3-(4-PHENYL-2-PYRIDYL)-5-PHENYL-1,2,4-TRIAZINE DISULFONIC ACID, DISODIUM SALT

Product Name: 3-(4-PHENYL-2-PYRIDYL)-5-PHENYL-1,2,4-TRIAZINE DISULFONIC ACID, DISODIUM SALT
CAS No.: 108775-03-7
Chemical Name: 3-(4-PHENYL-2-PYRIDYL)-5-PHENYL-1,2,4-TRIAZINE DISULFONIC ACID, DISODIUM SALT
Synonyms: PPTS;3-(4-PHENYL-2-PYRIDYL)-5-PHENYL-1,2,4-TRIAZINE DISULFONIC ACID, DISODIUM SALT;3-(4-PHENYL-2-PYRIDYL)-5-PHENYL-1,2,4-TRIAZINE DISULFONIC ACID, DISODIUM SALT (PPTS);3-(4-PHENYL-2-PYRIDYL)-5-PHENYL-1,2,4-TRIAZINE DISULFONIC ACID, DISODIUM SALT, (PPTS)3-(4-PHENYL-2-PYRIDYL)-5-PHENYL-1,2,4-TRIAZINE DISULFONIC ACID, DISODIUM SALT, (PPTS)3-(4-PHENYL-2-PYRIDYL)-5-PHENYL-1,2,4-TRIAZINE DISULFONIC ACID, DISODIUM SALT, (PPTS)
CBNumber: CB6410773
Molecular Formula: C20H15N4NaO6S2
Formula Weight: 494.47
MOL File: 108775-03-7.mol

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

American Custom Chemicals Corporation

Product number: CHM0290027
Product name: 3-(4-PHENYL-2-PYRIDYL)-5-PHENYL-1,2,4-TRIAZINE DISULFONIC ACID DISODIUM SALT
Purity: 98.00%
Packaging: 10G
Price: $1824.9
Updated: 2021/12/16

AHH

Product number: MT-21288
Product name: 3-(4-Phenyl-2-pyridyl)-5-phenyl-1,2,4-triazinedisulfonicaciddisodiumsalt
Purity: 98%
Packaging: 10g
Price: $330
Updated: 2021/12/16

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3-(4-PHENYL-2-PYRIDYL)-5-PHENYL-1,2,4-TRIAZINE DISULFONIC ACID, DISODIUM SALT Chemical Properties,Usage,Production

Uses

3-(4-phenyl-2-pyridyl)-5-phenyl-1,2,4-triazine Disulfonic Acid, Disodium Salt is used in organometallic metallurgy, mostly in laboratory research.

Synthesis

To a solution of tert-butyl [5-[(3,4-difluorophenylcarbonyl)amino]-6-{5-[1-(phenylethylaminocarbonyl)-piperidin-4-ylmethyl]-[1,2,4]oxadiazol-3-yl}-6-(tert-butyldimethylsilyloxy)-hexyl]-carbamate (150 mg, 0.29 mmol) and 3-[5-(sulfonylphenyl)-2-pyridinyl]-1,2,. 4-triazin-5-ylbenzenesulfonic acid to a solution of disodium salt (PPTS) (5 mg, mmol) in THF (10 mL), 1N TBAF in THF (0.28 mL, 0.28 mmol). The mixture was stirred at room temperature for 30 min and diluted with EtOAc (60 mL). The solution was washed with saturated NaHCO3 and brine. The organic phase was dried, filtered and concentrated under reduced pressure. To a solution of the crude product cooled in an ice bath in CH2Cl2 (8 mL) was added Dess-Martin sodium periodate (199 mg, 0.47 mmol). The mixture was stirred for 3 hours and diluted with ether (10 mL). Saturated NaHCO3 (4 mL) and 20% Na2S2O3 (4 mL) were added to the mixture. The mixture was stirred until the layers separated. The mixture was diluted with ether (30 mL) and washed with saturated NaHCO3 and brine. The organic phase was dried over MgSO4, filtered and concentrated under reduced pressure. The crude mixture was purified by column chromatography (50%-100% EtOAc/hexane) to afford sodium 3-(4-phenyl-2-pyridyl)-5-phenyl-1,2,4-thiazinedisulfonate (78 mg, 67% yield).

3-(4-PHENYL-2-PYRIDYL)-5-PHENYL-1,2,4-TRIAZINE DISULFONIC ACID, DISODIUM SALT Preparation Products And Raw materials

Raw materials

Preparation Products

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3-(4-PHENYL-2-PYRIDYL)-5-PHENYL-1,2,4-TRIAZINE DISULFONIC ACID, DISODIUM SALT Suppliers

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108775-03-7, 3-(4-PHENYL-2-PYRIDYL)-5-PHENYL-1,2,4-TRIAZINE DISULFONIC ACID, DISODIUM SALTRelated Search:

4-Phenylpyridine 3-(4-PHENYL-2-PYRIDYL)-5-PHENYL-1,2,4-TRIAZINE DISULFONIC ACID, DISODIUM SALT 2-METHYL-4-PHENYLPYRIDINE Pyridine methanesulfonate Sodium p-toluenesulfinate 1,2,4-Triazine 2,4-Lutidine Pyridinium p-Toluenesulfonate 3-Methyl-1,2,4-triazine

3-(4-PHENYL-2-PYRIDYL)-5-PHENYL-1,2,4-TRIAZINE DISULFONIC ACID, DISODIUM SALT

PPTS

3-(4-PHENYL-2-PYRIDYL)-5-PHENYL-1,2,4-TRIAZINE DISULFONIC ACID, DISODIUM SALT (PPTS)

3-(4-PHENYL-2-PYRIDYL)-5-PHENYL-1,2,4-TRIAZINE DISULFONIC ACID, DISODIUM SALT, (PPTS)3-(4-PHENYL-2-PYRIDYL)-5-PHENYL-1,2,4-TRIAZINE DISULFONIC ACID, DISODIUM SALT, (PPTS)3-(4-PHENYL-2-PYRIDYL)-5-PHENYL-1,2,4-TRIAZINE DISULFONIC ACID, DISODIUM SALT, (PPTS)

108775-03-7

C20H12N4O6S2Na2

C20H12N4O6S22Na