ChemicalBook > CAS DataBase List > 2-Chloro-1,10-phenanthroline

2-Chloro-1,10-phenanthroline

Product Name
2-Chloro-1,10-phenanthroline
CAS No.
7089-68-1
Chemical Name
2-Chloro-1,10-phenanthroline
Synonyms
VUF 7730;chlorophenanthroline;2-Chloro-1,10-phenan;2-Chloro-1,10-phenthroline;2-CHLORO-1,10-PHENANTHROLINE;1,10-Phenanthroline, 2-chloro-;2-Chloro-1,10-diazaphenanthrene;2-Chloro-1,10-phenanthroline >2-Chloro-1,10-phenanthroline Cas: 7089-68-1
CBNumber
CB6483144
Molecular Formula
C12H7ClN2
Formula Weight
214.65
MOL File
7089-68-1.mol
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2-Chloro-1,10-phenanthroline Property

Melting point:
130 °C
Boiling point:
391.8±22.0 °C(Predicted)
Density 
1.375
storage temp. 
under inert gas (nitrogen or Argon) at 2-8°C
solubility 
soluble in Methanol
form 
powder to crystal
pka
4.22±0.10(Predicted)
color 
White to Yellow to Orange
InChI
InChI=1S/C12H7ClN2/c13-10-6-5-9-4-3-8-2-1-7-14-11(8)12(9)15-10/h1-7H
InChIKey
JHRMQHFRVPVGHL-UHFFFAOYSA-N
SMILES
N1C2C(=CC=C3C=2N=CC=C3)C=CC=1Cl
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Safety

Safety Statements 
24/25
HS Code 
29339900
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TCI Chemical
Product number
C1560
Product name
2-Chloro-1,10-phenanthroline
Purity
>98.0%(HPLC)(T)
Packaging
1g
Price
$666
Updated
2025/07/31
TCI Chemical
Product number
C1560
Product name
2-Chloro-1,10-phenanthroline
Purity
>98.0%(HPLC)(T)
Packaging
100mg
Price
$171
Updated
2025/07/31
TRC
Product number
B419493
Product name
2-Chloro-1,10-phenanthroline
Packaging
50mg
Price
$200
Updated
2021/12/16
TRC
Product number
B419493
Product name
2-Chloro-1,10-phenanthroline
Packaging
100mg
Price
$310
Updated
2021/12/16
Biosynth Carbosynth
Product number
FC60892
Product name
2-Chloro-1,10-phenanthroline
Packaging
25mg
Price
$50
Updated
2021/12/16
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2-Chloro-1,10-phenanthroline Chemical Properties,Usage,Production

Chemical Properties

Light yellow solid

Synthesis

1891-19-6

7089-68-1

General procedure for the synthesis of 2-chloro-1,10-phenanthroline from 1,10-phenanthroline 1-oxide: the procedure was similar to General Procedure I, with the difference that the reaction conditions were adjusted to be carried out at room temperature using 1,10-phenanthroline 1-oxide (1.00 eq.), POBr3 (3.00 eq.), and DMF (1.50 eq.) at a concentration of 0.2M. General procedure I (0013) for the bromination of acridazine N-oxide was carried out as follows: an appropriate amount of acridazine N-oxide was dissolved in anhydrous CH2Cl2 (0.1 M) at 0 °C, POBr3 (1.2 eq.) was added with stirring, followed by a slow, dropwise addition of DMF (0.5 eq.) under argon gas protection. The reaction mixture was gradually warmed to 25 °C with continuous stirring until TLC showed completion of the reaction. Upon completion of the reaction, the pH was adjusted to 7-8 by slow addition of saturated aqueous sodium carbonate solution. the mixture was separated and the aqueous phase was fully extracted with CH2Cl2. All organic phases were combined, washed with brine, dried over anhydrous Na2SO4, filtered and concentrated under reduced pressure to obtain the crude product. The crude product was purified by fast column chromatography with PE/EA (100:1) as eluent.

References

[1] Tetrahedron, 2016, vol. 72, # 38, p. 5762 - 5768
[2] Journal of Organic Chemistry, 2007, vol. 72, # 7, p. 2318 - 2328
[3] Chemistry - A European Journal, 2017, vol. 23, # 27, p. 6499 - 6503
[4] Journal of Organic Chemistry, 2017, vol. 82, # 8, p. 4203 - 4215

2-Chloro-1,10-phenanthroline Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 2-Chloro-1,10-phenanthroline manufacturers

ZHENGZHOU JIUYI TIME NEW MATERIALS CO,.LTD
Product
2-Chloro[1,10]phenanthroline 7089-68-1
Price
US $1.10-9.90/KG
Min. Order
1KG
Purity
99%min
Supply Ability
100KG
Release date
2025-08-20
Henan Aochuang Chemical Co.,Ltd.
Product
2-Chloro-1,10-phenanthroline 7089-68-1
Price
US $0.00-0.00/KG
Min. Order
1KG
Purity
98%
Supply Ability
1ton
Release date
2022-10-14
Shanghai UCHEM Inc.
Product
2-chloro-1,10-phenanthroline 7089-68-1
Price
US $15.00-65.00/g
Min. Order
5g
Purity
0.98
Supply Ability
25kg
Release date
2024-10-25

7089-68-1, 2-Chloro-1,10-phenanthrolineRelated Search:

1,10-Phenanthroline hydrate o-Phenanthroline 1,7-PHENANTHROLINE Difluorochloromethane 4-Chloro-1,10-phenanthroline 5-CHLORO-1,10-PHENANTHROLINE o-Phenanthroline monohydrochloride monohydrate 2,9-Dichloro-1,10-phenanthroline 2-Chloro-1,10-phenanthroline

  • chlorophenanthroline
  • 2-CHLORO-1,10-PHENANTHROLINE
  • 2-Chloro-1,10-diazaphenanthrene
  • VUF 7730
  • 2-Chloro-1,10-phenan
  • 1,10-Phenanthroline, 2-chloro-
  • 2-Chloro-1,10-phenthroline
  • 2-Chloro-1,10-phenanthroline &gt
  • 2-Chloro-1,10-phenanthroline Cas: 7089-68-1
  • 7089-68-1