3-Bromobenzamide
- Product Name
- 3-Bromobenzamide
- CAS No.
- 22726-00-7
- Chemical Name
- 3-Bromobenzamide
- Synonyms
- 3-BROMOBENZAMIDE;M-BROMOBENZAMIDE;META-BROMOBENZAMIDE;TIMTEC-BB SBB009893;Benzamide, m-bromo-;Benzamide, 3-bromo-;Bromophenyl formamide;3-(Carbamoyl)bromobenzene
- CBNumber
- CB6278007
- Molecular Formula
- C7H6BrNO
- Formula Weight
- 200.03
- MOL File
- 22726-00-7.mol
3-Bromobenzamide Property
- Melting point:
- 156-159℃
- Boiling point:
- 297.4±23.0 °C(Predicted)
- Density
- 1.61
- refractive index
- 1.5500 (estimate)
- Flash point:
- 134℃
- storage temp.
- Sealed in dry,Room Temperature
- pka
- 15.38±0.50(Predicted)
- form
- Solid
- color
- White
- CAS DataBase Reference
- 22726-00-7(CAS DataBase Reference)
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P405Store locked up.
N-Bromosuccinimide Price
- Product number
- TMT00344
- Product name
- 3-Bromobenzamide
- Packaging
- 1 g
- Price
- $550
- Updated
- 2025/07/31
- Product number
- B5178
- Product name
- 3-Bromobenzamide
- Purity
- >98.0%(HPLC)(N)
- Packaging
- 5g
- Price
- $37
- Updated
- 2025/07/31
- Product number
- B5178
- Product name
- 3-Bromobenzamide
- Purity
- >98.0%(HPLC)(N)
- Packaging
- 25g
- Price
- $114
- Updated
- 2025/07/31
- Product number
- B680333
- Product name
- 3-Bromobenzamide
- Packaging
- 2.5g
- Price
- $65
- Updated
- 2021/12/16
- Product number
- FB70047
- Product name
- 3-Bromobenzamide
- Packaging
- 250g
- Price
- $205
- Updated
- 2021/12/16
3-Bromobenzamide Chemical Properties,Usage,Production
Synthesis
585-76-2
22726-00-7
Under argon protection, 820 mg of 3-bromobenzoic acid (4.0 mmol) was suspended in 14 mL of a 6:1 dichloromethane (DCM)/acetonitrile (MeCN) solvent mixture, to which 800 mg of HOBt (4.44 mmol) and 861 mg of EDOHCl (4.4 mmol) were added. After stirring for 10 min, the mixture changed to a clarified solution, which was subsequently cooled to 0 °C in an ice bath. In another round-bottomed flask, 1.64 g NaOH (40 mmol) was added to 2.8 mL of 28% NH4OH solution (20 mmol), and the resulting gaseous NH3 was passed through a NaOH trap and then drummed into the reaction vessel. After stopping the NH3 drumming, the reaction mixture was concentrated under reduced pressure and the residue was dissolved in ethyl acetate (AcOEt, 60 mL) and washed sequentially with 5% KHSO4 (2 × 30 mL), water (20 mL), 5% NaHCO3 (3 × 20 mL) and brine (20 mL). The organic phase was dried with Na2SO4, filtered and evaporated to dryness under reduced pressure to give 700 mg of 3-bromobenzamide in 87% yield.
References
[1] Patent: WO2017/12890, 2017, A1. Location in patent: Page/Page column 28
[2] Phosphorus, Sulfur and Silicon and the Related Elements, 2007, vol. 182, # 3, p. 657 - 666
[3] Tetrahedron Letters, 2005, vol. 46, # 40, p. 6879 - 6882
[4] Journal of Organic Chemistry, 2003, vol. 68, # 16, p. 6431 - 6434
[5] Chemische Berichte, 1871, vol. 4, p. 707
3-Bromobenzamide Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 3-Bromobenzamide manufacturers
- Product
- 3-Bromobenzamide 22726-00-7
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 2000
- Release date
- 2025-09-25
- Product
- 3-Bromobenzamide 22726-00-7
- Price
- US $15.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 500ton/Month
- Release date
- 2021-07-29
- Product
- 3-Bromobenzamide 22726-00-7
- Price
- US $1.00/KG
- Min. Order
- 1G
- Purity
- 98%
- Supply Ability
- 1000KG
- Release date
- 2018-08-10