 2014, vol. 25, # 1, p. 123 - 127
[3] Journal of Organic Chemistry, 1985, vol. 50, # 2, p. 283 - 284
[4] Patent: US2003/195259, 2003, A1
[5] Patent: WO2006/101977, 2006, A2. Location in patent: Page/Page column 112
(3-BroMo-4-Methylphenyl)Methanol Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from (3-BroMo-4-Methylphenyl)Methanol manufacturers
- Product
- 3-Bromo-4-methylbenzyl Alcohol 68120-35-4
- Price
- US $130.00-240.00/g
- Min. Order
- 1g
- Purity
- 99%
- Supply Ability
- 20tons
- Release date
- 2025-08-20
- Product
- 3-BroMo-4-Methylphenyl)Methanol 68120-35-4
- Price
- US $5.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 100KG
- Release date
- 2020-01-12