3-BROMOPHENETHYL ALCOHOL
- Product Name
- 3-BROMOPHENETHYL ALCOHOL
- CAS No.
- 28229-69-8
- Chemical Name
- 3-BROMOPHENETHYL ALCOHOL
- Synonyms
- m-Bromophenylethanol;3-Bromophenethylacohol;Benzeneethanol, 3-broMo-;3-BROMOPHENETHYL ALCOHOL;2-(3-BROMOPHENYL)ETHANOL;3-BROMOPHENYLETHYL ALCOHOL;2-(3-Bromophenyl)ethan-1-ol;3-Bromophenethylalcohol,97%;3-Bromophenethyl alcohol 97%;2-(3-Bromophenyl)ethyl Alcohol
- CBNumber
- CB6707761
- Molecular Formula
- C8H9BrO
- Formula Weight
- 201.06
- MOL File
- 28229-69-8.mol
3-BROMOPHENETHYL ALCOHOL Property
- Boiling point:
- 107-110 °C/1 mmHg (lit.)
- Density
- 1.478 g/mL at 25 °C (lit.)
- refractive index
- n20/D 1.5732(lit.)
- Flash point:
- >230 °F
- storage temp.
- Sealed in dry,Room Temperature
- form
- Liquid
- pka
- 14.83±0.10(Predicted)
- color
- Clear colorless
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- 394521
- Product name
- 3-Bromophenethyl alcohol
- Purity
- 99%
- Packaging
- 5g
- Price
- $67.2
- Updated
- 2025/07/31
- Product number
- 394521
- Product name
- 3-Bromophenethyl alcohol
- Purity
- 99%
- Packaging
- 1g
- Price
- $25
- Updated
- 2023/06/20
- Product number
- B3517
- Product name
- 2-(3-Bromophenyl)ethyl Alcohol
- Purity
- >98.0%(GC)
- Packaging
- 5g
- Price
- $68
- Updated
- 2025/07/31
- Product number
- B3517
- Product name
- 2-(3-Bromophenyl)ethyl Alcohol
- Purity
- >98.0%(GC)
- Packaging
- 25g
- Price
- $334
- Updated
- 2025/07/31
- Product number
- B698238
- Product name
- 2-(3-Bromophenyl)ethanol
- Packaging
- 500mg
- Price
- $65
- Updated
- 2021/12/16
3-BROMOPHENETHYL ALCOHOL Chemical Properties,Usage,Production
Chemical Properties
clear colorless liquid
Uses
3-Bromophenethyl alcohol may be used as a starting material in the synthesis of its mesylate derivative (m-Br-C6H4CH2CH2OMs) by treatment with mesyl chloride.
General Description
3-Bromophenethyl alcohol is a phenethyl alcohol derivative. Its enthalpy of vaporization at boiling point has been determined.
Synthesis
1878-67-7
28229-69-8
The general procedure for the synthesis of 3-bromophenylethanol using 3-bromophenylacetic acid as starting material was as follows: to a solution of 3-bromophenylacetic acid (2.00 g, 9.3 mmol) was slowly added BH3-Me2S (7 mL of a 2M THF solution, 14.0 mmol) at 0 °C. The reaction mixture was gradually warmed up to room temperature with continuous stirring for 20 hours. Upon completion of the reaction, the mixture was again cooled to 0 °C and water (10 mL) was added dropwise to quench the reaction. Subsequently, the organic layer was separated, washed with brine (20 mL), dried over anhydrous MgSO4, filtered and concentrated under reduced pressure to give a colorless oily crude product. Purification by column chromatography (eluent: 50% EtOAc in heptane solution) resulted in 3-bromophenethyl alcohol as a colorless oil (1.47 g, 79% yield). The product was detected by mass spectrometry showing m/z 224/226 [M + H]+, and the 1H NMR (300 MHz, CDCl3) data were as follows: δ 7.41-7.35 (2H, m), 7.23-7.16 (2H, m), 3.87 (2H, t, J = 6.5 Hz), 2.86 (2H, t, J = 6.5 Hz).
References
[1] Bioorganic and Medicinal Chemistry Letters, 2007, vol. 17, # 11, p. 3018 - 3022
[2] Journal of Labelled Compounds and Radiopharmaceuticals, 2007, vol. 50, # 3, p. 183 - 188
[3] Patent: WO2008/53136, 2008, A1. Location in patent: Page/Page column 38
[4] Journal of Medicinal Chemistry, 1991, vol. 34, # 9, p. 2882 - 2891
[5] Journal of Medicinal Chemistry, 1998, vol. 41, # 3, p. 358 - 378
3-BROMOPHENETHYL ALCOHOL Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 3-BROMOPHENETHYL ALCOHOL manufacturers
- Product
- 3-BROMOPHENETHYL ALCOHOL 28229-69-8
- Price
- US $15.00-10.00/KG
- Min. Order
- 1KG
- Purity
- 99%+ HPLC
- Supply Ability
- Monthly supply of 1 ton
- Release date
- 2021-06-27
- Product
- 3-BROMOPHENETHYL ALCOHOL 28229-69-8
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 100KG
- Release date
- 2019-12-25