4.4-oxybisbenzoic chloride
Physical Form- Product Name
- 4.4-oxybisbenzoic chloride
- CAS No.
- 7158-32-9
- Chemical Name
- 4.4-oxybisbenzoic chloride
- Synonyms
- BPDC;ODBC;4.4-oxybisbenzoic chloride;ODBC/DEDC;4,4'-Oxydibenzoyl chloride;4,4-OXY-DI-BENZOYLCHLORIDE;4,4'-OXYBISBENZOYL CHLORIDE;4,4-Chloroformylphenyl ether;p,p'-Oxybis(benzoyl chloride);4,4'-Oxybis(benzoyl Chloride)
- CBNumber
- CB6734365
- Molecular Formula
- C14H8Cl2O3
- Formula Weight
- 295.12
- MOL File
- 7158-32-9.mol
4.4-oxybisbenzoic chloride Property
- Melting point:
- 22-23℃
- Boiling point:
- 404℃
- Density
- 1.386
- Flash point:
- 164℃
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- solubility
- soluble in Toluene
- form
- powder to crystaline
- color
- White to Almost white
- InChI
- InChI=1S/C14H8Cl2O3/c15-13(17)9-1-5-11(6-2-9)19-12-7-3-10(4-8-12)14(16)18/h1-8H
- InChIKey
- OSUWBBMPVXVSOA-UHFFFAOYSA-N
- SMILES
- O(C1=CC=C(C=C1)C(Cl)=O)C1=CC=C(C=C1)C(Cl)=O
Safety
- RIDADR
- UN 3261 8/PG II
- RTECS
- DM6664000
- HS Code
- 2918.99.4700
- HazardClass
- 8
- PackingGroup
- II
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H302Harmful if swallowed
H312Harmful in contact with skin
H314Causes severe skin burns and eye damage
H332Harmful if inhaled
- Precautionary statements
-
P260Do not breathe dust/fume/gas/mist/vapours/spray.
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P301+P330+P331IF SWALLOWED: Rinse mouth. Do NOT induce vomiting.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P310Immediately call a POISON CENTER or doctor/physician.
P312Call a POISON CENTER or doctor/physician if you feel unwell.
P321Specific treatment (see … on this label).
P322Specific measures (see …on this label).
P330Rinse mouth.
P363Wash contaminated clothing before reuse.
P405Store locked up.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- O0399
- Product name
- 4,4'-Oxybis(benzoyl Chloride)
- Purity
- >98.0%(HPLC)(T)
- Packaging
- 25g
- Price
- $125
- Updated
- 2025/07/31
- Product number
- O990105
- Product name
- 4,4'-Oxybis(benzoyl Chloride)
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- CHM0150419
- Product name
- 4,4-OXY-DI-BENZOYLCHLORIDE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $503.65
- Updated
- 2021/12/16
- Product number
- 131959
- Product name
- 4,4'-Oxydibenzoylchloride
- Purity
- 97%
- Packaging
- 500g
- Price
- $1797
- Updated
- 2021/12/16
- Product number
- 131959
- Product name
- 4,4'-Oxydibenzoylchloride
- Purity
- 97%
- Packaging
- 1kg
- Price
- $2700
- Updated
- 2021/12/16
4.4-oxybisbenzoic chloride Chemical Properties,Usage,Production
Physical Form
Crystal - Powder
Uses
4.4-oxybisbenzoic chloride is a useful research chemical.
Uses
4.4-oxybisbenzoic chloride is a monomer used in high-performance polymers for the preparation of a new low-temperature curing photosensitive polymer (PHA-6F). The polymer exhibits high transparency at 365 nm (i-line). The photosensitivity and contrast of the 2.4 μm thick film were 15 mJ/cm2 and 2.5, respectively.
Synthesis
4.4-oxybisbenzoic chloride is reacted with chlorine to produce 4,4'-Oxybis(benzoyl Chloride) in high yield without using a large amount of reaction solvent. A 300 ml four-necked flask equipped with a stirrer, a thermometer and a reflux condenser was charged with 90.6 g (0.40 mol) of 4,4′-oxybisbenzaldehyde and 158.6 g of PCBTF, and heated and stirred to 143 ° C. The temperature was raised to. A high pressure mercury lamp was turned on and irradiated with light. The reaction was started by supplying chlorine gas at a chlorine gas blowing rate of 0.06 mol / hour so as to maintain a reaction temperature of 143 ° C. (reflux). After 15 hours from the start of the reaction, disappearance of the raw materials was confirmed by gas chromatography, and the reaction was completed. When this was analyzed using gas chromatography, the reaction yield of 4,4'-Oxybis(benzoyl Chloride) was 98.6% by mass.
References
[1] Patent: JP2017/149660, 2017, A. Location in patent: Paragraph 0232; 0233
[2] Patent: JP2017/149650, 2017, A. Location in patent: Paragraph 0188-0189
[3] Patent: JP2017/141213, 2017, A. Location in patent: Paragraph 0117
[4] Patent: JP2017/141212, 2017, A. Location in patent: Paragraph 0186
[5] Patent: JP2017/141211, 2017, A. Location in patent: Paragraph 0148
4.4-oxybisbenzoic chloride Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 4.4-oxybisbenzoic chloride manufacturers
- Product
- 4.4-oxybisbenzoic chloride (DEDC) 7158-32-9
- Price
- US $0.00-0.00/kg
- Min. Order
- 1kg
- Purity
- ≥99.5%
- Supply Ability
- 10TM
- Release date
- 2025-10-27
- Product
- 4,4'-Oxybis(benzoyl Chloride) 7158-32-9
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 99.5%
- Supply Ability
- 10000KGS
- Release date
- 2025-05-16
- Product
- 4,4'-OXYBISBENZOYL CHLORIDE 7158-32-9
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 500000kg
- Release date
- 2024-10-28