CYCLOHEXANE-1,3-DICARBOXYLIC ACID DIMETHYL ESTER
Application- Product Name
- CYCLOHEXANE-1,3-DICARBOXYLIC ACID DIMETHYL ESTER
- CAS No.
- 62638-06-6
- Chemical Name
- CYCLOHEXANE-1,3-DICARBOXYLIC ACID DIMETHYL ESTER
- Synonyms
- diMethyl cyclohexane-1,3-dicarboxylate;Dimethyl 1,3-cyclohexane dicarboxylate;Dimethyl cyclohexane-1,3-dixarboxylate;1,3-dimethyl cyclohexane-1,3-dicarboxylate;CYCLOHEXANE-1,3-DICARBOXYLIC ACID DIMETHYL ESTER;1,3-Cyclohexanedicarboxylic acid, 1,3-dimethyl ester
- CBNumber
- CB6403544
- Molecular Formula
- C10H16O4
- Formula Weight
- 200.23
- MOL File
- 62638-06-6.mol
CYCLOHEXANE-1,3-DICARBOXYLIC ACID DIMETHYL ESTER Property
- Boiling point:
- 258.1±15.0℃ (760 Torr)
- Density
- 1.102±0.06 g/cm3 (20 ºC 760 Torr)
- refractive index
- 1.4592 (589.3 nm 18℃)
- Flash point:
- 120.7±18.8℃
- storage temp.
- Sealed in dry,Room Temperature
- Appearance
- Colorless to light yellow Liquid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- D482570
- Product name
- dimethylcyclohexane-1,3-dicarboxylate
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- D482570
- Product name
- dimethylcyclohexane-1,3-dicarboxylate
- Packaging
- 100mg
- Price
- $65
- Updated
- 2021/12/16
- Product number
- FD142268
- Product name
- Dimethyl cyclohexane-1,3-dicarboxylate
- Packaging
- 50mg
- Price
- $67
- Updated
- 2021/12/16
- Product number
- FD142268
- Product name
- Dimethyl cyclohexane-1,3-dicarboxylate
- Packaging
- 100mg
- Price
- $116
- Updated
- 2021/12/16
- Product number
- FD142268
- Product name
- Dimethyl cyclohexane-1,3-dicarboxylate
- Packaging
- 250mg
- Price
- $230
- Updated
- 2021/12/16
CYCLOHEXANE-1,3-DICARBOXYLIC ACID DIMETHYL ESTER Chemical Properties,Usage,Production
Application
Dimethyl 1,3-cyclohexanoate can be used as a pharmaceutical synthesis intermediate and an organic synthesis intermediate, mainly in laboratory research and development processes and chemical and pharmaceutical synthesis processes.
Synthesis
67-56-1
3971-31-1
62638-06-6
1. cyclohexane-1,3-dicarboxylic acid (10.32 g, 60 mmol) was dissolved in methanol (130 mL). 2. Concentrated sulfuric acid (2.5 mL) was added as a catalyst and the reaction mixture was heated to reflux and stirred for 16 hours. 3. Upon completion of the reaction, the reaction mixture was concentrated under reduced pressure to remove most of the methanol. 4. The residue was adjusted to pH 7 with saturated aqueous sodium bicarbonate. 5. The aqueous phase was extracted with ethyl acetate (200 mL × 3) and the organic layers were combined. 6. 6. The organic layer was dried over anhydrous sodium sulfate, filtered and concentrated under reduced pressure to give dimethyl 1,3-cyclohexanedioate as a colorless oil (12 g, 100% yield). 7. The product was analyzed by 1H NMR. 7. The product was characterized by 1H NMR (400 MHz, DMSO-d6) and mass spectrometry (ESI): 1H NMR δ 3.61 (s, 6H), 2.69-1.13 (m, 10H); MS (ESI) m/e [M + 1] 201.1.
References
[1] Patent: WO2016/161960, 2016, A1. Location in patent: Paragraph 0542
[2] Acta Crystallographica Section C: Crystal Structure Communications, 2013, vol. 69, # 7, p. 727 - 729
[3] Patent: WO2012/88365, 2012, A1. Location in patent: Page/Page column 24
[4] Patent: WO2013/40535, 2013, A2. Location in patent: Page/Page column 23
[5] Patent: WO2016/106623, 2016, A1. Location in patent: Page/Page column 122
CYCLOHEXANE-1,3-DICARBOXYLIC ACID DIMETHYL ESTER Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from CYCLOHEXANE-1,3-DICARBOXYLIC ACID DIMETHYL ESTER manufacturers
- Product
- Dimethyl cyclohexane-1,3-dixarboxylate 62638-06-6
- Price
- US $0.00/gm
- Min. Order
- 100gm
- Purity
- 97%
- Supply Ability
- 100kgs
- Release date
- 2024-09-11