ChemicalBook > CAS DataBase List > 1-METHYL-1H-INDOLE-6-CARBOXYLIC ACID 97
1-METHYL-1H-INDOLE-6-CARBOXYLIC ACID 97
- Product Name
- 1-METHYL-1H-INDOLE-6-CARBOXYLIC ACID 97
- CAS No.
- 202745-73-1
- Chemical Name
- 1-METHYL-1H-INDOLE-6-CARBOXYLIC ACID 97
- Synonyms
- CC 44201;6-Carboxy-1-methyl-1H-indole;1-methyl-6-indolecarboxylic acid;1-Methyl-1H-indol-6-carboxylic acid;1-METHYL-1H-INDOLE-6-CARBOXYLIC ACID;1H-Indole-6-carboxylic acid, 1-methyl-;1-METHYL-1H-INDOLE-6-CARBOXYLIC ACID 97;1-Methyl-1H-indole-6-carboxylic acid 97%;1-methyl-1H-indole-6-carboxylic acid(SALTDATA: FREE)
- CBNumber
- CB6501251
- Molecular Formula
- C10H9NO2
- Formula Weight
- 175.18
- MOL File
- 202745-73-1.mol
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1-METHYL-1H-INDOLE-6-CARBOXYLIC ACID 97 Property
- Melting point:
- 197 °C
- Boiling point:
- 389.0±15.0 °C(Predicted)
- Density
- 1.24±0.1 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Sealed in dry,Room Temperature
- form
- solid
- pka
- 4.53±0.30(Predicted)
- color
- Pale yellow
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Safety
- Hazard Note
- Harmful
- HazardClass
- IRRITANT
- HS Code
- 2933998090
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Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P260Do not breathe dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P312Call a POISON CENTER or doctor/physician if you feel unwell.
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N-Bromosuccinimide Price
TRC
- Product number
- M321378
- Product name
- 1-Methyl-1H-indole-6-carboxylicAcid
- Packaging
- 100mg
- Price
- $60
- Updated
- 2021/12/16
SynQuest Laboratories
- Product number
- 4H21-1-K1
- Product name
- 1-Methyl-1H-indole-6-carboxylic acid
- Purity
- 97.0%
- Packaging
- 1g
- Price
- $192
- Updated
- 2021/12/16
Matrix Scientific
- Product number
- 063841
- Product name
- 1-Methyl-1H-indole-6-carboxylic acid
- Packaging
- 500mg
- Price
- $237
- Updated
- 2021/12/16
American Custom Chemicals Corporation
- Product number
- CHM0018155
- Product name
- 1-METHYL-1H-INDOLE-6-CARBOXYLIC ACID
- Purity
- 95.00%
- Packaging
- 250MG
- Price
- $647.36
- Updated
- 2021/12/16
American Custom Chemicals Corporation
- Product number
- CHM0018155
- Product name
- 1-METHYL-1H-INDOLE-6-CARBOXYLIC ACID
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $760.87
- Updated
- 2021/12/16
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1-METHYL-1H-INDOLE-6-CARBOXYLIC ACID 97 Chemical Properties,Usage,Production
Synthesis
1204-32-6
202745-73-1
Step 2: Synthesis of 1-methyl-1H-indole-6-carboxylic acid (167). Methyl 1-methyl-1H-indole-6-carboxylate (166, 1.24 mmol) was reacted with sodium hydroxide (0.59 g, 14.88 mmol) in a solvent mixture of methanol/THF/water (2:2:1, 7.5 mL) with stirring for 36 h at room temperature. A precipitate was generated during the reaction and the precipitate was collected by filtration followed by lyophilization overnight to afford the target product 1-methyl-6-indolecarboxylic acid (167, 0.54 g, 99% yield). Mass spectral data: calculated (Calc) 175.06, observed (Obs) 176.1.
References
[1] Patent: WO2005/30704, 2005, A1. Location in patent: Page/Page column 199-200
[2] Patent: WO2008/65508, 2008, A1. Location in patent: Page/Page column 32
[3] Heterocycles, 2006, vol. 67, # 2, p. 643 - 653
1-METHYL-1H-INDOLE-6-CARBOXYLIC ACID 97 Preparation Products And Raw materials
Raw materials
Preparation Products
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1-METHYL-1H-INDOLE-6-CARBOXYLIC ACID 97 Suppliers
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