ChemicalBook > CAS DataBase List > (6-METHOXY-PYRIDIN-2-YL)-METHANOL

(6-METHOXY-PYRIDIN-2-YL)-METHANOL

Product Name: (6-METHOXY-PYRIDIN-2-YL)-METHANOL
CAS No.: 63071-12-5
Chemical Name: (6-METHOXY-PYRIDIN-2-YL)-METHANOL
Synonyms: Zinc04352715;6-Methoxy-2-PyridineMethanol;(6-methoxy-2-pyridyl)methanol;2-Pyridinemethanol,6-methoxy-;(6-methoxy-2-pyridinyl)methanol;(6-METHOXY-PYRIDIN-2-YL)-METHANOL;6-Methoxy-2-(hydroxymethyl)pyridine
CBNumber: CB6291352
Molecular Formula: C7H9NO2
Formula Weight: 139.15
MOL File: 63071-12-5.mol

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(6-METHOXY-PYRIDIN-2-YL)-METHANOL Property

Boiling point:: 72-73 °C(Press: 0.06 Torr)
Density: 1.155±0.06 g/cm3(Predicted)
storage temp.: Inert atmosphere,Room Temperature
pka: 13.22±0.10(Predicted)
Appearance: Colorless to light yellow Liquid

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Safety

Hazard Codes: Xi,Xn
Risk Statements: 22
WGK Germany: 3
HazardClass: IRRITANT
HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: ADE000358
Product name: (6-Methoxy-pyridin-2-yl)-methanol
Purity: Aldrich
Packaging: 1g
Price: $463
Updated: 2023/01/07

TRC

Product number: M222805
Product name: (6-Methoxypyridin-2-yl)methanol
Packaging: 50mg
Price: $90
Updated: 2021/12/16

TRC

Product number: M222805
Product name: (6-Methoxypyridin-2-yl)methanol
Packaging: 250mg
Price: $310
Updated: 2021/12/16

Matrix Scientific

Product number: 023791
Product name: (6-Methoxy-pyridin-2-yl)-methanol
Purity: 97%
Packaging: 250mg
Price: $124
Updated: 2021/12/16

Matrix Scientific

Product number: 023791
Product name: (6-Methoxy-pyridin-2-yl)-methanol
Purity: 97%
Packaging: 500g
Price: $191
Updated: 2021/12/16

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(6-METHOXY-PYRIDIN-2-YL)-METHANOL Chemical Properties,Usage,Production

Synthesis

26256-72-4

63071-12-5

General procedure for the synthesis of 6-methoxy-2-pyridinemethanol from 6-methoxypyridine-2-carboxylic acid methyl ester: 6-methoxypyridine-2-carboxylic acid methyl ester (2 g, 11.96 mmol) was dissolved in anhydrous methanol (20 mL) and cooled down to 0 °C under nitrogen protection. Sodium borohydride (1.36 g, 35.89 mmol) was slowly added and the reaction system was kept stirred at 0 °C for 30 min. Subsequently, the reaction system was slowly warmed to room temperature and stirring was continued for 1 hour. After completion of the reaction, the reaction was quenched with water and the reaction mixture was concentrated on a rotary evaporator. The concentrated mixture was diluted with brine (100 mL) and then extracted with a mixture of dichloromethane and 2-propanol (2:1, 3 x 150 mL, by volume). The organic phases were combined, dried with magnesium sulfate, filtered, and concentrated on a rotary evaporator to give 6-methoxy-2-pyridinemethanol (500 mg, 30% yield) as an oily product. Mass spectrometry analysis showed [M+H]+ calculated value of 140.1 and measured value of 140.1.

References

[1] Patent: US2009/274632, 2009, A1
[2] Patent: US9247759, 2016, B2. Location in patent: Page/Page column 303
[3] Patent: US2016/376263, 2016, A1. Location in patent: Paragraph 0469; 0470
[4] Patent: WO2014/3483, 2014, A1. Location in patent: Page/Page column 34
[5] Patent: WO2011/79076, 2011, A1. Location in patent: Page/Page column 93

(6-METHOXY-PYRIDIN-2-YL)-METHANOL Preparation Products And Raw materials

Raw materials

Preparation Products

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(6-METHOXY-PYRIDIN-2-YL)-METHANOL Suppliers

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(6-METHOXY-PYRIDIN-2-YL)-METHANOL

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(6-methoxy-2-pyridyl)methanol

(6-methoxy-2-pyridinyl)methanol

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63071-12-5