TITANIUM(III) FLUORIDE
- Product Name
- TITANIUM(III) FLUORIDE
- CAS No.
- 13470-08-1
- Chemical Name
- TITANIUM(III) FLUORIDE
- Synonyms
- TiF3;TSCS(13470-08-1);TITANIUM FLUORIDE;TITANIUM TRIFLUORIDE;itanium(III)fluoride;TITANIUM(III) FLUORIDE;titaniumfluoride(tif3);Titanium fluoride(F3Ti);Titanium fluoride (TiF3);Titanium(III)fluoride99%
- CBNumber
- CB6377711
- Molecular Formula
- F3Ti
- Formula Weight
- 104.86
- MOL File
- 13470-08-1.mol
TITANIUM(III) FLUORIDE Property
- Melting point:
- 1200 °C
- Boiling point:
- 1400 °C
- Density
- 3.4 g/mL at 25 °C(lit.)
- solubility
- insoluble in H2O, dilute acid solutions, alkaline solutions
- form
- Crystalline Powder
- Specific Gravity
- 3.4
- color
- Red to brown
- Water Solubility
- Sparingly soluble. It hydrolyses in water.
- Sensitive
- Air & Moisture Sensitive
- Crystal Structure
- VF3 type
- crystal system
- Three sides
- Space group
- R3c
- Lattice constant
a/nm b/nm c/nm α/o β/o γ/o V/nm3 0.543 0.543 1.364 90 90 120 0.3488 - Exposure limits
- ACGIH: TWA 2.5 mg/m3
NIOSH: IDLH 250 mg/m3; TWA 2.5 mg/m3 - CAS DataBase Reference
- 13470-08-1(CAS DataBase Reference)
- EPA Substance Registry System
- Titanium fluoride (TiF3) (13470-08-1)
Safety
- Hazard Codes
- C
- Risk Statements
- 20/21/22-34-32-14
- Safety Statements
- 26-36/37/39-45
- RIDADR
- UN 3260 8/PG 2
- WGK Germany
- 3
- F
- 10
- Hazard Note
- Corrosive
- TSCA
- Yes
- HazardClass
- 8
- PackingGroup
- II
- HS Code
- 28261990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H314Causes severe skin burns and eye damage
- Precautionary statements
-
P260Do not breathe dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P363Wash contaminated clothing before reuse.
N-Bromosuccinimide Price
- Product number
- 399817
- Product name
- Titanium(III) fluoride
- Packaging
- 5g
- Price
- $63.7
- Updated
- 2024/03/01
- Product number
- 013079
- Product name
- Titanium(III) fluoride
- Packaging
- 10g
- Price
- $57.65
- Updated
- 2024/03/01
- Product number
- 013079
- Product name
- Titanium(III) fluoride
- Packaging
- 50g
- Price
- $273
- Updated
- 2023/06/20
- Product number
- 93-2224
- Product name
- Titanium(III) fluoride, min. 98%
- Packaging
- 5g
- Price
- $41
- Updated
- 2024/03/01
- Product number
- 93-2224
- Product name
- Titanium(III) fluoride, min. 98%
- Packaging
- 25g
- Price
- $149
- Updated
- 2024/03/01
TITANIUM(III) FLUORIDE Chemical Properties,Usage,Production
Chemical Properties
Red to brown crystalline powder
Blue rhombic crystals are stable in air and unusually resistant to acids and bases. Sublimation begins at about 930°C in a less than 0.1 mm vacuum. M.p. >1100°C; d%5 2.98. Insoluble in water and alcohol. Disproportionation to TiF4 and Ti begins at 950°C.
Uses
It is used as a laboratory chemicals & for manufacture of chemicals.
Production Methods
Titanium metal is hydrogenated at 600-700°C. It is then placed in a small nickel boat and inserted into the horizontal nickel tube (closed at one end). The hydride is fluorinated with gaseous HF. The open end of the tube has a cooling jacket and is sealed with picein to a copper cover. Two copper tubes are silver-soldered into the cover and serve as an inlet and outlet for the hydrogen; the inlet tube also contains a concentric silver tube for introducing HF. The output gases pass through an empty polyethylene bottle, a bubble counter filled with paraffin oil and a polyethylene trap to freeze excess HF gas. The closed end of the reaction tube is placed in a tubular furnace. The temperature is measured externally. After thoroughly flushing the apparatus with Hs, fluorination followed with a 1 4 mixture of H2 and HF for four to five hours. The HF flow is first started at a temperature above 200°C. The water temperature in the cooling jacket should be higher than 20°C to prevent condensation of the HF. After completion of the fluorination, the product is left to cool in a stream of hydrogen. The yield is 90%.
TITANIUM(III) FLUORIDE Preparation Products And Raw materials
Raw materials
Preparation Products
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